3-Fluorophenethyl alcohol

Product Name: 3-Fluorophenethyl alcohol
CAS No.: 52059-53-7
Chemical Name: 3-Fluorophenethyl alcohol
Synonyms: Pratraxa impurity 1;3-Fluorobenzeneethanol;3-Fluorophenylethanol ;3-fluorophenyl alcohol;3-FLUOROPHENETHYL ALCOHOL;2-(M-FLUOROPHENYL)ETHANOL;2-(3-FLUOROPHENYL)ETHANOL;3-Fluorophenethylealcohol;Benzeneethanol, 3-fluoro-;2-(3-Fluorophenyl)ethan-1-ol
CBNumber: CB7491498
Molecular Formula: C8H9FO
Formula Weight: 140.15
MOL File: 52059-53-7.mol

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3-Fluorophenethyl alcohol Property

Boiling point:: 90 °C/3 mmHg (lit.)
Density: 1.125 g/mL at 25 °C (lit.)
refractive index: n20/D 1.509(lit.)
Flash point:: 225 °F
storage temp.: Sealed in dry,Room Temperature
form: Liquid
pka: 14.76±0.10(Predicted)
color: Clear colorless

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Safety

Hazard Codes: C,Xn
Risk Statements: 36/37/38-21/22-34
Safety Statements: 26-36/37/39-45-27
RIDADR: 2810
WGK Germany: 3
HS Code: 29062990

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

Precautionary statements

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P280Wear protective gloves/protective clothing/eye protection/face protection.

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N-Bromosuccinimide Price

TCI Chemical

Product number: F0776
Product name: 2-(3-Fluorophenyl)ethanol
Purity: >98.0%(GC)
Packaging: 1g
Price: $36
Updated: 2025/07/31

TCI Chemical

Product number: F0776
Product name: 2-(3-Fluorophenyl)ethanol
Purity: >98.0%(GC)
Packaging: 5g
Price: $106
Updated: 2025/07/31

TRC

Product number: F632318
Product name: 2-(3-Fluorophenyl)ethanol
Packaging: 500mg
Price: $75
Updated: 2021/12/16

AK Scientific

Product number: J96582
Product name: 2-(3-Fluorophenyl)ethanol
Packaging: 10g
Price: $75
Updated: 2021/12/16

Apolloscientific

Product number: PC5701
Product name: 3-Fluorophenethyl alcohol
Purity: 98%
Packaging: 25g
Price: $98
Updated: 2021/12/16

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3-Fluorophenethyl alcohol Chemical Properties,Usage,Production

Chemical Properties

clear colorless liquid

General Description

3-Fluorophenethyl alcohol is a fluorinated β-phenethyl alcohol. Regioselective synthesis of 3-fluorophenethyl alcohol via regioselective hydroboration has been reported.

Synthesis

331-25-9

52059-53-7

The general procedure for the synthesis of 3-fluorophenylethanol from 3-fluorophenylacetic acid was as follows: to a stirred solution of 3-fluorophenylacetic acid (5.0 g, 32.0 mmol) in ether (100 ml) was slowly added dropwise an ether solution of lithium aluminum hydroxide (32.4 ml, 1 M, 32.4 mmol) at -10 °C. The reaction mixture was gradually warmed to 25°C and stirred continuously for 1 hour. Subsequently, the reaction mixture was cooled again to -10°C and the reaction was quenched by sequential addition of methanol (20 ml) and 4M sodium hydroxide solution (20 ml). The resulting slurry was filtered and the filtrate was concentrated by evaporation under vacuum. The crude product was purified by silica gel column chromatography using CH2Cl2/MeOH/NH3 (80:8:1) as eluent to give 3-fluorophenylethanol (3.80 g, 84% yield) finally. The product was confirmed by NMR hydrogen spectrum (250 MHz, CDCl3): δ 2.87 (3H, t, J = 6.5 Hz, CH2), 3.87 (3H, t, J = 6.5 Hz, CH2), 6.89-7.02 (3H, m, Ar-H), 7.23-7.33 (1H, m, Ar-H).

References

[1] Journal of Organic Chemistry, 2005, vol. 70, # 14, p. 5528 - 5535
[2] Tetrahedron Asymmetry, 2001, vol. 12, # 4, p. 585 - 596
[3] Patent: US5889008, 1999, A
[4] Helvetica Chimica Acta, 1973, vol. 56, p. 2460 - 2479
[5] Journal of the American Chemical Society, 1978, vol. 100, p. 228 - 246

3-Fluorophenethyl alcohol Preparation Products And Raw materials

Raw materials

Preparation Products

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3-Fluorophenethyl alcohol Suppliers

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52059-53-7, 3-Fluorophenethyl alcoholRelated Search:

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52059-53-7

ALCOHOL

Building Blocks

Alcohols

C7 to C8

Organic Building Blocks

Oxygen Compounds

Fluorine series

Oxygen Compounds

Phenyls & Phenyl-Het

Alcohols

C7 to C8