4-bromoisoindolin-1-one
- Product Name
- 4-bromoisoindolin-1-one
- CAS No.
- 337536-15-9
- Chemical Name
- 4-bromoisoindolin-1-one
- Synonyms
- 4-Bromo-1-isoindolinone;4-bromoisoindolin-1-one;4-BroMoisoindoline-1-one;4-Bromoisoindolin-1-one?New;4-Bromoisoindolin-1-one 97%;4-broMo-2,3-dihydro-1H-isoindol-1-one;1H-Isoindol-1-one,4-broMo-2 3-dihydro-;Ethanone,1-[3,6-dihydroxy-2-methoxy-7-(phenylmethoxy)phenyl]-
- CBNumber
- CB31515791
- Molecular Formula
- C8H6BrNO
- Formula Weight
- 212.04
- MOL File
- 337536-15-9.mol
4-bromoisoindolin-1-one Property
- Boiling point:
- 448.9±45.0 °C(Predicted)
- Density
- 1.666
- storage temp.
- Sealed in dry,Room Temperature
- pka
- 13.69±0.20(Predicted)
- form
- solid
- color
- Off-white to light yellow
Safety
- HS Code
- 2933790090
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P260Do not breathe dust/fume/gas/mist/vapours/spray.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P312Call a POISON CENTER or doctor/physician if you feel unwell.
N-Bromosuccinimide Price
- Product number
- B997138
- Product name
- 4-Bromo-2,3-dihydroisoindol-1-one
- Packaging
- 500mg
- Price
- $155
- Updated
- 2021/12/16
- Product number
- FB32629
- Product name
- 4-Bromoisoindolin-1-one
- Packaging
- 500mg
- Price
- $60
- Updated
- 2021/12/16
- Product number
- FB32629
- Product name
- 4-Bromoisoindolin-1-one
- Packaging
- 1g
- Price
- $94
- Updated
- 2021/12/16
- Product number
- 074520
- Product name
- 4-Bromoisoindolin-1-one
- Purity
- 95+%
- Packaging
- 1g
- Price
- $102
- Updated
- 2021/12/16
- Product number
- FB32629
- Product name
- 4-Bromoisoindolin-1-one
- Packaging
- 5G
- Price
- $280
- Updated
- 2021/12/16
4-bromoisoindolin-1-one Chemical Properties,Usage,Production
Uses
4-bromoisoindolin-1-one can be used as organic synthesis intermediate and pharmaceutical intermediate, mainly used in laboratory research and development process and chemical production process.
Synthesis
To a solution of the 3-bromo-2-bromomethyl-benzoic acid methyl ester (2.74 g, 8.88 [MMOL)] in tetrahydrofuran (70 [ML)] at [0??C] was added 30 percent aq. ammonia (10 ml) and the mixture stirred at room temperature under nitrogen for 18 hours. The solvent was removed by evaporation under reduced pressure. The white residue was partitioned between ethyl acetate (50 mi) and 2M citric acid (50 [ML).] The ethyl acetate was dried magnesium sulfate, filtered and solvent removed by evaporation under reduced pressure. The orange oil was dissolved in minimum [DICHLOROMETHANE] and purified by flash chromatography on silica gel eluting with a solvent gradient of [DICHOROMETHANE/METHANOL] (9: 1) to give the title compound (1.5 g, 80 percent) as a white solid.
4-bromoisoindolin-1-one Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 4-bromoisoindolin-1-one manufacturers
- Product
- 4-bromoisoindolin-1-one 337536-15-9
- Price
- US $1.00/KG
- Min. Order
- 1KG
- Purity
- 95%
- Supply Ability
- 500KG
- Release date
- 2018-08-19