DL-7-Azatryptophan Monohydrate
- Product Name
- DL-7-Azatryptophan Monohydrate
- CAS No.
- 7303-50-6
- Chemical Name
- DL-7-Azatryptophan Monohydrate
- Synonyms
- Aza-T;SWF-77;NSC 19495;DL-7-AzaTrp-OH;7-AZATRYPTOPHAN;DL-Azatryptophan;DL-7-AZATRYPTOPHAN;TIMTEC-BB SBB005480;7-Aza-DL-tryptophan;7-AZATRYPTOPHAN USP/EP/BP
- CBNumber
- CB7312816
- Molecular Formula
- C10H11N3O2
- Formula Weight
- 205.21
- MOL File
- 7303-50-6.mol
DL-7-Azatryptophan Monohydrate Property
- Melting point:
- 275°C dec.
- Boiling point:
- 540.2±50.0 °C(Predicted)
- Density
- 1.49±0.1 g/cm3(Predicted)
- storage temp.
- Keep in dark place,Sealed in dry,Store in freezer, under -20°C
- pka
- 2.20±0.10(Predicted)
- form
- Crystalline Powder
- color
- Slightly off-white
- optical activity
- 0.0848°(C=1.0029g/100ml 1N HCL)
- CAS DataBase Reference
- 7303-50-6(CAS DataBase Reference)
Safety
- WGK Germany
- 3
- RTECS
- UY8810000
- Hazard Note
- Harmful/Store below -10C
- HS Code
- 2933998090
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
- Precautionary statements
-
P264Wash hands thoroughly after handling.
P264Wash skin thouroughly after handling.
P280Wear protective gloves/protective clothing/eye protection/face protection.
N-Bromosuccinimide Price
- Product number
- A0557
- Product name
- DL-7-Azatryptophan Monohydrate
- Purity
- >98.0%(HPLC)(T)
- Packaging
- 100mg
- Price
- $184
- Updated
- 2021/12/16
- Product number
- BIA1485
- Product name
- DL-7-Azatryptophan
- Packaging
- 250mg
- Price
- $87
- Updated
- 2021/12/16
- Product number
- AS16220
- Product name
- 2-Amino-3-(1H-pyrrolo[2,3-b]pyridin-3-yl)propanoic acid
- Purity
- 97+%
- Packaging
- 250mg
- Price
- $216
- Updated
- 2021/12/16
- Product number
- BIA1485
- Product name
- DL-7-Azatryptophan
- Packaging
- 1g
- Price
- $261
- Updated
- 2021/12/16
- Product number
- 4H57-1-Z0
- Product name
- DL-7-Azatryptophan
- Purity
- 97%
- Packaging
- 250mg
- Price
- $359
- Updated
- 2021/12/16
DL-7-Azatryptophan Monohydrate Chemical Properties,Usage,Production
Chemical Properties
White Powder
Uses
DL-7-Azatryptophan is an unusual alpha-amino acid with a very potent fluorescent activity. Its used as a vehicle for probing the structure and dynamics of protein and peptides
Synthesis
211179-97-4
7303-50-6
Step 2: Diethyl 2-((1H-pyrrolo[2,3-b]pyridin-3-yl)methyl)-2-acetamidomalonate (3.5 g, 10.08 mmol) was mixed with 37% hydrochloric acid (30 mL) and the reaction was carried out at reflux for 15 hrs. Upon completion of the reaction, the mixture was concentrated to about 10 mL. acetonitrile (5 mL) was added to the concentrate and subsequently lyophilized to give an off-white solid product. The solid was redissolved in 15% aqueous ammonia solution, pH adjusted to 7, and then diluted with water (20 mL). The precipitated white solid was collected by filtration, washed sequentially with water and ethanol, and dried to give 2-amino-3-(1H-pyrrolo[2,3-b]pyridin-3-yl)propanoic acid (1.5 g, 72.5% yield) as a white solid. The product was analyzed by LCMS (condition A): retention time = 0.29 min; ESI-MS (+) m/z 206.0 ([M+H]+).
References
[1] Patent: WO2016/39749, A1. Location in patent: Page/Page column 190
[1] Patent: , 2016, . Location in patent: Page/Page column 190
[3] Journal of the American Chemical Society, 1955, vol. 77, p. 457,458, 6554, 6555
DL-7-Azatryptophan Monohydrate Preparation Products And Raw materials
Raw materials
Preparation Products
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