N-(2-Bromoethyl)phthalimide

Product Name: N-(2-Bromoethyl)phthalimide
CAS No.: 574-98-1
Chemical Name: N-(2-Bromoethyl)phthalimide
Synonyms: 2-(2-Bromoethyl)isoindoline-1,3-dione;2-(2-BROMO-ETHYL)-ISOINDOLE-1,3-DIONE;AURORA KA-575;N-(2-BromoethyL;TIMTEC-BB SBB003129;N-(2-Bromoethyl)phth;SPECS AE-641/00791032;-Bromoethylphthalimide;LABOTEST-BB LT00439821;N-BROMOETHYLPHTHALIMIDE
CBNumber: CB8227544
Molecular Formula: C10H8BrNO2
Formula Weight: 254.08
MOL File: 574-98-1.mol

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N-(2-Bromoethyl)phthalimide Property

Melting point:: 80-83 °C (lit.)
Boiling point:: 318 °C
Density: 1.6254 (rough estimate)
refractive index: 1.6320 (estimate)
storage temp.: Sealed in dry,Room Temperature
pka: -2.35±0.20(Predicted)
form: Crystalline Powder
color: White to slightly pink or beige
Water Solubility: insoluble
BRN: 148736
CAS DataBase Reference: 574-98-1(CAS DataBase Reference)
NIST Chemistry Reference: N-(beta-bromoethyl)phthalimide(574-98-1)
EPA Substance Registry System: 1H-Isoindole-1,3(2H)-dione, 2-(2-bromoethyl)- (574-98-1)

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Safety

Risk Statements: 36/37/38
Safety Statements: 24/25
WGK Germany: 3
TSCA: Yes
HS Code: 29251995

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Danger

Hazard statements

H290May be corrosive to metals

H314Causes severe skin burns and eye damage

Precautionary statements

P234Keep only in original container.

P260Do not breathe dust/fume/gas/mist/vapours/spray.

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P301+P330+P331IF SWALLOWED: Rinse mouth. Do NOT induce vomiting.

P303+P361+P353IF ON SKIN (or hair): Remove/Take off Immediately all contaminated clothing. Rinse SKIN with water/shower.

P363Wash contaminated clothing before reuse.

P390Absorb spillage to prevent material damage.

P405Store locked up.

P406Store in corrosive resistant/… container with a resistant inner liner.

P501Dispose of contents/container to..…

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N-Bromosuccinimide Price

Sigma-Aldrich

Product number: B66302
Product name: N-(2-Bromoethyl)phthalimide
Purity: 95%
Packaging: 25g
Price: $52.8
Updated: 2024/03/01

Sigma-Aldrich

Product number: B66302
Product name: N-(2-Bromoethyl)phthalimide
Purity: 95%
Packaging: 100g
Price: $57.78
Updated: 2024/03/01

TCI Chemical

Product number: B0597
Product name: N-(2-Bromoethyl)phthalimide
Purity: >98.0%(GC)(T)
Packaging: 25g
Price: $48
Updated: 2024/03/01

TCI Chemical

Product number: B0597
Product name: N-(2-Bromoethyl)phthalimide
Purity: >98.0%(GC)(T)
Packaging: 100g
Price: $157
Updated: 2024/03/01

Alfa Aesar

Product number: A12164
Product name: N-(2-Bromoethyl)phthalimide, 98+%
Packaging: 25g
Price: $38.65
Updated: 2024/03/01

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N-(2-Bromoethyl)phthalimide Chemical Properties,Usage,Production

Chemical Properties

white powder

Uses

N-(2-Bromoethyl)phthalimide is an intermediate used in organic synthesis. It can react with phenyl magnesium bromide to get 2-(2-bromo-ethyl)-3-hydroxy-3-phenyl-isoindolin-1-one.

Synthesis Reference(s)

Journal of the American Chemical Society, 71, p. 2425, 1949 DOI: 10.1021/ja01175a052
Organic Syntheses, Coll. Vol. 1, p. 119, 1941

Purification Methods

The following is to be carried out in an efficient FUME HOOD. Dissolve the compound (180g) in CS2 (500 mL) by refluxing for 15minutes (to cause the separation of the most likely impurity, 1,2-diphthalimidoethane), filter and evaporate under reduced pressure. The product forms light tan crystals (m 78-80o). Recrystallise it from EtOH (charcoal) [the compound (50g) is dissolved in hot 75% EtOH (200mL), boiled for ca 10 minutes, carbon is added (5g, Norite), filter and cool to 0o], to give white crystals (40g) which can be recrystallised (m 80-81o); and further recrystallisation gives m 82-83o. [Salzberg & Supniewski Org Synth Coll Vol I 119 1932, Landini & Rolla Synthesis 389 1976, Beilstein 21/10 V 275.]

