3-tert-Butoxycarbonylphenylboronic acid
- Product Name
- 3-tert-Butoxycarbonylphenylboronic acid
- CAS No.
- 220210-56-0
- Chemical Name
- 3-tert-Butoxycarbonylphenylboronic acid
- Synonyms
- B2006G1;T-BUTYL 3-BORONOBENZOATE;3-tert-Butoxycarbonylphenyl;tert-Butyl 3-boronobenzoate;3-(Tert-Butoxycarbonyl)Phenylb;3-(T-BUTOXYCARBONYL)PHENYLBORONIC ACID;1-(1,1-Dimethylethyl) 3-boronobenzoate;3-(T-BUTOXYCARBONYL)PHENYLBORBONIC ACID;3-(TERT-BUTOXYCARBONYL)PHENYLBORONIC ACID;3-(TERT-BUTOXYCARBONYL)BENZENEBORONIC ACID
- CBNumber
- CB7303214
- Molecular Formula
- C11H15BO4
- Formula Weight
- 222.05
- MOL File
- 220210-56-0.mol
3-tert-Butoxycarbonylphenylboronic acid Property
- Melting point:
- 96-102°C
- Boiling point:
- 375.0±44.0 °C(Predicted)
- Density
- 1.15±0.1 g/cm3(Predicted)
- storage temp.
- Keep in dark place,Sealed in dry,Room Temperature
- solubility
- soluble in Methanol
- form
- powder to crystal
- pka
- 7.72±0.10(Predicted)
- color
- White to Almost white
- CAS DataBase Reference
- 220210-56-0(CAS DataBase Reference)
Safety
- Hazard Codes
- Xi
- Risk Statements
- 36/37/38
- Safety Statements
- 26-36/37/39-60-37
- Hazard Note
- Irritant/Keep Cold
- HS Code
- 29319000
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
P405Store locked up.
N-Bromosuccinimide Price
- Product number
- B4726
- Product name
- 3-(tert-Butoxycarbonyl)phenylboronic Acid (contains varying amounts of Anhydride)
- Packaging
- 1g
- Price
- $42
- Updated
- 2024/03/01
- Product number
- B4726
- Product name
- 3-(tert-Butoxycarbonyl)phenylboronic Acid (contains varying amounts of Anhydride)
- Packaging
- 5g
- Price
- $181
- Updated
- 2024/03/01
- Product number
- H53007
- Product name
- 3-(tert-Butoxycarbonyl)benzeneboronic acid, 98%
- Packaging
- 1g
- Price
- $53.4
- Updated
- 2022/04/27
- Product number
- H53007
- Product name
- 3-(tert-Butoxycarbonyl)benzeneboronic acid, 98%
- Packaging
- 5g
- Price
- $209
- Updated
- 2021/12/16
- Product number
- B809218
- Product name
- 3-t-Butoxycarbonylphenylboronicacid
- Packaging
- 500mg
- Price
- $65
- Updated
- 2021/12/16
3-tert-Butoxycarbonylphenylboronic acid Chemical Properties,Usage,Production
Chemical Properties
White to light yellow crystal powde
Preparation
The 10L glass reactor is equipped with mechanical stirring, thermometer and constant pressure dropping funnel. Under nitrogen protection, add 3 moles of raw material m-carboxybenzene boric acid and 4kg tetrahydrofuran. Add 4.5 moles of thionyl chloride dropwise under reflux and stirring, react for 4 hours, cool to 0-5°C, add 7.5 moles of potassium tert-butoxide in batches, continue stirring for 1 hour after the addition, add 2kg of water, and acidify with acetic acid. Let sit and let the liquid separate. The organic phase was concentrated to obtain a crude product, which was recrystallized by adding 2 kg of petroleum ether to obtain a solid product, 3-tert-Butoxycarbonylphenylboronic acid, with a purity of 98% and a molar yield of 95%.
3-tert-Butoxycarbonylphenylboronic acid Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 3-tert-Butoxycarbonylphenylboronic acid manufacturers
- Product
- 3-tert-Butoxycarbonylphenylboronic acid 220210-56-0
- Price
- US $34.00-1.20/kg
- Min. Order
- 1kg
- Purity
- 99%
- Supply Ability
- g-kg-tons, free sample is available
- Release date
- 2024-04-08
- Product
- 3-tert-Butoxycarbonylphenylboronic acid 220210-56-0
- Price
- US $15.00-10.00/KG
- Min. Order
- 1KG
- Purity
- 99%+ HPLC
- Supply Ability
- Monthly supply of 1 ton
- Release date
- 2021-07-11
- Product
- 3-tert-Butoxycarbonylphenylboronic acid 220210-56-0
- Price
- US $15.00-10.00/KG
- Min. Order
- 1KG
- Purity
- 99%+ HPLC
- Supply Ability
- Monthly supply of 1 ton
- Release date
- 2021-07-09