1-Chloro-4-(2-chloroethoxy)benzene
- Product Name
- 1-Chloro-4-(2-chloroethoxy)benzene
- CAS No.
- 13001-28-0
- Chemical Name
- 1-Chloro-4-(2-chloroethoxy)benzene
- Synonyms
- 2-(4-CHLOROPHENOXY)ETHYL CHLORIDE;4-(2-Chloroethoxy)-Chloro-Benzene;1-Chloro-4-(chloroethoxy)-benzene;1-Chloro-2-(4-chlorophenoxy)ethane;1-CHLORO-4-(2-CHLOROETHOXY)BENZENE;Benzene, 1-chloro-4-(2-chloroethoxy)-
- CBNumber
- CB8300649
- Molecular Formula
- C8H8Cl2O
- Formula Weight
- 191.05
- MOL File
- 13001-28-0.mol
1-Chloro-4-(2-chloroethoxy)benzene Property
- Melting point:
- 39 °C
- Boiling point:
- 184-186 °C(Press: 92 Torr)
- Density
- 1.246±0.06 g/cm3(Predicted)
- storage temp.
- Sealed in dry,Room Temperature
- CAS DataBase Reference
- 13001-28-0(CAS DataBase Reference)
- EPA Substance Registry System
- Benzene, 1-chloro-4-(2-chloroethoxy)- (13001-28-0)
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Danger
- Hazard statements
-
H315Causes skin irritation
H318Causes serious eye damage
H411Toxic to aquatic life with long lasting effects
- Precautionary statements
-
P264Wash hands thoroughly after handling.
P264Wash skin thouroughly after handling.
P270Do not eat, drink or smoke when using this product.
P273Avoid release to the environment.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P332+P313IF SKIN irritation occurs: Get medical advice/attention.
P391Collect spillage. Hazardous to the aquatic environment
P501Dispose of contents/container to..…
N-Bromosuccinimide Price
- Product number
- FC151172
- Product name
- 2-(4-Chlorophenoxy)ethylchloride
- Packaging
- 500mg
- Price
- $80
- Updated
- 2021/12/16
- Product number
- FC151172
- Product name
- 2-(4-Chlorophenoxy)ethylchloride
- Packaging
- 1g
- Price
- $125
- Updated
- 2021/12/16
- Product number
- FC151172
- Product name
- 2-(4-Chlorophenoxy)ethylchloride
- Packaging
- 2g
- Price
- $200
- Updated
- 2021/12/16
- Product number
- FC151172
- Product name
- 2-(4-Chlorophenoxy)ethylchloride
- Packaging
- 5G
- Price
- $300
- Updated
- 2021/12/16
- Product number
- 5523AA
- Product name
- 1-Chloro-4-(2-chloroethoxy)benzene
- Packaging
- 1g
- Price
- $308
- Updated
- 2021/12/16
1-Chloro-4-(2-chloroethoxy)benzene Chemical Properties,Usage,Production
Synthesis
96-49-1
75-44-5
106-48-9
13001-28-0
Example P1: Synthesis of 4-chloro-(2-chloroethoxy)-benzene 1. 1 g of tributylamine was added to the reactor as a catalyst, followed by the sequential addition of 26.4 g of 4-chlorophenol and 18.7 g of ethylene carbonate. 2. The reaction mixture was slowly heated to 150 °C and the reaction was maintained at this temperature for about 3 hours until the release of carbon dioxide gas ceased. 3. Upon completion of the reaction, the mixture was cooled to 85 °C and 1 g of dimethylformamide was added as a solvent. 4. 24 g of phosgene was passed into the reaction mixture in the form of a bulb at 85 °C. 5. The reaction temperature was maintained at 85 °C for 8 hours, after which the temperature was reduced to 60 °C. The reaction temperature was reduced to 60 °C. 6. 100 ml of water was added to quench the excess phosgene, followed by neutralization of the reaction mixture with 10.5 g of 25% aqueous sodium hydroxide. 7. The organic layer was separated and purified by reduced pressure distillation (150°-152 °C/40 mb) to give 36.0 g (93% yield) of the target product 4-chloro-(2-chloroethoxy)-benzene.
References
[1] Patent: US4959501, 1990, A
[2] Patent: US4806528, 1989, A
1-Chloro-4-(2-chloroethoxy)benzene Preparation Products And Raw materials
Raw materials
Preparation Products
1-Chloro-4-(2-chloroethoxy)benzene Suppliers
- Tel
- 821-50328103-801 18930552037
- Fax
- 86-21-50328109
- 3bsc@sina.com
- Country
- China
- ProdList
- 15838
- Advantage
- 69
- Tel
- 86-027-67849912
- Fax
- 86-027-87531808
- sales@chemwish.com
- Country
- China
- ProdList
- 35896
- Advantage
- 56
- Tel
- 025-58862853 18915922038
- Fax
- +86-025-58862853
- sales@endesachem.com
- Country
- China
- ProdList
- 591
- Advantage
- 58
- Tel
- 025-025-58367986 18913956109
- Fax
- QQ:3209878052
- amy.xiang@ally-chem.com
- Country
- China
- ProdList
- 567
- Advantage
- 58
- Tel
- 571-89925085
- Fax
- 0086-571-89925065
- sales@amadischem.com
- Country
- China
- ProdList
- 131957
- Advantage
- 58
- Tel
- 022-59987777 13552403979
- jia_guoqiang@wuxiapptec.com
- Country
- China
- ProdList
- 22345
- Advantage
- 58
- Tel
- 025-58851090 15955137747
- Fax
- (6)02557626880
- sales01@aikonchem.com
- Country
- China
- ProdList
- 15949
- Advantage
- 58
- Tel
- 0512-87819718 18912655635
- 2587879032@qq.com
- Country
- China
- ProdList
- 1401
- Advantage
- 58
- Tel
- +86-0571-88938639 +8617705817739
- Fax
- +86-571-88938652，+86-571- 88492614
- info@dycnchem.com
- Country
- China
- ProdList
- 52846
- Advantage
- 58
- Tel
- 021-20432219 13918097649
- Fax
- QQ79021576
- li_jinfei@acblock-lab.com
- Country
- China
- ProdList
- 9673
- Advantage
- 58
View Lastest Price from 1-Chloro-4-(2-chloroethoxy)benzene manufacturers
- Product
- 1-Chloro-4-(2-chloroethoxy)benzene 13001-28-0
- Price
- US $3.00/KG
- Min. Order
- 1KG
- Purity
- 98%
- Supply Ability
- 200KG
- Release date
- 2020-02-20