2,3-Difluoronitrobenzene
- Product Name
- 2,3-Difluoronitrobenzene
- CAS No.
- 6921-22-8
- Chemical Name
- 2,3-Difluoronitrobenzene
- Synonyms
- 1,2-difluoro-3-nitrobenzene;2,3-DIFLUORONITROBENZENE;2,3-Difluoro-1-Nitrobenzene;2,3-Difluoronitrobenzene ,98%;Benzene, 1,2-difluoro-3-nitro-;2-methylthiazole-33-carboxylic acid;2,3-Difluoronitrobenzene ISO 9001：2015 REACH;Benzene, 1,2-difluoro-3-nitro- (7CI,8CI,9CI)
- CBNumber
- CB8122474
- Molecular Formula
- C6H3F2NO2
- Formula Weight
- 159.09
- MOL File
- 6921-22-8.mol
2,3-Difluoronitrobenzene Property
- Boiling point:
- 219.0±20.0 °C(Predicted)
- Density
- 1.450±0.06 g/cm3(Predicted)
- storage temp.
- Sealed in dry,Room Temperature
- form
- liquid
- color
- Light yellow to yellow
- CAS DataBase Reference
- 6921-22-8(CAS DataBase Reference)
Safety
- Hazard Codes
- Xi
- HazardClass
- IRRITANT
- HS Code
- 2904990090
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- D447188
- Product name
- 1,2-Difluoro-3-nitrobenzene
- Packaging
- 5g
- Price
- $215
- Updated
- 2021/12/16
- Product number
- 4654-3-X1
- Product name
- 2,3-Difluoronitrobenzene
- Purity
- 97%
- Packaging
- 10g
- Price
- $184
- Updated
- 2021/12/16
- Product number
- FD57718
- Product name
- 2,3-Difluoronitrobenzene
- Packaging
- 5G
- Price
- $200
- Updated
- 2021/12/16
- Product number
- 054330
- Product name
- 1,2-Difluoro-3-nitrobenzene
- Purity
- >95%
- Packaging
- 25g
- Price
- $283
- Updated
- 2021/12/16
- Product number
- FD57718
- Product name
- 2,3-Difluoronitrobenzene
- Packaging
- 10g
- Price
- $300
- Updated
- 2021/12/16
2,3-Difluoronitrobenzene Chemical Properties,Usage,Production
Chemical Properties
Light yellow transparent liquid
Synthesis
To a stirred solution of hydroxy peroxide (30 % in H2O, 35 mL, 356 mmol) under N2 at 0℃, a solution of trifluoroacetic anhydride (56 mL, 407 mmol) in 115 mL dichloromethane was added dropwise over 2 h. After the addition was complete, a solution of 2,3- difluorobenzenamine (5 g, 39 mmol) in 115 mL dichloromethane was added dropwise at 0℃. After the addition was complete, the reaction mixture was gradually warmed to room temperature and stirred overnight. The mixture was extracted by dichloromethane and dried over anhydrous Na2SO4. The mixture was filtered and concentrated under reduced pressure. The residue was purified by flash column with 0-15 % EtOAc in hexane to yield 3.5 g of 2,3-Difluoronitrobenzene (57%).
2,3-Difluoronitrobenzene Preparation Products And Raw materials
Raw materials
Preparation Products
2,3-Difluoronitrobenzene Suppliers
- Tel
- --
- Fax
- --
- sales@riccichimica.com
- Country
- Italy
- ProdList
- 2146
- Advantage
- 46
View Lastest Price from 2,3-Difluoronitrobenzene manufacturers
- Product
- 2,3-Difluoronitrobenzene 6921-22-8
- Price
- US $2.00/KG
- Min. Order
- 1g
- Purity
- 98%min
- Supply Ability
- ask
- Release date
- 2020-01-08