5-BROMO-2,2'-BIPYRIDINE

Product Name: 5-BROMO-2,2'-BIPYRIDINE
CAS No.: 15862-19-8
Chemical Name: 5-BROMO-2,2'-BIPYRIDINE
Synonyms: Abametapir Impurity 13;5-Bromo-2,2'-bipyridyl;-BROMO-2,2'-BIPYRIDINE;5-BROMO-2,2'-BIPYRIDINE;2,2'-Bipyridine,5-broMo-;5-Bromo-[2,2']bipyridinyl;2-(2-Pyridyl)-5-broMopyridine;3-Bromo-6-(2-pyridyl)pyridine;5-Bromo-2,2'-bipyridine, >=97%;5-BROMO-2-(PYRIDIN-2-YL)PYRIDINE
CBNumber: CB7379196
Molecular Formula: C10H7BrN2
Formula Weight: 235.08
MOL File: 15862-19-8.mol

More

Less

5-BROMO-2,2'-BIPYRIDINE Property

Melting point:: 73 °C
Boiling point:: 322.4±27.0 °C(Predicted)
Density: 1.493±0.06 g/cm3(Predicted)
storage temp.: Inert atmosphere,Room Temperature
form: crystalline solid
pka: 3.55±0.22(Predicted)
color: White to faint brown
InChI: InChI=1S/C10H7BrN2/c11-8-4-5-10(13-7-8)9-3-1-2-6-12-9/h1-7H
InChIKey: AWJPULCSDFBFDR-UHFFFAOYSA-N
SMILES: C1(C2=NC=CC=C2)=NC=C(Br)C=C1

More

Less

Safety

HS Code: 2933399990

More

Less

Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P280Wear protective gloves/protective clothing/eye protection/face protection.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

More

Less

N-Bromosuccinimide Price

TCI Chemical

Product number: B6181
Product name: 5-Bromo-2,2'-bipyridine
Purity: min. 98.0 %
Packaging: 1G
Price: $216
Updated: 2025/07/31

AK Scientific

Product number: 7965AA
Product name: 5-Bromo-2,2'-bipyridine
Packaging: 1g
Price: $234
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: HCH0035349
Product name: 5-BROMO-[2,2']BIPYRIDINYL
Purity: 95.00%
Packaging: 250MG
Price: $282.45
Updated: 2021/12/16

Matrix Scientific

Product number: 086314
Product name: 5-Bromo-[2,2']bipyridinyl
Purity: 97%
Packaging: 1g
Price: $289
Updated: 2021/12/16

Rieke Metals

Product number: 11141
Product name: 5-Bromo-2,2'-bipyridine
Purity: 97%
Packaging: 1g
Price: $355
Updated: 2021/12/16

More

Less

5-BROMO-2,2'-BIPYRIDINE Chemical Properties,Usage,Production

Chemical Properties

White solid

Synthesis

624-28-2

13737-05-8

15862-19-8

The general procedure for the synthesis of 5-bromo-2,2'-bipyridine from 2,5-dibromopyridine and 2-(trimethylstannyl)pyridine was as follows: 1.91 g (7.89 mmol, 1.0 eq.) of 2-(trimethylstannyl)pyridine and 2.08 g (8.77 mmol, 1.1 eq.) of 2,5-dibromopyridine were dissolved in 16 mL of freshly distilled xylene. The solution was degassed and 0.061 g (0.053 mmol, 0.06 eq.) of Pd(PPh3)4 was added and stirred under reflux conditions for 15 hours. Upon completion of the reaction, 40 mL of 2N NaOH solution was added, followed by three extractions with 40 mL of toluene. The organic phases were combined, washed with brine, dried over anhydrous MgSO4 and concentrated under reduced pressure to remove the solvent. Purification by silica gel column chromatography (SiO2, 3.3 × 10 cm, pentane/EtOAc = 20:1) afforded 2.57 g (63% yield) of 5-bromo-2,2'-bipyridine as a colorless solid.

References

[1] Journal of Organic Chemistry, 2002, vol. 67, # 2, p. 443 - 449
[2] Synlett, 2016, vol. 27, # 7, p. 1056 - 1060
[3] Inorganica Chimica Acta, 2013, vol. 395, p. 145 - 150
[4] Bioorganic and Medicinal Chemistry Letters, 2012, vol. 22, # 4, p. 1670 - 1673

5-BROMO-2,2'-BIPYRIDINE Preparation Products And Raw materials

Raw materials

Preparation Products

More

Less

5-BROMO-2,2'-BIPYRIDINE Suppliers

Americas 1 China 142 Europe 1 Germany 1 India 2 Japan 1 Lithuania 1 South Korea 1 Switzerland 3 United States 8 Global 161

Shanghai Uchem Inc.

