6-bromoisoindolin-1-one

Product Name: 6-bromoisoindolin-1-one
CAS No.: 675109-26-9
Chemical Name: 6-bromoisoindolin-1-one
Synonyms: 6-broMo-2,3-dihydro-1H-isoindol-1-one;6-bromoisoindolin-1-one;6-BroMoisoindolin-1-one, 95+%;6-BroMo-2,3-dihydro-isoindol-1-one;6-Bromo-2,3-dihydroisoindolin-1-one;1H-Isoindol-1-one, 6-broMo-2,3-dihydro-;1-Piperidinecarboxylicacid,4-(2-bromoethyl)-,1,4-dimethylethylester
CBNumber: CB81560165
Molecular Formula: C8H6BrNO
Formula Weight: 212.04
MOL File: 675109-26-9.mol

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6-bromoisoindolin-1-one Property

Boiling point:: 431.7±45.0 °C(Predicted)
Density: 1.666±0.06 g/cm3(Predicted)
storage temp.: Sealed in dry,Room Temperature
pka: 13.87±0.20(Predicted)
form: solid
color: White to off-white
InChI: InChI=1S/C8H6BrNO/c9-6-2-1-5-4-10-8(11)7(5)3-6/h1-3H,4H2,(H,10,11)
InChIKey: HYTCKZQYVIURAW-UHFFFAOYSA-N
SMILES: C1(=O)C2=C(C=CC(Br)=C2)CN1

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Safety

HS Code: 2925199590

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P260Do not breathe dust/fume/gas/mist/vapours/spray.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P312Call a POISON CENTER or doctor/physician if you feel unwell.

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N-Bromosuccinimide Price

TRC

Product number: B699450
Product name: 6-Bromoisoindolin-1-one
Packaging: 100mg
Price: $75
Updated: 2021/12/16

Matrix Scientific

Product number: 076521
Product name: 6-Bromoisoindolin-1-one
Purity: 95+%
Packaging: 1g
Price: $27
Updated: 2021/12/16

AK Scientific

Product number: J50559
Product name: 6-Bromoisoindolin-1-one
Packaging: 1g
Price: $28
Updated: 2021/12/16

SynQuest Laboratories

Product number: 4H48-9-10
Product name: 6-Bromo-2,3-dihydro-1H-isoindol-1-one
Purity: 98%
Packaging: 1g
Price: $42
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FB10748
Product name: 6-Bromoisoindolin-1-one
Packaging: 1g
Price: $50
Updated: 2021/12/16

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6-bromoisoindolin-1-one Chemical Properties,Usage,Production

Synthesis

79670-17-0

675109-26-9

The general procedure for the synthesis of 6-bromoisoindolin-1-one from 5-bromo-2-bromomethylbenzoic acid methyl ester was as follows: gentle bubbling of ammonia into a 1:1 THF/MeOH mixture of 5-bromo-2-bromomethylbenzoic acid methyl ester (1 eq.) was carried out for 40 min at room temperature. Upon completion of the reaction, the reaction mixture was concentrated under vacuum. The concentrated residue was sonicated in CH2Cl2 for 15 min followed by filtration to afford the target product 6-bromo-2,3-dihydro-isoindol-1-one as a white solid (98% yield, 90% purity). Product mass spectral data: m/z (LC-MS, ESP): 212.3/214.3 [M + H]+, retention time R/T = 2.98 min.

References

[1] Patent: WO2008/23161, 2008, A1. Location in patent: Page/Page column 117
[2] Organic and Biomolecular Chemistry, 2017, vol. 15, # 48, p. 10172 - 10183
[3] Patent: CN107474006, 2017, A. Location in patent: Paragraph 0050; 0051; 0054; 0056-0057; 0060; 0062-0063; 0066
[4] Patent: WO2008/20306, 2008, A2. Location in patent: Page/Page column 38
[5] E-Journal of Chemistry, 2011, vol. 8, # 3, p. 1108 - 1113

6-bromoisoindolin-1-one Preparation Products And Raw materials

Raw materials

Preparation Products

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6-bromoisoindolin-1-one Suppliers

China 142 China Hong Kong 1 India 2 United Kingdom 2 United States 8 Global 155

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View Lastest Price from 6-bromoisoindolin-1-one manufacturers

Shanghai UCHEM Inc.

Product: 6-Bromoisoindolin-1-one 675109-26-9
Price: US $58.00-492.00/g
Min. Order: 5g
Purity: 0.98
Supply Ability: 25kg
Release date: 2023-12-18

Jinan Honest Pharm Co., Ltd

Product: 6-bromoisoindolin-1-one 675109-26-9
Price: US $0.00/g
Min. Order: 10g
Purity: 97%
Supply Ability: 100000kg
Release date: 2020-04-08

Career Henan Chemical Co

Product: 6-bromoisoindolin-1-one 675109-26-9
Price: US $1.00/g
Min. Order: 1g
Purity: 99%
Supply Ability: 1000KGS
Release date: 2019-12-20

675109-26-9, 6-bromoisoindolin-1-oneRelated Search:

6-NITRO-ISOINDOLIN-1-ONE 5-BROMO-2,3-DIHYDRO-ISOINDOL-1-ONE 4-bromoisoindolin-1-one 4-nitroisoindolin-1-one 6-AMino-2,3-dihydroisoindol-1-one

6-Bromo-2,3-dihydroisoindolin-1-one

1H-Isoindol-1-one, 6-broMo-2,3-dihydro-

6-bromoisoindolin-1-one

6-broMo-2,3-dihydro-1H-isoindol-1-one

6-BroMo-2,3-dihydro-isoindol-1-one

6-BroMoisoindolin-1-one, 95+%

1-Piperidinecarboxylicacid,4-(2-bromoethyl)-,1,4-dimethylethylester

675109-26-9