ChemicalBook > CAS DataBase List > 4-bromoisoindolin-1-one

4-bromoisoindolin-1-one

Product Name
4-bromoisoindolin-1-one
CAS No.
337536-15-9
Chemical Name
4-bromoisoindolin-1-one
Synonyms
4-Bromo-1-isoindolinone;4-bromoisoindolin-1-one;4-BroMoisoindoline-1-one;4-Bromoisoindolin-1-one?New;4-Bromoisoindolin-1-one 97%;4-broMo-2,3-dihydro-1H-isoindol-1-one;1H-Isoindol-1-one,4-broMo-2 3-dihydro-;Ethanone,1-[3,6-dihydroxy-2-methoxy-7-(phenylmethoxy)phenyl]-
CBNumber
CB31515791
Molecular Formula
C8H6BrNO
Formula Weight
212.04
MOL File
337536-15-9.mol
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4-bromoisoindolin-1-one Property

Boiling point:
448.9±45.0 °C(Predicted)
Density 
1.666
storage temp. 
Sealed in dry,Room Temperature
pka
13.69±0.20(Predicted)
form 
solid
color 
Off-white to light yellow
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Safety

HS Code 
2933790090
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P260Do not breathe dust/fume/gas/mist/vapours/spray.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P312Call a POISON CENTER or doctor/physician if you feel unwell.

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N-Bromosuccinimide Price

TRC
Product number
B997138
Product name
4-Bromo-2,3-dihydroisoindol-1-one
Packaging
500mg
Price
$155
Updated
2021/12/16
Biosynth Carbosynth
Product number
FB32629
Product name
4-Bromoisoindolin-1-one
Packaging
500mg
Price
$60
Updated
2021/12/16
Biosynth Carbosynth
Product number
FB32629
Product name
4-Bromoisoindolin-1-one
Packaging
1g
Price
$94
Updated
2021/12/16
Matrix Scientific
Product number
074520
Product name
4-Bromoisoindolin-1-one
Purity
95+%
Packaging
1g
Price
$102
Updated
2021/12/16
Biosynth Carbosynth
Product number
FB32629
Product name
4-Bromoisoindolin-1-one
Packaging
5G
Price
$280
Updated
2021/12/16
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4-bromoisoindolin-1-one Chemical Properties,Usage,Production

Uses

4-bromoisoindolin-1-one can be used as organic synthesis intermediate and pharmaceutical intermediate, mainly used in laboratory research and development process and chemical production process.

Synthesis


To a solution of the 3-bromo-2-bromomethyl-benzoic acid methyl ester (2.74 g, 8.88 [MMOL)] in tetrahydrofuran (70 [ML)] at [0??C] was added 30 percent aq. ammonia (10 ml) and the mixture stirred at room temperature under nitrogen for 18 hours. The solvent was removed by evaporation under reduced pressure. The white residue was partitioned between ethyl acetate (50 mi) and 2M citric acid (50 [ML).] The ethyl acetate was dried magnesium sulfate, filtered and solvent removed by evaporation under reduced pressure. The orange oil was dissolved in minimum [DICHLOROMETHANE] and purified by flash chromatography on silica gel eluting with a solvent gradient of [DICHOROMETHANE/METHANOL] (9: 1) to give the title compound (1.5 g, 80 percent) as a white solid.

4-bromoisoindolin-1-one Preparation Products And Raw materials

Raw materials

Preparation Products

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4-bromoisoindolin-1-one Suppliers

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View Lastest Price from 4-bromoisoindolin-1-one manufacturers

Career Henan Chemical Co
Product
4-bromoisoindolin-1-one 337536-15-9
Price
US $1.00/KG
Min. Order
1KG
Purity
95%
Supply Ability
500KG
Release date
2018-08-19

337536-15-9, 4-bromoisoindolin-1-oneRelated Search:

methyl 4-bromoquinoline-8-carboxylate 6-bromoisoindolin-1-one 6-NITRO-ISOINDOLIN-1-ONE 5-BROMO-2,3-DIHYDRO-ISOINDOL-1-ONE 4-nitroisoindolin-1-one 6-AMino-2,3-dihydroisoindol-1-one 1,2-Bis(tetrabromophthalimido) ethane 3,4,5,6-TETRABROMOPHTHALIMIDE 4-BROMO-6,7-DIMETHOXY-ISOINDOLIN-1-ONE 4-bromoisoindolin-1-one AURORA 17475 AURORA 17478 4,5,6,7-TETRABROMO-2-(OXIRAN-2-YLMETHYL)ISOINDOLINE-1,3-DIONE N,N'-(methylenedi-p-phenylene)bis[3,4,5,6,-tetrabromophthalimide] AURORA 17477 AURORA 17474 AURORA 17308 AURORA 17476

  • 4-bromoisoindolin-1-one
  • 4-BroMoisoindoline-1-one
  • 1H-Isoindol-1-one,4-broMo-2 3-dihydro-
  • 4-broMo-2,3-dihydro-1H-isoindol-1-one
  • 4-Bromoisoindolin-1-one 97%
  • Ethanone,1-[3,6-dihydroxy-2-methoxy-7-(phenylmethoxy)phenyl]-
  • 4-Bromo-1-isoindolinone
  • 4-Bromoisoindolin-1-one?New
  • 337536-15-9