(R)-1-BOC-3-DIMETHYLAMINOPYRROLIDINE

Product Name: (R)-1-BOC-3-DIMETHYLAMINOPYRROLIDINE
CAS No.: 1004538-33-3
Chemical Name: (R)-1-BOC-3-DIMETHYLAMINOPYRROLIDINE
Synonyms: -1-Boc-3-(Dimethylamino);(R)-1-BOC-3-DIMETHYLAMINOPYRROLIDINE;Tert-butyl (R)-3-(dimethylamino)pyrrolidine-1-carboxylate;(R)-tert-butyl 3-(dimethylamino)pyrrolidine-1-carboxylate;(R)-3-DIMETHYLAMINO-PYRROLIDINE-1-CARBOXYLIC ACID TERT-BUTYL ESTER;(3R)-3-(dimethylamino)-1-pyrrolidinecarboxylic acid tert-butyl ester;(3R)-3-(Dimethylamino)-1-pyrrolidinecarboxylic acid 1,1-dimethylethyl ester;3-(Dimethylamino)-1-pyrrolidinecarboxylic acid 1,1-dimethylethyl ester, (3R)-;1-Pyrrolidinecarboxylicacid, 3-(diMethylaMino)-, 1,1-diMethylethyl ester, (3R)-
CBNumber: CB81519279
Molecular Formula: C11H22N2O2
Formula Weight: 214.3
MOL File: 1004538-33-3.mol

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(R)-1-BOC-3-DIMETHYLAMINOPYRROLIDINE Property

storage temp.: 2-8°C

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H227Combustible liquid

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC

Product number: B201898
Product name: (R)-1-Boc-3-(dimethylamino)pyrrolidine
Packaging: 10mg
Price: $45
Updated: 2021/12/16

Activate Scientific

Product number: AS113983
Product name: (R)-1-Boc-3-(Dimethylamino)pyrrolidine
Purity: 97+% ee
Packaging: 1g
Price: $157
Updated: 2021/12/16

Activate Scientific

Product number: AS113983
Product name: (R)-1-Boc-3-(Dimethylamino)pyrrolidine
Purity: 97+% ee
Packaging: 250mg
Price: $265
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: CCH0001340
Product name: (R)-1-BOC-3-DIMETHYLAMINOPYRROLIDINE
Purity: 95.00%
Packaging: 250MG
Price: $326.55
Updated: 2021/12/16

AK Scientific

Product number: 8044DH
Product name: (R)-1-Boc-3-(dimethylamino)pyrrolidine
Packaging: 500mg
Price: $401
Updated: 2021/12/16

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(R)-1-BOC-3-DIMETHYLAMINOPYRROLIDINE Chemical Properties,Usage,Production

Synthesis

1004538-32-2

1004538-33-3

Step 9-2: Preparation of (R)-1-(tert-butoxycarbonyl)-3-dimethylaminopyrrolidine. 1.25 g of (R)-1-(tert-butoxycarbonyl)-3-dimethylaminopyrrolidine hydrochloride (chemical purity: 99.9 area %) was dissolved in a mixed system of 2.46 g of 23 wt% brine, 5.03 g of toluene, and 738 mg of 30 wt% aqueous sodium hydroxide, and the reaction mixture was stirred thoroughly. After completion of the reaction, liquid-liquid separation was carried out and the organic phase was collected. The organic phase was concentrated under reduced pressure to remove the solvent, followed by vacuum drying to afford 999 mg of (R)-1-Boc-3-(dimethylamino)pyrrolidine as a colorless transparent liquid (chemical purity: 99.5 area %, 95% yield). The structure of the product was confirmed by 1H-NMR (CDCl3): δ (ppm) 1.46 (s, 9H), 1.74 (m, 1H), 2.05 (m, 1H), 2.24 (s, 6H), 2.63 (m, 1H), 3.05 (m, 1H), 3.27 (m, 1H), 3.45-3.69 (m, 2H).

References

[1] Patent: EP2050735, 2009, A1. Location in patent: Page/Page column 21-22

(R)-1-BOC-3-DIMETHYLAMINOPYRROLIDINE Preparation Products And Raw materials

Raw materials

Preparation Products

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(R)-1-BOC-3-DIMETHYLAMINOPYRROLIDINE Suppliers

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1004538-33-3, (R)-1-BOC-3-DIMETHYLAMINOPYRROLIDINERelated Search:

3-(DIMETHYLAMINO)PYRROLIDINE L-N-[(4'-BOC)PIPERIDINO]PROLINE (R)-1-BOC-3-DIMETHYLAMINOPYRROLIDINE 1-Pyrrolidinecarboxylicacid,3-(methylamino)-,1,1-dimethylethylester,(R)-(9CI)

(R)-1-BOC-3-DIMETHYLAMINOPYRROLIDINE

(R)-3-DIMETHYLAMINO-PYRROLIDINE-1-CARBOXYLIC ACID TERT-BUTYL ESTER

(R)-tert-butyl 3-(dimethylamino)pyrrolidine-1-carboxylate

1-Pyrrolidinecarboxylicacid, 3-(diMethylaMino)-, 1,1-diMethylethyl ester, (3R)-

(3R)-3-(Dimethylamino)-1-pyrrolidinecarboxylic acid 1,1-dimethylethyl ester

-1-Boc-3-(Dimethylamino)

(3R)-3-(dimethylamino)-1-pyrrolidinecarboxylic acid tert-butyl ester

Tert-butyl (R)-3-(dimethylamino)pyrrolidine-1-carboxylate

3-(Dimethylamino)-1-pyrrolidinecarboxylic acid 1,1-dimethylethyl ester, (3R)-

1004538-33-3