4-PHENYLPIPERIDINE HYDROCHLORIDE
- Product Name
- 4-PHENYLPIPERIDINE HYDROCHLORIDE
- CAS No.
- 10272-49-8
- Chemical Name
- 4-PHENYLPIPERIDINE HYDROCHLORIDE
- Synonyms
- 4-Phenylpiperdine HCL;4-phenylpiperidinium chloride;4-Phenylpiperdine hydrochloride;4-PHENYLPIPERIDINE HYDROCHLORIDE;Piperidine, 4-phenyl-,hydrochloride (1:1);1,2,3,6-Tetrahydro-4-phenylpiperidine hydrochloride
- CBNumber
- CB7376302
- Molecular Formula
- C11H16ClN
- Formula Weight
- 197.7
- MOL File
- 10272-49-8.mol
4-PHENYLPIPERIDINE HYDROCHLORIDE Property
- Melting point:
- 164-165℃
- storage temp.
- Inert atmosphere,Room Temperature
- Appearance
- White to off-white Solid
- InChI
- InChI=1S/C11H15N.ClH/c1-2-4-10(5-3-1)11-6-8-12-9-7-11;/h1-5,11-12H,6-9H2;1H
- InChIKey
- UPZJLQCUYUTZIE-UHFFFAOYSA-N
- SMILES
- C1(C=CC=CC=1)C1CCNCC1.Cl
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- P336355
- Product name
- 4-Phenylpiperidinehydrochloride
- Packaging
- 50mg
- Price
- $45
- Updated
- 2021/12/16
- Product number
- P336355
- Product name
- 4-Phenylpiperidinehydrochloride
- Packaging
- 100mg
- Price
- $60
- Updated
- 2021/12/16
- Product number
- P336355
- Product name
- 4-Phenylpiperidinehydrochloride
- Packaging
- 500mg
- Price
- $90
- Updated
- 2021/12/16
- Product number
- Z3814
- Product name
- 4-Phenylpiperidinehydrochloride
- Packaging
- 5g
- Price
- $154
- Updated
- 2021/12/16
- Product number
- HCH0013309
- Product name
- 4-PHENYL-PIPERIDINE HYDROCHLORIDE
- Purity
- 95.00%
- Packaging
- 1G
- Price
- $424
- Updated
- 2021/12/16
4-PHENYLPIPERIDINE HYDROCHLORIDE Chemical Properties,Usage,Production
Chemical Properties
mp 154-158°C
Synthesis
43064-12-6
10272-49-8
The general procedure for the synthesis of 4-phenylpiperidine hydrochloride from 4-phenyl-1,2,3,6-tetrahydropyridine hydrochloride was as follows: 10% palladium carbon (100 mg) was added to a stirred solution of 4-phenyl-1,2,3,6-tetrahydropyridine hydrochloride (300 mg, 1.53 mmol) in methanol (10 mL) under argon protection. Subsequently, the reaction mixture was flushed with hydrogen three times and the reaction was stirred under hydrogen atmosphere (balloon) for 4 hours. The reaction progress was monitored by LCMS. After completion of the reaction, the reaction mixture was filtered through a short diatomaceous earth pad and washed with methanol (5 mL). The filtrate was concentrated under reduced pressure and the residue was washed with anhydrous ether (2 x 5 mL) to give the final 4-phenylpiperidine hydrochloride (300 mg, 99%) as an off-white hygroscopic solid. m/z 162.3 [M+H]+ by LCMS.
References
[1] Patent: US2003/171370, 2003, A1
[2] Patent: WO2018/125961, 2018, A1. Location in patent: Page/Page column 42; 43
[3] Patent: US2004/92524, 2004, A1. Location in patent: Page/Page column 38
[4] Patent: US6355642, 2002, B1. Location in patent: Page column 14
[5] Patent: EP1020434, 2000, A1
4-PHENYLPIPERIDINE HYDROCHLORIDE Preparation Products And Raw materials
Raw materials
Preparation Products
4-PHENYLPIPERIDINE HYDROCHLORIDE Suppliers
- Tel
- --
- Fax
- --
- enamine@enamine.net
- Country
- Ukraine
- ProdList
- 6216
- Advantage
- 67
View Lastest Price from 4-PHENYLPIPERIDINE HYDROCHLORIDE manufacturers
- Product
- 4-PHENYLPIPERIDINE HYDROCHLORIDE 10272-49-8
- Price
- US $100.00/KG
- Min. Order
- 1KG
- Purity
- 99%
- Supply Ability
- 100KG
- Release date
- 2018-08-04