Tel: 15618758386; 15618758386
Fax: QQ:3004479444
Email: sales3@myuchem.com
Country: China
ProdList: 1999
Advantage: 55

Zhengzhou HQ Material Co., Ltd.

Tel: 0371-67759225 13526468238
Email: sale@hqmat.com
Country: China
ProdList: 1256
Advantage: 58

Energy Chemical

Tel: 021-021-58432009 400-005-6266
Fax: 021-58436166
Email: sales8178@energy-chemical.com
Country: China
ProdList: 44801
Advantage: 61

Shijiazhuang Sdyano Fine Chemical Co., Ltd.

Tel: 0311-89250318 031166536426
Fax: 4000311741
Email: master@sjzsdyn.com
Country: China
ProdList: 2807
Advantage: 65

Jia Xing Isenchem Co.,Ltd

Tel: 0573-85285100 18627885956
Fax: 0573-85285100
Email: isenchem@163.com
Country: China
ProdList: 9310
Advantage: 66

Tetranov Biopharm

Tel: 13526569071
Email: sales@leadmedpharm.com
Country: China
ProdList: 7892
Advantage: 64

Shanghai Harvest Chemical Industrial Co., Ltd.

Tel: 021-31038972,31038973 17321035817
Fax: +86-21-51385350
Email: sales@harvest-chem.com
Country: China
ProdList: 2816
Advantage: 64

Shanghai Hanhong Scientific Co.,Ltd.

Tel: 021-54306202 13764082696
Email: info@hanhongsci.com
Country: China
ProdList: 42934
Advantage: 64

Sichuan Kulinan Technology Co., Ltd

Tel: 400-1166-196 18981987031
Fax: 028-84555506 800101999
Email: cdhxsj@163.com
Country: China
ProdList: 11705
Advantage: 57

Springchem New Material Technology Co.,Limited

Tel: +86-021-62885108 +8613917661608
Email: info@spring-chem.com
Country: China
ProdList: 2068
Advantage: 57

More

Less

View Lastest Price from 5-BROMO-2,2'-BIPYRIDINE manufacturers

Henan Aochuang Chemical Co.,Ltd.

Product: 5-BROMO-2,2'-BIPYRIDINE 15862-19-8
Price: US $0.00-0.00/KG
Min. Order: 1KG
Purity: 98%
Supply Ability: 1ton
Release date: 2022-09-27

Shanghai UCHEM Inc.

Product: 5-Bromo-2,2'-bipyridine 15862-19-8
Price: US $57.00-252.00/g
Min. Order: 1g
Purity: 0.98
Supply Ability: 10kg
Release date: 2024-07-09

Career Henan Chemical Co

Product: 5-BROMO-2,2'-BIPYRIDINE 15862-19-8
Price: US $1.00/KG
Min. Order: 1G
Purity: 99%
Supply Ability: 100kg
Release date: 2018-08-12

15862-19-8, 5-BROMO-2,2'-BIPYRIDINERelated Search:

2,2'-BipyridiniuM,1,1'-diMethyl-, iodide (1:2) 2,2'-bipyridne-6,6'(1H,1'H)-dione, 1,1'-diMethyl- 4,4'-DIBROMO-2,2'-BIPYRIDINE 2,2'-bipyridine-5,5'-diamine 4-Bromo-2,2''-bipyridine 4'-CHLORO-2,2':6',2''-TERPYRIDINE 2,2'-BIPYRIDINE-5-CARBOXYLIC ACID 2,2'-DIPYRIDYL N,N'-DIOXIDE 2,2':6',2''-TERPYRIDINE-4,4',4''-TRICARBOXYLIC ACID 4,4'-Dimethyl-2,2'-bipyridyl 4‘-(4-hydroxyphenyl)-2, 2':6‘, 2“-terpyridine 1,3,5-Tris(m-iodophenyl)benzene 4'-BROMO-2,2':6',2''-TERPYRIDINE 4-Methyl-4'-(3-carboxypropyl)-2,2'-bipyridine 6-BROMO-2,2'-BIPYRIDINE 5,5'-Dibromo-2,2'-bipyridyl 1,10-Phenanthroline-5,6-dione,3,8-dibromo 5-BROMO-2,2'-BIPYRIDINE

5-BROMO-2,2'-BIPYRIDINE

2-(pyridin-2-yl)-5-bromopyridine

5-Bromo-[2,2']bipyridinyl

2,2'-Bipyridine,5-broMo-

2-(2-Pyridyl)-5-broMopyridine

5-Bromo-2,2'-bipyridine, >=97%

3-Bromo-6-(2-pyridyl)pyridine

5-BROMO-2-(PYRIDIN-2-YL)PYRIDINE

-BROMO-2,2'-BIPYRIDINE

5-Bromo-2,2'-bipyridyl

Abametapir Impurity 13

15862-19-8