N-(2-Bromoethyl)phthalimide Preparation Products And Raw materials

Raw materials

Monoethanolamine Phthalic anhydride

Preparation Products

hexahydro-2H-azocine-1-ethylamine guanethidine

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N-(2-Bromoethyl)phthalimide Suppliers

Americas 1 Austria 1 Belgium 3 China 195 Europe 3 France 1 Germany 10 India 29 Japan 5 Slovakia 1 South Korea 1 Switzerland 2 The Netherlands 5 United Kingdom 15 United States 48 Global 320

Alkemi BVBA

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Country: Belgium
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Advantage: 58

Acros Organics (Part of Thermo Fisher Scientific )

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Acros Organics

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Country: Belgium
ProdList: 6772
Advantage: 81

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View Lastest Price from N-(2-Bromoethyl)phthalimide manufacturers

Hebei Chuanghai Biotechnology Co,.LTD

Product: N-(2-Bromoethyl)phthalimide 574-98-1
Price: US $10.00/KG
Min. Order: 1KG
Purity: 99.8%
Supply Ability: 100000kgs
Release date: 2024-08-20

Career Henan Chemical Co

Product: N-(2-Bromoethyl)phthalimide 574-98-1
Price: US $1.00/g
Min. Order: 100g
Purity: 99%
Supply Ability: G/KG/T
Release date: 2019-12-20

574-98-1, N-(2-Bromoethyl)phthalimideRelated Search:

N-(3-BROMOPROPYL)PHTHALIMIDE N-Methylphthalimide Succinimide Bismaleimide Potassium phthalimide 4-Aminophthalimide 4-Nitrophthalimide 3-Nitrophthalimide N-Hydroxyphthalimide O-Phthalimide DIALIFOS Isoindoline BROMO 2-DEOXY-2-N-PHTHALIMIDO-3,4,6-TRI-O-ACETYL-A, B-D-GLUCOPYRANOSIDE (S)-N-(1-BROMO-2-PROPYL)PHTHALIMIDE N-(2-Bromoethyl)phthalimide 2-(2-bromoethyl)-5-nitro-2,3-dihydro-1H-isoindole-1,3-dione 2-(2-bromoethyl)-4-nitro-1H-isoindole-1,3(2H)-dione SPECS AJ-333/25116002

AURORA KA-575

BETA-BROMOETHYLPHTHALIMIDE

2-(2-BROMO-ETHYL)-ISOINDOLE-1,3-DIONE

TIMTEC-BB SBB003129

1-Bromo-2-phthalimidoethane

1H-Isoindole-1,3(2H)-dione, 2-(2-bromoethyl)-

2-(2-Bromoethyl)-1H-isoindole-1,3(2H)-dione

2-(2-bromoethyl)-1h-isoindole-3(2h)-dione

2-(2-Bromoethyl)phthalimide

2-(Bromoethyl)phthalimide

2-Phthalimidoethyl bromide

beta-Phthalimidoethyl bromide

b-Phthalimidoethyl bromide

-Bromoethylphthalimide

N-(2-Bromoethyl)pthalimide

LABOTEST-BB LT00439821

N-(b-Bromoethyl)phthalimide

SPECS AE-641/00791032

N-(2-BROMOETHYL)PHTALIMIDE

N-(2-BROMOETHYL)PHTHALIMIDE

N-(2-BROMOETHYLYL)-PHTALIMIDE

N-(2-BROMETHYL)-PHTHALIMID

N-2-Bromethylphthalimide

Phthalimide, N-(2-bromoethyl)-

N-BROMOETHYLPHTHALIMIDE

N-(2-Bromoethyl)phthalimide,98+%

N-(2-Bromoethyl)phthalimide, 99+%

N-(2-BroMoethyl)phthaliMide, 99+% 100GR

N-(2-BroMoethyl)phthaliMide, 99+% 25GR

2-(2-Bromoethyl)-2H-isoindole-1,3-dione

2-(2-Bromoethyl)isoindoline-1,3-dione

N-(2-Bromoethyl)phthalimide ,96%

N-(2-Bromoethyl)phth

<i>N</i>-(2-Bromoethyl)phthalimide

2-(2-bromoethyl)isoindoline-1,3-quinone

N-(2-BroMoethyl)phthaliMide 95%

Phthalimide, N-(2-bromoethyl)- (8CI)

N-(2-BromoethyL

N-(2-Bromoethyl)phthalimide&gt

574-98-1

Carbonyl Compounds

Building Blocks

Organic Building Blocks

Cyclic Imides

N-Substituted Maleimides, Succinimides & Phthalimides

N-Substituted Phthalimides

N-Substituted Maleimides, Succinimides & Phthalimides

N-Substituted Phthalimides

Bifunctional CrosslinkersOrganic Building Blocks

Carbonyl Compounds

Cyclic Imides

Linkers

Peptide Synthesis

Bifunctional Linkers

Building Blocks

Carbonyl Compounds

Chemical Biology

Chemical Synthesis