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N-(2-Bromoethyl)phthalimide

Product Name
N-(2-Bromoethyl)phthalimide
CAS No.
574-98-1
Chemical Name
N-(2-Bromoethyl)phthalimide
Synonyms
2-(2-Bromoethyl)isoindoline-1,3-dione;2-(2-BROMO-ETHYL)-ISOINDOLE-1,3-DIONE;AURORA KA-575;N-(2-BromoethyL;TIMTEC-BB SBB003129;N-(2-Bromoethyl)phth;SPECS AE-641/00791032;-Bromoethylphthalimide;LABOTEST-BB LT00439821;N-BROMOETHYLPHTHALIMIDE
CBNumber
CB8227544
Molecular Formula
C10H8BrNO2
Formula Weight
254.08
MOL File
574-98-1.mol
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N-(2-Bromoethyl)phthalimide Property

Melting point:
80-83 °C (lit.)
Boiling point:
318 °C
Density 
1.6254 (rough estimate)
refractive index 
1.6320 (estimate)
storage temp. 
Sealed in dry,Room Temperature
pka
-2.35±0.20(Predicted)
form 
Crystalline Powder
color 
White to slightly pink or beige
Water Solubility 
insoluble
BRN 
148736
CAS DataBase Reference
574-98-1(CAS DataBase Reference)
NIST Chemistry Reference
N-(beta-bromoethyl)phthalimide(574-98-1)
EPA Substance Registry System
1H-Isoindole-1,3(2H)-dione, 2-(2-bromoethyl)- (574-98-1)
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Safety

Risk Statements 
36/37/38
Safety Statements 
24/25
WGK Germany 
3
TSCA 
Yes
HS Code 
29251995
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Danger
Hazard statements

H290May be corrosive to metals

H314Causes severe skin burns and eye damage

Precautionary statements

P234Keep only in original container.

P260Do not breathe dust/fume/gas/mist/vapours/spray.

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P301+P330+P331IF SWALLOWED: Rinse mouth. Do NOT induce vomiting.

P303+P361+P353IF ON SKIN (or hair): Remove/Take off Immediately all contaminated clothing. Rinse SKIN with water/shower.

P363Wash contaminated clothing before reuse.

P390Absorb spillage to prevent material damage.

P405Store locked up.

P406Store in corrosive resistant/… container with a resistant inner liner.

P501Dispose of contents/container to..…

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N-Bromosuccinimide Price

Sigma-Aldrich
Product number
B66302
Product name
N-(2-Bromoethyl)phthalimide
Purity
95%
Packaging
25g
Price
$52.8
Updated
2024/03/01
Sigma-Aldrich
Product number
B66302
Product name
N-(2-Bromoethyl)phthalimide
Purity
95%
Packaging
100g
Price
$57.78
Updated
2024/03/01
TCI Chemical
Product number
B0597
Product name
N-(2-Bromoethyl)phthalimide
Purity
>98.0%(GC)(T)
Packaging
25g
Price
$48
Updated
2024/03/01
TCI Chemical
Product number
B0597
Product name
N-(2-Bromoethyl)phthalimide
Purity
>98.0%(GC)(T)
Packaging
100g
Price
$157
Updated
2024/03/01
Alfa Aesar
Product number
A12164
Product name
N-(2-Bromoethyl)phthalimide, 98+%
Packaging
25g
Price
$38.65
Updated
2024/03/01
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N-(2-Bromoethyl)phthalimide Chemical Properties,Usage,Production

Chemical Properties

white powder

Uses

N-(2-Bromoethyl)phthalimide is an intermediate used in organic synthesis. It can react with phenyl magnesium bromide to get 2-(2-bromo-ethyl)-3-hydroxy-3-phenyl-isoindolin-1-one.

Synthesis Reference(s)

Journal of the American Chemical Society, 71, p. 2425, 1949 DOI: 10.1021/ja01175a052
Organic Syntheses, Coll. Vol. 1, p. 119, 1941

Purification Methods

The following is to be carried out in an efficient FUME HOOD. Dissolve the compound (180g) in CS2 (500 mL) by refluxing for 15minutes (to cause the separation of the most likely impurity, 1,2-diphthalimidoethane), filter and evaporate under reduced pressure. The product forms light tan crystals (m 78-80o). Recrystallise it from EtOH (charcoal) [the compound (50g) is dissolved in hot 75% EtOH (200mL), boiled for ca 10 minutes, carbon is added (5g, Norite), filter and cool to 0o], to give white crystals (40g) which can be recrystallised (m 80-81o); and further recrystallisation gives m 82-83o. [Salzberg & Supniewski Org Synth Coll Vol I 119 1932, Landini & Rolla Synthesis 389 1976, Beilstein 21/10 V 275.]

