ChemicalBook > CAS DataBase List > 5-METHOXYQUINOLINE

5-METHOXYQUINOLINE

Product Name: 5-METHOXYQUINOLINE
CAS No.: 6931-19-7
Chemical Name: 5-METHOXYQUINOLINE
Synonyms: 5-METHOXYQUINOLINE;Quinoline, 5-methoxy-;5-METHOXYQUINOLINE ISO 9001：2015 REACH
CBNumber: CB7530124
Molecular Formula: C10H9NO
Formula Weight: 159.18
MOL File: 6931-19-7.mol

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5-METHOXYQUINOLINE Property

Boiling point:: 282 °C(Press: 758 Torr)
Density: 1.130±0.06 g/cm3(Predicted)
storage temp.: Sealed in dry,Room Temperature
solubility: Chloroform
form: Oil
pka: 4.84±0.12(Predicted)
color: Brown

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Safety

HS Code: 2933499090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P321Specific treatment (see … on this label).

P332+P313IF SKIN irritation occurs: Get medical advice/attention.

P362Take off contaminated clothing and wash before reuse.

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N-Bromosuccinimide Price

TRC

Product number: M267395
Product name: 5-Methoxyquinoline
Packaging: 100mg
Price: $140
Updated: 2021/12/16

AK Scientific

Product number: W7912
Product name: 5-Methoxyquinoline
Packaging: 5g
Price: $188
Updated: 2021/12/16

Matrix Scientific

Product number: 074651
Product name: 5-Methoxyquinoline
Purity: 95+%
Packaging: 25g
Price: $320
Updated: 2021/12/16

Matrix Scientific

Product number: 074651
Product name: 5-Methoxyquinoline
Purity: 95+%
Packaging: 1g
Price: $46
Updated: 2021/12/16

AK Scientific

Product number: W7912
Product name: 5-Methoxyquinoline
Packaging: 1g
Price: $91
Updated: 2021/12/16

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5-METHOXYQUINOLINE Chemical Properties,Usage,Production

Chemical Properties

Brown Oil

Uses

5-Methoxyquinoline (cas# 6931-19-7) is a compound useful in organic synthesis.

Synthesis

578-67-6

74-88-4

6931-19-7

4.2 Synthesis of 5-methoxyquinoline (1) 5-Hydroxyquinoline (4.0 g, 27.6 mmol) was dissolved in anhydrous DMF (60 mL) under argon protection and cooled to 0 °C. NaH (1.33 g, 33.12 mmol, 60% mineral oil dispersion) was then slowly added. The reaction mixture was kept stirred at 0 °C for 30 min. Then, methyl iodide (4.7 g, 33.12 mmol) was added dropwise to the suspension and the reaction mixture was allowed to gradually warm up to room temperature with continued stirring for 30 min. Upon completion of the reaction, the reaction was quenched with 300 mL of water and then extracted with ether (6 x 100 mL). The organic layers were combined, washed sequentially with water and brine, dried with anhydrous Na2SO4, filtered and the solvent was concentrated under reduced pressure to give the brown oily target product 5-methoxyquinoline. Yield: 4.03 g (92%). 1H NMR (400 MHz, CDCl3) δ 8.95 (dd, J = 4.2, 2.0 Hz, 1H), 8.62 (dd, J = 8.4, 1.2 Hz, 1H), 7.74 (d, J = 8.0 Hz, 1H), 7.65 (t, J = 8.4 Hz, 1H), 7.42 (dd, J = 8.4, 4.4 Hz, 1H), 6.90 (d, J = 8.0 Hz, 1H), 4.05 (s, 3H). 13C NMR (100 MHz, CDCl3) δ 155.17, 150.66, 148.70, 130.81, 129.37, 121.58, 120.85, 120.19, 104.22, 55.76.

References

[1] European Journal of Medicinal Chemistry, 2015, vol. 101, p. 754 - 768
[2] Patent: KR101778938, 2017, B1. Location in patent: Paragraph 0147-0148; 0155; 0164-0166
[3] Dissertation , S. 23,
[4] Chemische Berichte, 1882, vol. 15, p. 1979
[5] Chemische Berichte, 1887, vol. 20, p. 731

5-METHOXYQUINOLINE Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from 5-METHOXYQUINOLINE manufacturers

Career Henan Chemical Co

Product: 5-METHOXYQUINOLINE 6931-19-7
Price: US $5.50/KG
Min. Order: 1KG
Purity: 98%min
Supply Ability: 1kg-100kg
Release date: 2020-01-14

6931-19-7, 5-METHOXYQUINOLINERelated Search:

5,8-DIMETHOXYQUINOLINE 2-CHLORO-5,6,7-TRIMETHOXY-QUINOLINE-3-CARBALDEHYDE 8-Benzyloxyquinoline MS 209 ZOSUQUIDAR TRIHYSROCHLORIDE 5-METHOXYQUINOLINE 2-CHLORO-5,8-DIMETHOXY-QUINOLINE-3-CARBALDEHYDE 5,7-DIMETHOXY-3-(4-PYRIDINYL)QUINOLINE DIHYDROCHLORIDE 5-METHOXYQUINOLIN-8-AMINE MS 073 4-HYDROXY-2-METHYL-5,6,7-TRIMETHOXYQUINOLINE SQI-PR 10-METHOXYCAMPTOTHECIN alpha-((Diethylamino)methyl)-p-((1-methoxy-6-nitro-9-acridinyl)amino)b enzyl alcohol 4-HYDROXY-5,6,7-TRIMETHOXYQUINOLINE 2-CHLORO-5,8-DIMETHOXY-3-PHENYLQUINOLINE 4-CHLORO-5,6,7-TRIMETHOXYQUINOLINE Iodure de diacetoxy-1,4 methoxy-2 methyl-10 acridinium [French]

5-METHOXYQUINOLINE

Quinoline, 5-methoxy-

5-METHOXYQUINOLINE ISO 9001：2015 REACH

6931-19-7

Chemical Amines

Amines

Aromatics