7-Bromo-1-tetralone
- Product Name
- 7-Bromo-1-tetralone
- CAS No.
- 32281-97-3
- Chemical Name
- 7-Bromo-1-tetralone
- Synonyms
- 7-BROMO-3,4-DIHYDRONAPHTHALEN-1(2H)-ONE;7-BROMO-3,4-DIHYDRO-1(2H)-NAPHTHALENONE;H50604;NSC 74917;en-1(2H)-one;7-BROMOTETRALONE;7-BROMO-1-TETRALONE;7-bromo-à-tetralone;7-bromotetralin-1-one;7-bromo-1-tetralin-one
- CBNumber
- CB8138459
- Molecular Formula
- C10H9BrO
- Formula Weight
- 225.08
- MOL File
- 32281-97-3.mol
7-Bromo-1-tetralone Property
- Melting point:
- 78 °C
- Boiling point:
- 157°C/8mmHg(lit.)
- Density
- 1.511±0.06 g/cm3(Predicted)
- storage temp.
- 2-8°C
- solubility
- soluble in Methanol
- form
- powder to crystal
- color
- White to Light yellow to Dark green
- λmax
- 305nm(EtOH)(lit.)
- InChI
- InChI=1S/C10H9BrO/c11-8-5-4-7-2-1-3-10(12)9(7)6-8/h4-6H,1-3H2
- InChIKey
- YGVDCGFUUUJCDF-UHFFFAOYSA-N
- SMILES
- C1(=O)C2=C(C=CC(Br)=C2)CCC1
- CAS DataBase Reference
- 32281-97-3(CAS DataBase Reference)
Safety
- Hazard Codes
- Xi,Xn
- Risk Statements
- 36/37/38-22
- Safety Statements
- 26-36/37/39-24/25
- WGK Germany
- 2
- HazardClass
- IRRITANT
- HS Code
- 29147000
- Storage Class
- 11 - Combustible Solids
- Hazard Classifications
- Acute Tox. 4 Oral
Aquatic Chronic 3
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H412Harmful to aquatic life with long lasting effects
- Precautionary statements
-
P264Wash hands thoroughly after handling.
P264Wash skin thouroughly after handling.
P270Do not eat, drink or smoke when using this product.
P273Avoid release to the environment.
P301+P312IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.
P501Dispose of contents/container to..…
N-Bromosuccinimide Price
- Product number
- 708453
- Product name
- 7-Bromo-3,4-dihydronaphthalen-1(2H)-one
- Purity
- 97%
- Packaging
- 10g
- Price
- $228
- Updated
- 2025/07/31
- Product number
- 708453
- Product name
- 7-Bromo-3,4-dihydronaphthalen-1(2H)-one
- Purity
- 97%
- Packaging
- 1g
- Price
- $29
- Updated
- 2023/06/20
- Product number
- B4545
- Product name
- 7-Bromo-1-tetralone
- Purity
- >95.0%(GC)
- Packaging
- 1g
- Price
- $51
- Updated
- 2025/07/31
- Product number
- B4545
- Product name
- 7-Bromo-1-tetralone
- Purity
- >95.0%(GC)
- Packaging
- 5g
- Price
- $153
- Updated
- 2025/07/31
- Product number
- 10007135
- Product name
- 7-Bromotetralone
- Purity
- >98%
- Packaging
- 50mg
- Price
- $15
- Updated
- 2024/03/01
7-Bromo-1-tetralone Chemical Properties,Usage,Production
Chemical Properties
White to yellow to tan powder or crystal
Uses
7-Bromo-1-tetralone is a biochemical reagent that can be used as a biological material or organic compound for life science related research.
Synthesis
A mixture of 4-(8-methoxynaphthalen-2-yl)-2-methyl-1,2,3,4-tetrahydroisoquinoline maleate (57 g, 223 mmol), potassium hydroxide (43 g, 760 mmol), and hydrazine hydrate (26 m1, 830 mmol) in diethylene glycol (2,865 ml) was stirred for 3 hr at 195 ??C. After cooling to below 40??C, the mixture was diluted with water (300 ml), poured into 3 M NaOH and washed three times with dichloromethane. Brine was added to break up the emulsion. The aqueous layer was acidified to pH 1 with 6M HCl and extracted three times with methyl tert-butyl ether. The combined organic extracts were dried with magnesium sulfate to give 4-(4-bromophenyl)butyric acid (41 g, 75%). The product of the previous step (97 g, 397 mmol) was added to polyphosphoric acid (580 g) and the resulting mixture was stirred at 90??C for 10 min. After cooling to 0??C, 6 M NaOH was added and the mixture was extracted with methyl tert-butyl ether. The organic extract was dried with magnesium sulfate to give 7-bromo-3,4-dihydronaphthalen-1-one (49 g, 55%), chromatographed (6:1 to 4:1 heptane/ethyl acetate) and recrystallized from cyclohexane to give the product 7-bromo-3,4-dihydro-2H-1-naphthalenone.
7-Bromo-1-tetralone Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 7-Bromo-1-tetralone manufacturers
- Product
- 7-Bromo-1-tetralone 32281-97-3
- Price
- US $0.00-0.00/kg
- Min. Order
- 1kg
- Purity
- 98%
- Supply Ability
- 1Ton
- Release date
- 2022-10-10
- Product
- 7-Bromo-1-tetralone 32281-97-3
- Price
- US $27.00-480.00/g
- Min. Order
- 25g
- Purity
- 0.99
- Supply Ability
- 10kg
- Release date
- 2024-10-25
- Product
- 7-Bromo-1-tetralone 32281-97-3
- Price
- US $200.00-1.00/KG
- Min. Order
- 1KG
- Purity
- 99%, 99.5% Sublimated
- Supply Ability
- g-kg-tons, free sample is available
- Release date
- 2023-12-30