Benzonitrile, 3-amino-5-methoxy- (9CI)
- Product Name
- Benzonitrile, 3-amino-5-methoxy- (9CI)
- CAS No.
- 269411-71-4
- Chemical Name
- Benzonitrile, 3-amino-5-methoxy- (9CI)
- Synonyms
- 3-aMino-5-Methoxybenzonitrile;Benzonitrile,3-aMino-5-Methoxy-;Benzonitrile, 3-amino-5-methoxy- (9CI)
- CBNumber
- CB81044425
- Molecular Formula
- C8H8N2O
- Formula Weight
- 148.16
- MOL File
- 269411-71-4.mol
Benzonitrile, 3-amino-5-methoxy- (9CI) Property
- Melting point:
- 81-85 °C
- Boiling point:
- 322.6±27.0 °C(Predicted)
- Density
- 1.17±0.1 g/cm3(Predicted)
- storage temp.
- Keep in dark place,Inert atmosphere,Room temperature
- pka
- 2.37±0.10(Predicted)
- Appearance
- Light yellow to brown Solid
N-Bromosuccinimide Price
- Product number
- FA141413
- Product name
- 3-Amino-5-methoxybenzonitrile
- Packaging
- 100mg
- Price
- $90
- Updated
- 2021/12/16
- Product number
- 2469AB
- Product name
- 3-Amino-5-methoxybenzonitrile
- Packaging
- 100mg
- Price
- $104
- Updated
- 2021/12/16
- Product number
- FA141413
- Product name
- 3-Amino-5-methoxybenzonitrile
- Packaging
- 250mg
- Price
- $175
- Updated
- 2021/12/16
- Product number
- 120732
- Product name
- 3-Amino-5-methoxybenzonitrile
- Purity
- 97%
- Packaging
- 1g
- Price
- $209
- Updated
- 2021/12/16
- Product number
- 2469AB
- Product name
- 3-Amino-5-methoxybenzonitrile
- Packaging
- 1g
- Price
- $242
- Updated
- 2021/12/16
Benzonitrile, 3-amino-5-methoxy- (9CI) Chemical Properties,Usage,Production
Synthesis
33224-19-0
269411-71-4
In a three-necked flask, 3-methoxy-5-nitrobenzonitrile (8.0 g, 0.045 mol) was dissolved in methanol (80 mL), 10% palladium-carbon catalyst (1.4 g) and ammonium acetate (6.9 g, 0.090 mol) were added. Hydrogen was introduced and the reaction was stirred at 40 °C for 8 hours. After completion of the reaction, filtration was carried out and the filter cake was washed with methanol (15 mL x 3). The filtrates were combined and concentrated under reduced pressure. The concentrate was poured into 50 mL of water and extracted with ethyl acetate (40 mL x 3). The organic phases were combined, dried with anhydrous sodium sulfate, and the solvent was removed by evaporation under reduced pressure to give 3-amino-5-methoxybenzonitrile as a solid 6.5 g in 98.2% yield.
References
[1] Patent: CN107573264, 2018, A. Location in patent: Paragraph 0023-0025; 0040-0042; 0057-0059; 0074-0076
Benzonitrile, 3-amino-5-methoxy- (9CI) Preparation Products And Raw materials
Raw materials
Preparation Products
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