N-(2-Bromoethyl)phthalimide Preparation Products And Raw materials

Raw materials

Monoethanolamine Phthalic anhydride

Preparation Products

hexahydro-2H-azocine-1-ethylamine guanethidine
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N-(2-Bromoethyl)phthalimide Suppliers

Americas 1 Austria 1 Belgium 3 China 195 Europe 3 France 1 Germany 10 India 29 Japan 5 Slovakia 1 South Korea 1 Switzerland 2 The Netherlands 5 United Kingdom 15 United States 48 Global 320
MDP ChemControl Ltd.
Tel
--
Fax
--
Email
chemcontrol@nextra.sk
Country
Slovakia
ProdList
6700
Advantage
60
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View Lastest Price from N-(2-Bromoethyl)phthalimide manufacturers

Hebei Chuanghai Biotechnology Co,.LTD
Product
N-(2-Bromoethyl)phthalimide 574-98-1
Price
US $10.00/KG
Min. Order
1KG
Purity
99.8%
Supply Ability
100000kgs
Release date
2024-08-20
Career Henan Chemical Co
Product
N-(2-Bromoethyl)phthalimide 574-98-1
Price
US $1.00/g
Min. Order
100g
Purity
99%
Supply Ability
G/KG/T
Release date
2019-12-20

574-98-1, N-(2-Bromoethyl)phthalimideRelated Search:

N-(3-BROMOPROPYL)PHTHALIMIDE N-Methylphthalimide Succinimide Bismaleimide Potassium phthalimide 4-Aminophthalimide 4-Nitrophthalimide 3-Nitrophthalimide N-Hydroxyphthalimide O-Phthalimide DIALIFOS Isoindoline BROMO 2-DEOXY-2-N-PHTHALIMIDO-3,4,6-TRI-O-ACETYL-A, B-D-GLUCOPYRANOSIDE (S)-N-(1-BROMO-2-PROPYL)PHTHALIMIDE N-(2-Bromoethyl)phthalimide 2-(2-bromoethyl)-5-nitro-2,3-dihydro-1H-isoindole-1,3-dione 2-(2-bromoethyl)-4-nitro-1H-isoindole-1,3(2H)-dione SPECS AJ-333/25116002

  • AURORA KA-575
  • BETA-BROMOETHYLPHTHALIMIDE
  • 2-(2-BROMO-ETHYL)-ISOINDOLE-1,3-DIONE
  • TIMTEC-BB SBB003129
  • 1-Bromo-2-phthalimidoethane
  • 1H-Isoindole-1,3(2H)-dione, 2-(2-bromoethyl)-
  • 2-(2-Bromoethyl)-1H-isoindole-1,3(2H)-dione
  • 2-(2-bromoethyl)-1h-isoindole-3(2h)-dione
  • 2-(2-Bromoethyl)phthalimide
  • 2-(Bromoethyl)phthalimide
  • 2-Phthalimidoethyl bromide
  • beta-Phthalimidoethyl bromide
  • b-Phthalimidoethyl bromide
  • -Bromoethylphthalimide
  • N-(2-Bromoethyl)pthalimide
  • LABOTEST-BB LT00439821
  • N-(b-Bromoethyl)phthalimide
  • SPECS AE-641/00791032
  • N-(2-BROMOETHYL)PHTALIMIDE
  • N-(2-BROMOETHYL)PHTHALIMIDE
  • N-(2-BROMOETHYLYL)-PHTALIMIDE
  • N-(2-BROMETHYL)-PHTHALIMID
  • N-2-Bromethylphthalimide
  • Phthalimide, N-(2-bromoethyl)-
  • N-BROMOETHYLPHTHALIMIDE
  • N-(2-Bromoethyl)phthalimide,98+%
  • N-(2-Bromoethyl)phthalimide, 99+%
  • N-(2-BroMoethyl)phthaliMide, 99+% 100GR
  • N-(2-BroMoethyl)phthaliMide, 99+% 25GR
  • 2-(2-Bromoethyl)-2H-isoindole-1,3-dione
  • 2-(2-Bromoethyl)isoindoline-1,3-dione
  • N-(2-Bromoethyl)phthalimide ,96%
  • N-(2-Bromoethyl)phth
  • <i>N</i>-(2-Bromoethyl)phthalimide
  • 2-(2-bromoethyl)isoindoline-1,3-quinone
  • N-(2-BroMoethyl)phthaliMide 95%
  • Phthalimide, N-(2-bromoethyl)- (8CI)
  • N-(2-BromoethyL
  • N-(2-Bromoethyl)phthalimide&gt
  • 574-98-1
  • Carbonyl Compounds
  • Building Blocks
  • Organic Building Blocks
  • Cyclic Imides
  • N-Substituted Maleimides, Succinimides & Phthalimides
  • N-Substituted Phthalimides
  • N-Substituted Maleimides, Succinimides & Phthalimides
  • N-Substituted Phthalimides
  • Bifunctional CrosslinkersOrganic Building Blocks
  • Carbonyl Compounds
  • Cyclic Imides
  • Linkers
  • Peptide Synthesis
  • Bifunctional Linkers
  • Building Blocks
  • Carbonyl Compounds
  • Chemical Biology
  • Chemical Synthesis