ChemicalBook > CAS DataBase List > 6-Carboxyfluorescein

6-Carboxyfluorescein

Product Name
6-Carboxyfluorescein
CAS No.
3301-79-9
Chemical Name
6-Carboxyfluorescein
Synonyms
6-FAM;Carboxyfluorescein;6-FAM, 6-CF;6-FAM, FLUOS;6-Carboxyfluoroscein;6-CARBOXYFLUORESCEIN;6-carboxy' Uorescein;Fluorescein, 6-carboxy-;6-Carboxyfluorescein,>97%;6-Carboxyfluorescein Hydrate
CBNumber
CB7288380
Molecular Formula
C21H12O7
Formula Weight
376.32
MOL File
3301-79-9.mol
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6-Carboxyfluorescein Property

Melting point:
>300 °C(lit.)
Boiling point:
736.4±60.0 °C(Predicted)
Density 
1.73±0.1 g/cm3(Predicted)
storage temp. 
Sealed in dry,2-8°C
solubility 
DMSO: soluble
form 
Solid
pka
3.3, 4.6, 6.4, 7.0(at 25℃)
color 
Yellow to orange
PH Range
Weak green ' uorescence (6.0) to strong green ' uourescence (7.2)
λmax
492nm
BRN 
54341
Major Application
Diagnosis of hematologic cancer, nongastric diseases, detection of genetically modified wheat, chromosomes, gene expression, nucleic acid, hepatitis A virus, avian influenza virus subtype H5 and H5N1, SARS virus, herpex simplex virus
Biological Applications
Diagnosing bladder cancer; evaluating corneal endothelial barrier function; as a substrate for measuring protein kinase activity, methyltransferase activity, phospholipase activity, rhodanese activity,sulfotransferase activity;use in ophthalmology
CAS DataBase Reference
3301-79-9(CAS DataBase Reference)
EPA Substance Registry System
Spiro[isobenzofuran-1(3H),9'-[9H]xanthene]-6-carboxylic acid, 3',6'-dihydroxy-3-oxo- (3301-79-9)
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Safety

Hazard Codes 
Xi
Risk Statements 
36/37/38
Safety Statements 
26-36/37
WGK Germany 
3
10-21
HS Code 
3204 90 00
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

Precautionary statements

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P280Wear protective gloves/protective clothing/eye protection/face protection.

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N-Bromosuccinimide Price

Sigma-Aldrich
Product number
8.51072
Product name
6-Carboxyfluorescein
Purity
Novabiochem?
Packaging
25mg
Price
$53.2
Updated
2024/03/01
Sigma-Aldrich
Product number
C0662
Product name
6-Carboxyfluorescein
Purity
~97% (HPLC)
Packaging
50mg
Price
$142
Updated
2024/03/01
Sigma-Aldrich
Product number
8.51072
Product name
6-Carboxyfluorescein
Purity
Novabiochem?
Packaging
100mg
Price
$154
Updated
2024/03/01
TCI Chemical
Product number
C2478
Product name
6-Carboxyfluorescein Hydrate
Purity
>97.0%(HPLC)
Packaging
100mg
Price
$134
Updated
2024/03/01
Cayman Chemical
Product number
21233
Product name
6-Carboxyfluorescein
Purity
≥98%
Packaging
100mg
Price
$121
Updated
2024/03/01
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6-Carboxyfluorescein Chemical Properties,Usage,Production

Chemical Properties

Orange Solid

Uses

6-Carboxyfluorescein (6-FAM) is derivative of fluorescein giving stable derivative upon conjugation with biopolymers.It has been used to check the plasma membrane integrity in sperm cells. The single isomer, 6-FAM, contains a carboxylic acid that can be used to react with primary amines via carbodiimide activation of the carboxylic acid. Commercially available FAM is a mixture of two isomers, 5-FAM and 6-FAM, and the correct name is 5(6)-carboxyfluorescein.

