RARECHEM AL BI 0500

Product Name: RARECHEM AL BI 0500
CAS No.: 86239-00-1
Chemical Name: RARECHEM AL BI 0500
Synonyms: RARECHEM AL BI 0500;Ethyl 3-fluoro-4-Methylbenzoate;3-FLUORO-4-METHYLBENZOIC ACID ETHYL ESTER;Benzoic acid, 3-fluoro-4-methyl-, ethyl ester
CBNumber: CB7677876
Molecular Formula: C10H11FO2
Formula Weight: 182.19
MOL File: 86239-00-1.mol

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RARECHEM AL BI 0500 Property

Boiling point:: 240.8±28.0 °C(Predicted)
Density: 1.108±0.06 g/cm3(Predicted)
storage temp.: Sealed in dry,Room Temperature
Appearance: Light yellow to yellow Liquid

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Safety

HS Code: 2916399090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

Apolloscientific

Product number: PC911426
Product name: Ethyl3-fluoro-4-methylbenzoate
Purity: 95%
Packaging: 1g
Price: $110
Updated: 2021/12/16

Apolloscientific

Product number: PC911426
Product name: Ethyl3-fluoro-4-methylbenzoate
Purity: 95%
Packaging: 5g
Price: $285
Updated: 2021/12/16

Apolloscientific

Product number: PC911426
Product name: Ethyl3-fluoro-4-methylbenzoate
Purity: 95%
Packaging: 10g
Price: $470
Updated: 2021/12/16

Rieke Metals

Product number: EE0266
Product name: 3-Fluoro-4-methylbenzoicacidethylester
Packaging: 1g
Price: $661
Updated: 2021/12/16

Rieke Metals

Product number: EE0266
Product name: 3-Fluoro-4-methylbenzoicacidethylester
Packaging: 5g
Price: $1728
Updated: 2021/12/16

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RARECHEM AL BI 0500 Chemical Properties,Usage,Production

Synthesis

64-17-5

350-28-7

86239-00-1

Thionyl chloride (3 mL) was added slowly and dropwise to a solution of 3-fluoro-4-methylbenzoic acid (13.23 g, 85.85 mmol) in anhydrous ethanol (200 mL) at 0 °C. The reaction mixture was warmed to 60 °C and stirred overnight. Upon completion of the reaction, the mixture was cooled to room temperature and subsequently concentrated under reduced pressure. The concentrate was diluted with dichloromethane and the resulting organic phase was washed sequentially with 1N sodium hydroxide solution (100 mL x 2). The organic layer was dried over anhydrous magnesium sulfate and concentrated under reduced pressure to give ethyl 3-fluoro-4-methylbenzoate (15.02 g, 96% yield).

References

[1] Patent: WO2011/71565, 2011, A1. Location in patent: Page/Page column 163
[2] Patent: WO2010/93845, 2010, A1. Location in patent: Page/Page column 153
[3] Journal of Medicinal Chemistry, 1983, vol. 26, # 9, p. 1282 - 1293
[4] Bioorganic and Medicinal Chemistry Letters, 2006, vol. 16, # 5, p. 1421 - 1425
[5] Patent: WO2009/145360, 2009, A1. Location in patent: Page/Page column 129-130

RARECHEM AL BI 0500 Preparation Products And Raw materials

Raw materials

Preparation Products

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RARECHEM AL BI 0500 Suppliers

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86239-00-1, RARECHEM AL BI 0500Related Search:

3-Fluoro-4-methylbenzoic acid ethyl 4-(aminomethyl)-2,3,5,6-tetrafluorobenzoate RARECHEM AL BI 0529 RARECHEM AL BI 0450 RARECHEM AL BI 0524 ethyl 2,3,5,6-tetrafluoro-4-(trifluoromethyl)benzoate RARECHEM AL BI 0503 RARECHEM AL BI 0528 3-FLUORO-5-HYDROXY-4-METHYLBENZOIC ACID ETHYL ESTER RARECHEM AL BI 0500 RARECHEM AL BI 0448 ethyl 4-cyano-3-fluorobenzenecarboxylate RARECHEM AL BI 0525

RARECHEM AL BI 0500

3-FLUORO-4-METHYLBENZOIC ACID ETHYL ESTER

Ethyl 3-fluoro-4-Methylbenzoate

Benzoic acid, 3-fluoro-4-methyl-, ethyl ester

86239-00-1