ChemicalBook > CAS DataBase List > METHYL 4-(4-PYRIDINYL)BENZOATE

METHYL 4-(4-PYRIDINYL)BENZOATE

Product Name: METHYL 4-(4-PYRIDINYL)BENZOATE
CAS No.: 106047-17-0
Chemical Name: METHYL 4-(4-PYRIDINYL)BENZOATE
Synonyms: AKOS BAR-0605;METHYL 4-PYRIDIN-4-YL-BENZATE;Methyl 4-(pyridin-4-yl)benoate;METHYL 4-(4-PYRIDINYL)BENZOATE;METHYL 4-(PYRIDIN-4-YL)BENZOATE;Benzoic acid, 4-(4-pyridinyl)-, methyl ester
CBNumber: CB7703427
Molecular Formula: C13H11NO2
Formula Weight: 213.23
MOL File: 106047-17-0.mol

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METHYL 4-(4-PYRIDINYL)BENZOATE Property

Melting point:: 103-105℃
Boiling point:: 160 °C(Press: 1 Torr)
Density: 1.147
storage temp.: Inert atmosphere,Room Temperature
pka: 4.98±0.10(Predicted)

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Safety

HS Code: 2933399990

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H320Causes eye irritation

H371May cause damage to organs

H400Very toxic to aquatic life

Precautionary statements

P260Do not breathe dust/fume/gas/mist/vapours/spray.

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P270Do not eat, drink or smoke when using this product.

P273Avoid release to the environment.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P337+P313IF eye irritation persists: Get medical advice/attention.

P391Collect spillage. Hazardous to the aquatic environment

P405Store locked up.

P501Dispose of contents/container to..…

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N-Bromosuccinimide Price

Apolloscientific

Product number: OR346705
Product name: 4-(Pyridin-4-yl)benzoic acid methyl ester
Packaging: 1g
Price: $187
Updated: 2021/12/16

AK Scientific

Product number: 1335AA
Product name: Methyl4-(pyridin-4-yl)benzoate
Packaging: 250mg
Price: $101
Updated: 2021/12/16

Apolloscientific

Product number: OR346705
Product name: 4-(Pyridin-4-yl)benzoic acid methyl ester
Packaging: 5g
Price: $578
Updated: 2021/12/16

AK Scientific

Product number: 1335AA
Product name: Methyl4-(pyridin-4-yl)benzoate
Packaging: 10g
Price: $594
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: CHM0290536
Product name: METHYL-4-(PYRIDIN-4-YL)BENZOATE
Purity: 98.00%
Packaging: 0.5G
Price: $1347.5
Updated: 2021/12/16

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METHYL 4-(4-PYRIDINYL)BENZOATE Chemical Properties,Usage,Production

Synthesis

1120-87-2

99768-12-4

106047-17-0

Step A: 4-Bromopyridine (3.0 g, 19.0 mmol), 4-methoxycarbonylphenylboronic acid (2.63 g, 14.6 mmol), Pd(PPh3)2Cl2 (0.35 g, 0.5 mmol) and sodium carbonate (6.91 g, 65.2 mmol) were dissolved in 1,2-dimethoxyethane (40 mL) under nitrogen protection. The reaction mixture was heated to 90 °C and stirred for 10 hours. Upon completion of the reaction, the mixture was concentrated under reduced pressure and the residue was purified by silica gel column chromatography (eluent: petroleum ether/ethyl acetate = 6:1 to 2:1) to afford methyl 4-(pyridin-4-yl)benzoate (2.7 g, yield: 86.8%) as a white solid. m/z MS (ESI): 214 [M+H]+.

References

[1] Patent: EP3190113, 2017, A1. Location in patent: Paragraph 0101
[2] Patent: TWI558709, 2016, B. Location in patent: Page/Page column 50; 51
[3] Patent: US2004/242572, 2004, A1. Location in patent: Page/Page column 73

METHYL 4-(4-PYRIDINYL)BENZOATE Preparation Products And Raw materials

Raw materials

Preparation Products

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106047-17-0, METHYL 4-(4-PYRIDINYL)BENZOATERelated Search:

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AKOS BAR-0605

Benzoic acid, 4-(4-pyridinyl)-, methyl ester

106047-17-0