ChemicalBook > CAS DataBase List > 2-CHLORO-3-NITROBENZALDEHYDE

2-CHLORO-3-NITROBENZALDEHYDE

Product Name
2-CHLORO-3-NITROBENZALDEHYDE
CAS No.
58755-57-0
Chemical Name
2-CHLORO-3-NITROBENZALDEHYDE
Synonyms
2-CHLORO-3-NITROBENZALDEHYDE;2-CHLORO-3-NIRO BENZALDEHYDE;Benzaldehyde, 2-chloro-3-nitro-;2-Chloro-3-nitrobenzaldehyde 95%;2-chloro-3-nitrobenzaldehyde58755-57-0
CBNumber
CB8110260
Molecular Formula
C7H4ClNO3
Formula Weight
185.56
MOL File
58755-57-0.mol
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2-CHLORO-3-NITROBENZALDEHYDE Property

Boiling point:
293.5±25.0 °C(Predicted)
Density 
1.485±0.06 g/cm3(Predicted)
storage temp. 
under inert gas (nitrogen or Argon) at 2-8°C
form 
powder
color 
Yellow
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Safety

HS Code 
2913000090
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H302Harmful if swallowed

Precautionary statements

P280Wear protective gloves/protective clothing/eye protection/face protection.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC
Product number
C611595
Product name
2-Chloro-3-nitrobenzaldehyde
Packaging
250mg
Price
$65
Updated
2021/12/16
Biosynth Carbosynth
Product number
FC139771
Product name
2-Chloro-3-nitrobenzaldehyde
Packaging
1g
Price
$67
Updated
2021/12/16
AK Scientific
Product number
W7175
Product name
2-Chloro-3-nitrobenzaldehyde
Packaging
100mg
Price
$72
Updated
2021/12/16
AK Scientific
Product number
W7175
Product name
2-Chloro-3-nitrobenzaldehyde
Packaging
1g
Price
$109
Updated
2021/12/16
Biosynth Carbosynth
Product number
FC139771
Product name
2-Chloro-3-nitrobenzaldehyde
Packaging
2g
Price
$117
Updated
2021/12/16
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2-CHLORO-3-NITROBENZALDEHYDE Chemical Properties,Usage,Production

Synthesis

89639-98-5

58755-57-0

Step 2. Synthesis of 2-chloro-3-nitrobenzaldehyde: To a 250 mL three-necked round-bottomed flask, a solution of oxalyl chloride (5.42 g, 42.70 mmol, 1.10 eq.) in dichloromethane (DCM, 100 mL) was added. Subsequently, a solution of dimethyl sulfoxide (DMSO, 6.65 g, 85.11 mmol, 2.20 eq.) in DCM (15 mL) was added dropwise and the reaction system was kept at -78 °C. At this temperature, a solution of (2-chloro-3-nitrophenyl)methanol (7.23 g, 38.54 mmol, 1.00 eq.) in DCM (35 mL) was slowly added and stirred continuously for 1 hour. Then, triethylamine (TEA, 30 mL) was added at the same temperature and stirring was continued for 1 hour. Upon completion of the reaction, the reaction was quenched with water and extracted with DCM (3 x 100 mL). The organic layers were combined, dried over anhydrous sodium sulfate, filtered and concentrated on a rotary evaporator. The residue was purified by silica gel column chromatography using petroleum ether (PE):ethyl acetate (EA) = 10:1 as eluent to afford 2-chloro-3-nitrobenzaldehyde (5.3 g, 74% yield) as a light yellow solid.

References

[1] Journal of Medicinal Chemistry, 1988, vol. 31, # 5, p. 936 - 944
[2] Patent: US2011/34450, 2011, A1. Location in patent: Page/Page column 101; 102
[3] Patent: US2003/225053, 2003, A1. Location in patent: Page 24
[4] Patent: US8080566, 2011, B1. Location in patent: Page/Page column 72
[5] Tetrahedron, 2000, vol. 56, # 2, p. 165 - 173

2-CHLORO-3-NITROBENZALDEHYDE Preparation Products And Raw materials

Raw materials

Preparation Products

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2-CHLORO-3-NITROBENZALDEHYDE Suppliers

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58755-57-0, 2-CHLORO-3-NITROBENZALDEHYDERelated Search:

3-CHLORO-5-NITROBENZALDEHYDE 4-CHLORO-3-NITROBENZALDEHYDE,4-Chloro-3-Nitrobenzaldehyde 3-Nitro-4-Chlorobenzaldehyde 2,4-Dichloro-5-nitrobenzalehyde 3-Nitrobenzaldehyde 2,6-DICHLORO-3-NITROBENZOIC ACID 2-Chloro-3,5-dinitrobenzoic acid 2-CHLORO-3-NITROBENZALDEHYDE 2,4-Dichloro-5-fluoro-3-nitrobenzoic acid 2,6-Dichloro-3-nitrobenzaldehyde 2,5-Dichloro-3-nitrobenzoic acid 2,4-DICHLORO-3,5-DINITROBENZOIC ACID 2-Chloro-3-nitrobenzoic acid 4-CHLORO-2-NITROBENZALDEHYDE,4-chloro-2-nitrobenzaldehyde*crystalline 5-Chloro-2-nitrobenzaldehyde 2-Chloro-5-nitrobenzaldehyde 97%,2-CHLORO-5-NITROBENZALDEHYDE,6-Chloro-3-nitrobenzaldehyde methyl 2,5-dichloro-3-nitrobenzoate ETHYL 2-CHLORO-3-NITROBENZOATE 2,4-DICHLORO-3,5-DINITROBENZAMIDE

  • 2-CHLORO-3-NITROBENZALDEHYDE
  • 2-Chloro-3-nitrobenzaldehyde 95%
  • Benzaldehyde, 2-chloro-3-nitro-
  • 2-chloro-3-nitrobenzaldehyde58755-57-0
  • 2-CHLORO-3-NIRO BENZALDEHYDE
  • 58755-57-0