Synthesis
ChemicalBook > CAS DataBase List > 1-Benzyl-3-ethoxycarbonyl-4-piperidone

1-Benzyl-3-ethoxycarbonyl-4-piperidone

Synthesis
Product Name
1-Benzyl-3-ethoxycarbonyl-4-piperidone
CAS No.
41276-30-6
Chemical Name
1-Benzyl-3-ethoxycarbonyl-4-piperidone
Synonyms
-3-ethoxycarbonyL;LABOTEST-BB LT00440756;1-Benzyl-3-carbethoxy-4-piperidone;N-BENZYL-3-CARBOETHOXY-4-PIPERIDONE;1-BENZYL-3-CARBOETHOXY-4-PIPERIDONE;-Benzyl-3-ethoxycarbonyl-4-piperidone;1-BENZYL-3-ETHOXYCARBONYL-4-PIPERIDONE;ethyl 1-benzyl-4-oxopiperidine-3-carboxylate;1-(benzyl)-4-keto-nipecotic acid ethyl ester;ethyl 4-oxo-1-(phenylmethyl)piperidine-3-carboxylate
CBNumber
CB8135913
Molecular Formula
C15H19NO3
Formula Weight
261.32
MOL File
41276-30-6.mol
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1-Benzyl-3-ethoxycarbonyl-4-piperidone Property

Boiling point:
379.7±42.0 °C(Predicted)
Density 
1.154±0.06 g/cm3(Predicted)
storage temp. 
under inert gas (nitrogen or Argon) at 2-8°C
pka
10.77±0.20(Predicted)
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

Precautionary statements

P280Wear protective gloves/protective clothing/eye protection/face protection.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P332+P313IF SKIN irritation occurs: Get medical advice/attention.

P337+P313IF eye irritation persists: Get medical advice/attention.

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N-Bromosuccinimide Price

TRC
Product number
B276375
Product name
1-Benzyl-3-ethoxycarbonyl-4-piperidone
Packaging
500mg
Price
$90
Updated
2021/12/16
Biosynth Carbosynth
Product number
FB71817
Product name
1-Benzyl-3-ethoxycarbonyl-4-piperidone
Packaging
500mg
Price
$150
Updated
2021/12/16
Matrix Scientific
Product number
114008
Product name
Ethyl 1-benzyl-4-oxo-3-piperidinecarboxylate
Purity
97%
Packaging
1g
Price
$165
Updated
2021/12/16
AK Scientific
Product number
R187
Product name
1-Benzyl-3-ethoxycarbonyl-4-piperidone
Packaging
1g
Price
$166
Updated
2021/12/16
Biosynth Carbosynth
Product number
FB71817
Product name
1-Benzyl-3-ethoxycarbonyl-4-piperidone
Packaging
1g
Price
$200
Updated
2021/12/16
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1-Benzyl-3-ethoxycarbonyl-4-piperidone Chemical Properties,Usage,Production

Synthesis

To a suspension of NaH (5.38 g, 0.13 mol) in benzene, a solution of Michael adduct 131 (25 g, 0.09 mol) in PhH was added drop-wise and refluxed for 3 hours. The reaction mixture was allowed to cool and quenched with saturated NH4Cl solution, extracted with ethyl acetate, washed with water, brine, dried over anhydrous Na2SO4, filtered and concentrated in vacuo. Column chromatographic separation over silica gel (EtOAc- pet ether) afforded ketoester, as a pale yellow oil (18.15 g).

1-Benzyl-3-ethoxycarbonyl-4-piperidone Preparation Products And Raw materials

Raw materials

Preparation Products

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1-Benzyl-3-ethoxycarbonyl-4-piperidone Suppliers

J & K SCIENTIFIC LTD.
Tel
010-82848833 400-666-7788
Fax
86-10-82849933
Email
jkinfo@jkchemical.com
Country
China
ProdList
96815
Advantage
76
ShangHai DEMO Chemical Co.,Ltd
Tel
400-021-7337 2355568890
Fax
0086-21-50182339
Email
sales@demochem.com
Country
China
ProdList
2572
Advantage
57
Wuhan Chemwish Technology Co., Ltd
Tel
86-027-67849912
Fax
86-027-87531808
Email
sales@chemwish.com
Country
China
ProdList
35906
Advantage
56
Shanghai Longsheng chemical Co.,Ltd.
Tel
021-58099652-8005 13585536065
Fax
021-58099609
Email
bin.wu@shlschem.com
Country
China
ProdList
9816
Advantage
59
Shanghai Sunway Pharmaceutical Technology Co., Ltd
Tel
+8618575662672 18575662672
Fax
021 51613951
Email
mzeng@3wpharm.com
Country
China
ProdList
10053
Advantage
57
Chongqing Werlchem Fine Chemical Co.Ltd.
Tel
023-67521957 13320292971
Fax
86-23-67511575
Email
sales@werlchem.com
Country
China
ProdList
28
Advantage
62
Shanghai Topbiochem Technology Co., Ltd
Tel
+86-21-60341587
Fax
+86-21-61294319
Email
sales@topbiochem.com
Country
China
ProdList
6181
Advantage
58
9ding chemical ( Shanghai) Limited
Tel
4009209199
Fax
86-021-52271987
Email
sales@9dingchem.com
Country
China
ProdList
18216
Advantage
56
Shanghai Chainpharm Bio-medical Technology Co., Ltd.
Tel
021-61727342 13611721451
Fax
021-61294107
Email
sales@chainpharm.com
Country
China
ProdList
932
Advantage
58
Amatek Scientific Co. Ltd.
Tel
0512-56316828 4008675858
Fax
+86-512-56316826
Email
sales@amateksci.com
Country
China
ProdList
9908
Advantage
55
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View Lastest Price from 1-Benzyl-3-ethoxycarbonyl-4-piperidone manufacturers

Career Henan Chemical Co
Product
1-Benzyl-3-ethoxycarbonyl-4-piperidone 41276-30-6
Price
US $3.00/KG
Min. Order
1KG
Purity
98%
Supply Ability
1kg,5kg,50kg
Release date
2020-01-18

41276-30-6, 1-Benzyl-3-ethoxycarbonyl-4-piperidone Related Search:


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