ChemicalBook > CAS DataBase List > 1-METHYL-1H-INDAZOL-6-YLAMINE

1-METHYL-1H-INDAZOL-6-YLAMINE

Product Name: 1-METHYL-1H-INDAZOL-6-YLAMINE
CAS No.: 74728-65-7
Chemical Name: 1-METHYL-1H-INDAZOL-6-YLAMINE
Synonyms: 1-methylindazol-6-amine;6-AMINO-1-METHYLINDAZOLE;1-Methyl-1H-indazol-6-amine;6-AMino-1-Methyl-1H-indaz...;1-methyl-1H-indazole-6-amine;6-Amino-1-methyl-1H-indazole;1-METHYL-1H-INDAZOL-6-YLAMINE;1H-Indazol-6-amine, 1-methyl-;1-Methyl-1H-indazole-6-ylamine
CBNumber: CB8442558
Molecular Formula: C8H9N3
Formula Weight: 147.18
MOL File: 74728-65-7.mol

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1-METHYL-1H-INDAZOL-6-YLAMINE Property

Melting point:: 172-173
Boiling point:: 321.6±15.0 °C(Predicted)
Density: 1.27±0.1 g/cm3(Predicted)
storage temp.: Keep in dark place,Inert atmosphere,Room temperature
form: solid
pka: 3.65±0.10(Predicted)
color: Brown

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Safety

Hazard Codes: Xi,Xn
Risk Statements: 22
HazardClass: IRRITANT
HS Code: 29339980

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P271Use only outdoors or in a well-ventilated area.

P280Wear protective gloves/protective clothing/eye protection/face protection.

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N-Bromosuccinimide Price

TRC

Product number: M320908
Product name: 1-Methyl-1H-indazol-6-amine
Packaging: 100mg
Price: $60
Updated: 2021/12/16

Matrix Scientific

Product number: 046137
Product name: 1-Methyl-1H-indazol-6-amine
Purity: >95%
Packaging: 500mg
Price: $65
Updated: 2021/12/16

Matrix Scientific

Product number: 046137
Product name: 1-Methyl-1H-indazol-6-amine
Purity: >95%
Packaging: 1g
Price: $100
Updated: 2021/12/16

Frontier Specialty Chemicals

Product number: CAPOM11356
Product name: 6-Amino-1-methyl-1H-indazole
Purity: 95%
Packaging: 1g
Price: $100
Updated: 2021/12/16

AK Scientific

Product number: Y5542
Product name: 1-Methyl-1H-indazol-6-amine
Packaging: 1g
Price: $117
Updated: 2021/12/16

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1-METHYL-1H-INDAZOL-6-YLAMINE Chemical Properties,Usage,Production

Synthesis

6850-23-3

74728-65-7

Step B: Synthesis of 1-methyl-1H-indazol-6-amine; A mixture of 1-methyl-6-nitro-1H-indazole (0.480 g, 2.71 mmol), platinum oxide (50 mg), ethanol (20 mL), and tetrahydrofuran (5 mL) was subjected to a hydrogenation reaction apparatus under atmospheric pressure. The reaction was stirred at room temperature for 1.5 hours under hydrogen pressure of 30 psi. Upon completion of the reaction, the catalyst was removed by filtration and the filtrate was concentrated under reduced pressure to give 1-methyl-1H-indazol-6-amine (0.395 g, 99% yield) as an off-white solid. The product was characterized by 1H NMR (500 MHz, CDCl3): δ 7.80 (s, 1H), 7.48 (d, J = 8.5 Hz, 1H), 6.57 (dd, J = 8.5, 1.8 Hz, 1H), 6.53 (s, 1H), 3.94 (s, 3H), 3.86 (br s, 2H); ESI MS m/z 148 [M + H ]+.

References

[1] Patent: WO2009/42907, 2009, A1. Location in patent: Page/Page column 84-85
[2] Bioorganic and Medicinal Chemistry, 2015, vol. 23, # 21, p. 6855 - 6868
[3] Patent: CN104876912, 2017, B. Location in patent: Paragraph 0047; 0193; 0194; 0197; 0198
[4] Patent: WO2013/100632, 2013, A1. Location in patent: Page/Page column 88
[5] Patent: US2014/371219, 2014, A1. Location in patent: Paragraph 0611

1-METHYL-1H-INDAZOL-6-YLAMINE Preparation Products And Raw materials

Raw materials

Preparation Products

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1-METHYL-1H-INDAZOL-6-YLAMINE Suppliers

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View Lastest Price from 1-METHYL-1H-INDAZOL-6-YLAMINE manufacturers

Career Henan Chemical Co

Product: 1-METHYL-1H-INDAZOL-6-YLAMINE 74728-65-7
Price: US $1.00/g
Min. Order: 1g
Purity: 99.0%
Supply Ability: 100 kg
Release date: 2020-01-10

74728-65-7, 1-METHYL-1H-INDAZOL-6-YLAMINERelated Search:

1-METHYL-1H-INDAZOL-6-YLAMINE 1-METHYL-6-NITRO-1H-INDAZOLE 3-methyl-1H-indazol-6-amine 6-AMINO-2-METHYL-2H-INDAZOLE 2-METHYL-2H-INDAZOL-5-YLAMINE 6-METHYL-1H-INDAZOL-5-YLAMINE 1-Methyl-1H-indazol-4-ylamine 1-METHYL-1H-INDAZOL-5-YLAMINE,1-METHYL-1H-INDAZOL-5-YLAMINE TRIHYDROCHLORIDE 3-METHYL-1H-INDAZOL-5-YLAMINE 2-METHYL-2H-INDAZOL-4-YLAMINE 2-METHYL-2H-INDAZOL-7-YLAMINE Indazole 6-CYANOAMINO-INDAZOLE-1-CARBOXYLIC ACID TERT-BUTYL ESTER 1-(2,6-DICHLORO-BENZYL)-3-PYRROLIDIN-1-YLMETHYL-1H-INDAZOL-6-YLAMINE 6-NITRO-1-(4-TRIFLUOROMETHYL-PHENYL)-1H-INDAZOLE 6-AMINO-3-PYRROLIDIN-1-YLMETHYL-INDAZOLE-1-CARBOXYLIC ACID TERT-BUTYL ESTER 1-BOC-6-AMINO-INDAZOLE 4-Iodo-1-methyl-1H-indazol-3-ylamine

6-AMINO-1-METHYLINDAZOLE

1-METHYL-1H-INDAZOL-6-YLAMINE

1-Methyl-1H-indazol-6-amine

6-Amino-1-methyl-1H-indazole

1-methyl-1H-indazole-6-amine

6-AMino-1-Methyl-1H-indaz...

1-Methyl-1H-indazole-6-ylamine

1H-Indazol-6-amine, 1-methyl-

1-methylindazol-6-amine

74728-65-7

Building Blocks

Indazole

pharmacetical