1-METHYL-1H-INDAZOL-6-YLAMINE
- Product Name
- 1-METHYL-1H-INDAZOL-6-YLAMINE
- CAS No.
- 74728-65-7
- Chemical Name
- 1-METHYL-1H-INDAZOL-6-YLAMINE
- Synonyms
- 1-methylindazol-6-amine;6-AMINO-1-METHYLINDAZOLE;1-Methyl-1H-indazol-6-amine;6-AMino-1-Methyl-1H-indaz...;1-methyl-1H-indazole-6-amine;6-Amino-1-methyl-1H-indazole;1-METHYL-1H-INDAZOL-6-YLAMINE;1H-Indazol-6-amine, 1-methyl-;1-Methyl-1H-indazole-6-ylamine
- CBNumber
- CB8442558
- Molecular Formula
- C8H9N3
- Formula Weight
- 147.18
- MOL File
- 74728-65-7.mol
1-METHYL-1H-INDAZOL-6-YLAMINE Property
- Melting point:
- 172-173
- Boiling point:
- 321.6±15.0 °C(Predicted)
- Density
- 1.27±0.1 g/cm3(Predicted)
- storage temp.
- Keep in dark place,Inert atmosphere,Room temperature
- form
- solid
- pka
- 3.65±0.10(Predicted)
- color
- Brown
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H315Causes skin irritation
H319Causes serious eye irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P271Use only outdoors or in a well-ventilated area.
P280Wear protective gloves/protective clothing/eye protection/face protection.
N-Bromosuccinimide Price
- Product number
- M320908
- Product name
- 1-Methyl-1H-indazol-6-amine
- Packaging
- 100mg
- Price
- $60
- Updated
- 2021/12/16
- Product number
- 046137
- Product name
- 1-Methyl-1H-indazol-6-amine
- Purity
- >95%
- Packaging
- 500mg
- Price
- $65
- Updated
- 2021/12/16
- Product number
- 046137
- Product name
- 1-Methyl-1H-indazol-6-amine
- Purity
- >95%
- Packaging
- 1g
- Price
- $100
- Updated
- 2021/12/16
- Product number
- CAPOM11356
- Product name
- 6-Amino-1-methyl-1H-indazole
- Purity
- 95%
- Packaging
- 1g
- Price
- $100
- Updated
- 2021/12/16
- Product number
- Y5542
- Product name
- 1-Methyl-1H-indazol-6-amine
- Packaging
- 1g
- Price
- $117
- Updated
- 2021/12/16
1-METHYL-1H-INDAZOL-6-YLAMINE Chemical Properties,Usage,Production
Synthesis
6850-23-3
74728-65-7
Step B: Synthesis of 1-methyl-1H-indazol-6-amine; A mixture of 1-methyl-6-nitro-1H-indazole (0.480 g, 2.71 mmol), platinum oxide (50 mg), ethanol (20 mL), and tetrahydrofuran (5 mL) was subjected to a hydrogenation reaction apparatus under atmospheric pressure. The reaction was stirred at room temperature for 1.5 hours under hydrogen pressure of 30 psi. Upon completion of the reaction, the catalyst was removed by filtration and the filtrate was concentrated under reduced pressure to give 1-methyl-1H-indazol-6-amine (0.395 g, 99% yield) as an off-white solid. The product was characterized by 1H NMR (500 MHz, CDCl3): δ 7.80 (s, 1H), 7.48 (d, J = 8.5 Hz, 1H), 6.57 (dd, J = 8.5, 1.8 Hz, 1H), 6.53 (s, 1H), 3.94 (s, 3H), 3.86 (br s, 2H); ESI MS m/z 148 [M + H ]+.
References
[1] Patent: WO2009/42907, 2009, A1. Location in patent: Page/Page column 84-85
[2] Bioorganic and Medicinal Chemistry, 2015, vol. 23, # 21, p. 6855 - 6868
[3] Patent: CN104876912, 2017, B. Location in patent: Paragraph 0047; 0193; 0194; 0197; 0198
[4] Patent: WO2013/100632, 2013, A1. Location in patent: Page/Page column 88
[5] Patent: US2014/371219, 2014, A1. Location in patent: Paragraph 0611
1-METHYL-1H-INDAZOL-6-YLAMINE Preparation Products And Raw materials
Raw materials
Preparation Products
1-METHYL-1H-INDAZOL-6-YLAMINE Suppliers
- Tel
- --
- Fax
- --
- interchim@interchim.com
- Country
- France
- ProdList
- 6302
- Advantage
- 76
View Lastest Price from 1-METHYL-1H-INDAZOL-6-YLAMINE manufacturers
- Product
- 1-METHYL-1H-INDAZOL-6-YLAMINE 74728-65-7
- Price
- US $1.00/g
- Min. Order
- 1g
- Purity
- 99.0%
- Supply Ability
- 100 kg
- Release date
- 2020-01-10