RARECHEM AL BI 0500
- Product Name
- RARECHEM AL BI 0500
- CAS No.
- 86239-00-1
- Chemical Name
- RARECHEM AL BI 0500
- Synonyms
- RARECHEM AL BI 0500;Ethyl 3-fluoro-4-Methylbenzoate;3-FLUORO-4-METHYLBENZOIC ACID ETHYL ESTER;Benzoic acid, 3-fluoro-4-methyl-, ethyl ester
- CBNumber
- CB7677876
- Molecular Formula
- C10H11FO2
- Formula Weight
- 182.19
- MOL File
- 86239-00-1.mol
RARECHEM AL BI 0500 Property
- Boiling point:
- 240.8±28.0 °C(Predicted)
- Density
- 1.108±0.06 g/cm3(Predicted)
- storage temp.
- Sealed in dry,Room Temperature
- Appearance
- Light yellow to yellow Liquid
Safety
- HS Code
- 2916399090
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- PC911426
- Product name
- Ethyl3-fluoro-4-methylbenzoate
- Purity
- 95%
- Packaging
- 1g
- Price
- $110
- Updated
- 2021/12/16
- Product number
- PC911426
- Product name
- Ethyl3-fluoro-4-methylbenzoate
- Purity
- 95%
- Packaging
- 5g
- Price
- $285
- Updated
- 2021/12/16
- Product number
- PC911426
- Product name
- Ethyl3-fluoro-4-methylbenzoate
- Purity
- 95%
- Packaging
- 10g
- Price
- $470
- Updated
- 2021/12/16
- Product number
- EE0266
- Product name
- 3-Fluoro-4-methylbenzoicacidethylester
- Packaging
- 1g
- Price
- $661
- Updated
- 2021/12/16
- Product number
- EE0266
- Product name
- 3-Fluoro-4-methylbenzoicacidethylester
- Packaging
- 5g
- Price
- $1728
- Updated
- 2021/12/16
RARECHEM AL BI 0500 Chemical Properties,Usage,Production
Synthesis
64-17-5
350-28-7
86239-00-1
Thionyl chloride (3 mL) was added slowly and dropwise to a solution of 3-fluoro-4-methylbenzoic acid (13.23 g, 85.85 mmol) in anhydrous ethanol (200 mL) at 0 °C. The reaction mixture was warmed to 60 °C and stirred overnight. Upon completion of the reaction, the mixture was cooled to room temperature and subsequently concentrated under reduced pressure. The concentrate was diluted with dichloromethane and the resulting organic phase was washed sequentially with 1N sodium hydroxide solution (100 mL x 2). The organic layer was dried over anhydrous magnesium sulfate and concentrated under reduced pressure to give ethyl 3-fluoro-4-methylbenzoate (15.02 g, 96% yield).
References
[1] Patent: WO2011/71565, 2011, A1. Location in patent: Page/Page column 163
[2] Patent: WO2010/93845, 2010, A1. Location in patent: Page/Page column 153
[3] Journal of Medicinal Chemistry, 1983, vol. 26, # 9, p. 1282 - 1293
[4] Bioorganic and Medicinal Chemistry Letters, 2006, vol. 16, # 5, p. 1421 - 1425
[5] Patent: WO2009/145360, 2009, A1. Location in patent: Page/Page column 129-130
RARECHEM AL BI 0500 Preparation Products And Raw materials
Raw materials
Preparation Products
RARECHEM AL BI 0500 Suppliers
- Tel
- --
- Fax
- --
- sales@ajchem.in
- Country
- India
- ProdList
- 6100
- Advantage
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