4-Ethynylbenzenesulfonamide
- Product Name
- 4-Ethynylbenzenesulfonamide
- CAS No.
- 1788-08-5
- Chemical Name
- 4-Ethynylbenzenesulfonamide
- Synonyms
- 4-Ethynybenzenesulfonamide;4-ethynylbenzenesulfonamide;BenzenesulfonaMide, 4-ethynyl-;4-ethynylbenzene-1-sulfonaMide;4-Ethynylbenzenesulfonamide >Benzenesulfonamide, 4-ethynyl- (9CI);4-Ethynylbenzenesulfonamide - [E48489]
- CBNumber
- CB81071913
- Molecular Formula
- C8H7NO2S
- Formula Weight
- 181.21
- MOL File
- 1788-08-5.mol
4-Ethynylbenzenesulfonamide Property
- Melting point:
- 178.0 to 182.0 °C
- Boiling point:
- 338.2±44.0 °C(Predicted)
- Density
- 1.38±0.1 g/cm3(Predicted)
- storage temp.
- 2-8°C
- form
- powder to crystal
- pka
- 9.88±0.10(Predicted)
- color
- Light yellow to Yellow to Orange
Safety
- HS Code
- 2935.90.9500
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
- Precautionary statements
-
P264Wash hands thoroughly after handling.
P264Wash skin thouroughly after handling.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P302+P352IF ON SKIN: wash with plenty of soap and water.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
P321Specific treatment (see … on this label).
P332+P313IF SKIN irritation occurs: Get medical advice/attention.
P362Take off contaminated clothing and wash before reuse.
N-Bromosuccinimide Price
- Product number
- E1130
- Product name
- 4-Ethynylbenzenesulfonamide
- Purity
- >98.0%(HPLC)(N)
- Packaging
- 200mg
- Price
- $167
- Updated
- 2025/07/31
- Product number
- E1130
- Product name
- 4-Ethynylbenzenesulfonamide
- Purity
- >98.0%(HPLC)(N)
- Packaging
- 1g
- Price
- $581
- Updated
- 2025/07/31
- Product number
- E940020
- Product name
- 4-Ethynylbenzenesulfonamide
- Packaging
- 50mg
- Price
- $65
- Updated
- 2021/12/16
- Product number
- E48489
- Product name
- 4-Ethynylbenzenesulfonamide
- Purity
- 98%
- Packaging
- 100mg
- Price
- $90
- Updated
- 2021/12/16
- Product number
- AS38296
- Product name
- 4-Ethynylbenzenesulfonamide
- Purity
- 98%
- Packaging
- 250mg
- Price
- $182
- Updated
- 2021/12/16
4-Ethynylbenzenesulfonamide Chemical Properties,Usage,Production
Synthesis
775331-26-5
1788-08-5
Under nitrogen protection, 4-((trimethylmethylsilyl)ethynyl)benzenesulfonamide (1.69 g, 3.13 mmol) prepared in step 1 was dissolved in anhydrous tetrahydrofuran and tetrabutylammonium fluoride (TBAF, 10 mL, 1.0 M solution in tetrahydrofuran, 10 mmol) was added. The reaction mixture was stirred at room temperature. The progress of the reaction was monitored by silica gel thin layer chromatography (TLC, unfolding agent ratio 1:1 hexane:ethyl acetate). Upon completion of the reaction, 10% hydrochloric acid and ethyl acetate were added. The organic layer was separated, washed twice sequentially with water and aqueous ammonium chloride, dried over anhydrous sodium sulfate, and concentrated under reduced pressure to afford the target product, 4-alkynylbenzenesulfonamide, 0.748 g in 62% yield. High-resolution electrospray ionization mass spectrometry (ESHRMS) measured m/z of 199.0506 ([M+NH4]+, calculated value of 199.0541 for C8H7NO2SNH4).
References
[1] MedChemComm, 2018, vol. 9, # 3, p. 534 - 544
[2] Patent: WO2004/87686, 2004, A2. Location in patent: Page 229
[3] Patent: WO2004/87687, 2004, A1. Location in patent: Page 229
[4] Organic and biomolecular chemistry, 2003, vol. 1, # 3, p. 498 - 506
[5] Bioorganic and Medicinal Chemistry, 2008, vol. 16, # 4, p. 1948 - 1956
4-Ethynylbenzenesulfonamide Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 4-Ethynylbenzenesulfonamide manufacturers
- Product
- 4-Ethynylbenzenesulfonamide 1788-08-5
- Price
- US $5.00/KG
- Min. Order
- 1KG
- Purity
- 98%
- Supply Ability
- 100KG
- Release date
- 2020-01-12