Synthesis
ChemicalBook > CAS DataBase List > 1-Benzyl-3-ethoxycarbonyl-4-piperidone

1-Benzyl-3-ethoxycarbonyl-4-piperidone

Synthesis
Product Name
1-Benzyl-3-ethoxycarbonyl-4-piperidone
CAS No.
41276-30-6
Chemical Name
1-Benzyl-3-ethoxycarbonyl-4-piperidone
Synonyms
-3-ethoxycarbonyL;LABOTEST-BB LT00440756;1-Benzyl-3-carbethoxy-4-piperidone;N-BENZYL-3-CARBOETHOXY-4-PIPERIDONE;1-BENZYL-3-CARBOETHOXY-4-PIPERIDONE;-Benzyl-3-ethoxycarbonyl-4-piperidone;1-BENZYL-3-ETHOXYCARBONYL-4-PIPERIDONE;ethyl 1-benzyl-4-oxopiperidine-3-carboxylate;1-(benzyl)-4-keto-nipecotic acid ethyl ester;ethyl 4-oxo-1-(phenylmethyl)piperidine-3-carboxylate
CBNumber
CB8135913
Molecular Formula
C15H19NO3
Formula Weight
261.32
MOL File
41276-30-6.mol
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1-Benzyl-3-ethoxycarbonyl-4-piperidone Property

Boiling point:
379.7±42.0 °C(Predicted)
Density 
1.154±0.06 g/cm3(Predicted)
storage temp. 
under inert gas (nitrogen or Argon) at 2-8°C
pka
10.77±0.20(Predicted)
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

Precautionary statements

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P332+P313IF SKIN irritation occurs: Get medical advice/attention.

P337+P313IF eye irritation persists: Get medical advice/attention.

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N-Bromosuccinimide Price

TRC
Product number
B276375
Product name
1-Benzyl-3-ethoxycarbonyl-4-piperidone
Packaging
500mg
Price
$90
Updated
2021/12/16
Biosynth Carbosynth
Product number
FB71817
Product name
1-Benzyl-3-ethoxycarbonyl-4-piperidone
Packaging
500mg
Price
$150
Updated
2021/12/16
Matrix Scientific
Product number
114008
Product name
Ethyl 1-benzyl-4-oxo-3-piperidinecarboxylate
Purity
97%
Packaging
1g
Price
$165
Updated
2021/12/16
AK Scientific
Product number
R187
Product name
1-Benzyl-3-ethoxycarbonyl-4-piperidone
Packaging
1g
Price
$166
Updated
2021/12/16
Biosynth Carbosynth
Product number
FB71817
Product name
1-Benzyl-3-ethoxycarbonyl-4-piperidone
Packaging
1g
Price
$200
Updated
2021/12/16
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1-Benzyl-3-ethoxycarbonyl-4-piperidone Chemical Properties,Usage,Production

Synthesis

To a suspension of NaH (5.38 g, 0.13 mol) in benzene, a solution of Michael adduct 131 (25 g, 0.09 mol) in PhH was added drop-wise and refluxed for 3 hours. The reaction mixture was allowed to cool and quenched with saturated NH4Cl solution, extracted with ethyl acetate, washed with water, brine, dried over anhydrous Na2SO4, filtered and concentrated in vacuo. Column chromatographic separation over silica gel (EtOAc- pet ether) afforded ketoester, as a pale yellow oil (18.15 g).

1-Benzyl-3-ethoxycarbonyl-4-piperidone Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from 1-Benzyl-3-ethoxycarbonyl-4-piperidone manufacturers

Career Henan Chemical Co
Product
1-Benzyl-3-ethoxycarbonyl-4-piperidone 41276-30-6
Price
US $3.00/KG
Min. Order
1KG
Purity
98%
Supply Ability
1kg,5kg,50kg
Release date
2020-01-18

41276-30-6, 1-Benzyl-3-ethoxycarbonyl-4-piperidone Related Search:


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