3-AMINO-5-CHLORO-BENZONITRILE
- Product Name
- 3-AMINO-5-CHLORO-BENZONITRILE
- CAS No.
- 53312-78-0
- Chemical Name
- 3-AMINO-5-CHLORO-BENZONITRILE
- Synonyms
- 3-Chloro-5-cyanoanisole;3-Chloro-5-cyanoaniline;5-Cyano-3-chloroaniline;5-Amino-3-chlorobenzonitrile;3-AMINO-5-CHLORO-BENZONITRILE;Benzonitrile, 3-aMino-5-chloro-;3-Amino-5-chlorobenzonitrile 97%
- CBNumber
- CB8127116
- Molecular Formula
- C7H5ClN2
- Formula Weight
- 152.58
- MOL File
- 53312-78-0.mol
3-AMINO-5-CHLORO-BENZONITRILE Property
- Boiling point:
- 309.0±22.0 °C(Predicted)
- Density
- 1.33
- storage temp.
- 2-8°C, protect from light
- pka
- 1.73±0.10(Predicted)
- form
- Powder
- Appearance
- Off-white to light yellow Solid
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- A617728
- Product name
- 3-Amino-5-chlorobenzonitrile
- Packaging
- 500mg
- Price
- $110
- Updated
- 2021/12/16
- Product number
- 3637-5-X3
- Product name
- 3-Amino-5-chlorobenzonitrile
- Purity
- 98%
- Packaging
- 1g
- Price
- $117
- Updated
- 2021/12/16
- Product number
- J94223
- Product name
- 3-Amino-5-chlorobenzonitrile
- Packaging
- 5g
- Price
- $165
- Updated
- 2021/12/16
- Product number
- V6448
- Product name
- 3-Amino-5-chlorobenzonitrile
- Packaging
- 5g
- Price
- $221
- Updated
- 2021/12/16
- Product number
- J94223
- Product name
- 3-Amino-5-chlorobenzonitrile
- Packaging
- 10g
- Price
- $295
- Updated
- 2021/12/16
3-AMINO-5-CHLORO-BENZONITRILE Chemical Properties,Usage,Production
Synthesis
34662-30-1
53312-78-0
The general procedure for the synthesis of 3-amino-5-chlorobenzonitrile from 3-chloro-5-nitrobenzonitrile was as follows: 3-chloro-5-nitrobenzonitrile was dissolved in DMF at room temperature, and 6 equivalents of SnCl2-2H2O was added, and the reaction was carried out overnight for reduction. After completion of the reaction, the target product was purified by silica gel column chromatography in 40% yield. LCMS analysis of the product (Condition A) showed a retention time of 1.61 min and a molecular ion peak [M+H]+ of 153.1.1 The 1H NMR (500 MHz, CDCl3) data were as follows: δ 6.97 (s, 1H), 6.84 (t, J = 2.0 Hz, 1H), 6.77 (s, 1H).
References
[1] Patent: US2006/287287, 2006, A1. Location in patent: Page/Page column 17-18
3-AMINO-5-CHLORO-BENZONITRILE Preparation Products And Raw materials
Raw materials
Preparation Products
3-AMINO-5-CHLORO-BENZONITRILE Suppliers
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View Lastest Price from 3-AMINO-5-CHLORO-BENZONITRILE manufacturers
- Product
- 3-AMINO-5-CHLORO-BENZONITRILE 53312-78-0
- Price
- US $1.00/KG
- Min. Order
- 1KG
- Purity
- 99%
- Supply Ability
- 100KG
- Release date
- 2020-01-08