1-Benzyl-3-ethoxycarbonyl-4-piperidone
Synthesis- Product Name
- 1-Benzyl-3-ethoxycarbonyl-4-piperidone
- CAS No.
- 41276-30-6
- Chemical Name
- 1-Benzyl-3-ethoxycarbonyl-4-piperidone
- Synonyms
- -3-ethoxycarbonyL;LABOTEST-BB LT00440756;1-Benzyl-3-carbethoxy-4-piperidone;N-BENZYL-3-CARBOETHOXY-4-PIPERIDONE;1-BENZYL-3-CARBOETHOXY-4-PIPERIDONE;-Benzyl-3-ethoxycarbonyl-4-piperidone;1-BENZYL-3-ETHOXYCARBONYL-4-PIPERIDONE;ethyl 1-benzyl-4-oxopiperidine-3-carboxylate;1-(benzyl)-4-keto-nipecotic acid ethyl ester;ethyl 4-oxo-1-(phenylmethyl)piperidine-3-carboxylate
- CBNumber
- CB8135913
- Molecular Formula
- C15H19NO3
- Formula Weight
- 261.32
- MOL File
- 41276-30-6.mol
1-Benzyl-3-ethoxycarbonyl-4-piperidone Property
- Boiling point:
- 379.7±42.0 °C(Predicted)
- Density
- 1.154±0.06 g/cm3(Predicted)
- storage temp.
- under inert gas (nitrogen or Argon) at 2-8°C
- pka
- 10.77±0.20(Predicted)
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
- Precautionary statements
-
P280Wear protective gloves/protective clothing/eye protection/face protection.
P302+P352IF ON SKIN: wash with plenty of soap and water.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
P332+P313IF SKIN irritation occurs: Get medical advice/attention.
P337+P313IF eye irritation persists: Get medical advice/attention.
N-Bromosuccinimide Price
- Product number
- B276375
- Product name
- 1-Benzyl-3-ethoxycarbonyl-4-piperidone
- Packaging
- 500mg
- Price
- $90
- Updated
- 2021/12/16
- Product number
- FB71817
- Product name
- 1-Benzyl-3-ethoxycarbonyl-4-piperidone
- Packaging
- 500mg
- Price
- $150
- Updated
- 2021/12/16
- Product number
- 114008
- Product name
- Ethyl 1-benzyl-4-oxo-3-piperidinecarboxylate
- Purity
- 97%
- Packaging
- 1g
- Price
- $165
- Updated
- 2021/12/16
- Product number
- R187
- Product name
- 1-Benzyl-3-ethoxycarbonyl-4-piperidone
- Packaging
- 1g
- Price
- $166
- Updated
- 2021/12/16
- Product number
- FB71817
- Product name
- 1-Benzyl-3-ethoxycarbonyl-4-piperidone
- Packaging
- 1g
- Price
- $200
- Updated
- 2021/12/16
1-Benzyl-3-ethoxycarbonyl-4-piperidone Chemical Properties,Usage,Production
Synthesis
To a suspension of NaH (5.38 g, 0.13 mol) in
benzene, a solution of Michael adduct 131 (25 g,
0.09 mol) in PhH was added drop-wise and
refluxed for 3 hours. The reaction mixture was
allowed to cool and quenched with saturated
NH4Cl solution, extracted with ethyl acetate, washed with water, brine, dried over
anhydrous Na2SO4, filtered and concentrated in vacuo. Column chromatographic
separation over silica gel (EtOAc- pet ether) afforded ketoester, as a pale yellow oil (18.15
g).
1-Benzyl-3-ethoxycarbonyl-4-piperidone Preparation Products And Raw materials
Raw materials
Preparation Products
1-Benzyl-3-ethoxycarbonyl-4-piperidone Suppliers
View Lastest Price from 1-Benzyl-3-ethoxycarbonyl-4-piperidone manufacturers
- Product
- 1-Benzyl-3-ethoxycarbonyl-4-piperidone 41276-30-6
- Price
- US $3.00/KG
- Min. Order
- 1KG
- Purity
- 98%
- Supply Ability
- 1kg,5kg,50kg
- Release date
- 2020-01-18