Preparation

1,2,4-Benzenetricarboxylic anhydride (also called 4- carboxyphthalic anhydride, 25.0 g, 0.13 mol) was added to a solution of 1,3-dihydroxybenzene (also called resorcinol, 28.6 g, 0.26 mol) in methane sulfonic acid (1M). An air condenser was attached to the flask and the reaction was heated at 85 oC in an open vessel for 24 h. After cooling to room temperature, the reaction mixture was poured into 7 volumes of ice/water. An orange-yellow precipitate formed; this was collected by filtration and dried in an oven at 200 oC. This residue was recrystallized two times from methanol/hexane to give 1.0 g of 6- carboxyfluorescein methanesulfonic acid adduct preferentially crystallizes from MeOH/hexanes. The mother liquors from this procedure were collected, the solvent was removed in vacuo, and the residues were recrystallized two times from ethanol/hexanes to give 3.2 g of 5-carboxyfluorescein methanesulfonic acid adduct preferentially crystallizes from EtOH/hexanes. Finally, the mother liquors from this experiment were combined, evaporated to dryness, and recrystallized two times from methanol/hexanes to give another 3.0 g of 6-carboxyfluorescein methanesulfonic acid adduct preferentially crystallizes from MeOH/hexanes, making a total yield of 4.0 g, 40 %. Careful dropwise addition of conc. HCl(aq) to solutions of these methanesulfonic esters preferentially crystallizes from EtOH/hexanes and preferentially crystallizes from MeOH/hexanes in 4M sodium hydroxide gave 5-carboxyfluorescein and 6-carboxyfluorescein, respectively in near quantitative yield.

Definition

ChEBI: 6-carboxyfluorescein is a monocarboxylic acid. It derives from a fluorescein (lactone form).

Application

6-Carboxyfluorescein is a useful reagent for the preparation of hydrolytically stable fluorescent conjugates and is a useful starting material for the synthesis of other fluorescein-derives reagent. Fluorescein is the most common fluorescent derivatization reagent for labeling biomolecules. In addition to its relatively high absorptivity, excellent fluorescence quantum yield, and good water solubility, fluorescein has an excitation maximum that closely matches the 488 nm spectral line of the argon-ion laser.

Biochem/physiol Actions

6-Carboxyfluorescein diacetate is a membrane permeable compound. It can be hydrolysed by intracellular esterases to form a membrane impermeable bright green fluorescent molecule, 6-carboxyfluorescein.

6-Carboxyfluorescein Preparation Products And Raw materials

Raw materials

Preparation Products

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6-Carboxyfluorescein Suppliers

Suzhouhongxiong
Tel
18051745768 18051745768
Email
Suzhouhongxiong@163.com
Country
China
ProdList
70
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58
Okeanos Tech Co,. Ltd.
Tel
010-62651721 18610486005
Fax
01062651521-808
Email
minghui.yu@okeanos.com.cn
Country
China
ProdList
498
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60
Yantai Beite Chemical Technology Co., Ltd.
Tel
13853550371
Email
yang11360@163.com
Country
China
ProdList
25
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58
Nanjing Habo Medical Technology Co., Ltd.
Tel
025-85760892 13376090521
Fax
025-85766769
Email
sales@habotech.com
Country
China
ProdList
979
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60
J & K SCIENTIFIC LTD.
Tel
010-82848833 400-666-7788
Fax
86-10-82849933
Email
jkinfo@jkchemical.com
Country
China
ProdList
94657
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INTATRADE GmbH
Tel
+49 3493/605464
Fax
+49 3493/605470
Email
sales@intatrade.de
Country
Germany
ProdList
3572
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66
3B Pharmachem (Wuhan) International Co.,Ltd.
Tel
821-50328103-801 18930552037
Fax
86-21-50328109
Email
3bsc@sina.com
Country
China
ProdList
15839
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69
TCI (Shanghai) Development Co., Ltd.
Tel
021-67121386
Fax
021-67121385
Email
Sales-CN@TCIchemicals.com
Country
China
ProdList
24529
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81
Energy Chemical
Tel
021-021-58432009 400-005-6266
Fax
021-58436166
Email
sales8178@energy-chemical.com
Country
China
ProdList
44689
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61
Beijing Ouhe Technology Co., Ltd
Tel
010-82967028 13552068683
Fax
+86-10-82967029
Email
2355560935@qq.com
Country
China
ProdList
12390
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60
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View Lastest Price from 6-Carboxyfluorescein manufacturers

Hebei Zhuanglai Chemical Trading Co.,Ltd
Product
6-Carboxyfluorescein 3301-79-9
Price
US $40.00/kg
Min. Order
1kg
Purity
99%
Supply Ability
5000kg/week
Release date
2024-05-30
Hebei Chuanghai Biotechnology Co,.LTD
Product
6-Carboxyfluorescein 3301-79-9
Price
US $5.00-2.00/KG
Min. Order
1KG
Purity
99%
Supply Ability
10000kg
Release date
2024-08-21
Shaanxi Dideu Medichem Co. Ltd
Product
6-Carboxyfluorescein 3301-79-9
Price
US $1.00/KG
Min. Order
1KG
Purity
99%
Supply Ability
20T
Release date
2024-07-11

3301-79-9, 6-CarboxyfluoresceinRelated Search:


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