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5-CHLORO-3-CYANOINDOLE

Product Name
5-CHLORO-3-CYANOINDOLE
CAS No.
194490-14-7
Chemical Name
5-CHLORO-3-CYANOINDOLE
Synonyms
5-CHLORO-3-CYANOINDOLE;5-chloro -1H-indole-3-carbonitrile;1H-INDOLE-3-CARBONITRILE, 5-CHLORO-;5-CHLORO-1H-INDOLE-3-CARBONITRILE5-CHLORO-3-CYANOINDOLE
CBNumber
CB8668413
Molecular Formula
C9H5ClN2
Formula Weight
176.6
MOL File
194490-14-7.mol
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5-CHLORO-3-CYANOINDOLE Property

Melting point:
198-199 °C
Boiling point:
383.8±22.0 °C(Predicted)
Density 
1.41
storage temp. 
under inert gas (nitrogen or Argon) at 2-8°C
pka
13.69±0.30(Predicted)
Appearance
White to yellow Solid
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Safety

HS Code 
2933998090
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

AK Scientific
Product number
W4151
Product name
5-Chloro-1H-indole-3-carbonitrile
Packaging
250mg
Price
$169
Updated
2021/12/16
Apolloscientific
Product number
OR913260
Product name
5-Chloro-3-cyanoindole
Purity
95%
Packaging
250mg
Price
$200
Updated
2021/12/16
Matrix Scientific
Product number
074789
Product name
5-Chloro-1H-indole-3-carbonitrile
Purity
95+%
Packaging
250mg
Price
$231
Updated
2021/12/16
SynQuest Laboratories
Product number
3H37-5-2A
Product name
5-Chloro-3-cyanoindole
Purity
95%
Packaging
250mg
Price
$320
Updated
2021/12/16
Apolloscientific
Product number
OR913260
Product name
5-Chloro-3-cyanoindole
Purity
95%
Packaging
1g
Price
$495
Updated
2021/12/16
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5-CHLORO-3-CYANOINDOLE Chemical Properties,Usage,Production

Synthesis

17422-32-1

140-29-4

194490-14-7

GENERAL METHOD: A mixture of CuI (0.6 mmol), 5-chloroindole (0.5 mmol), and phenylacetonitrile (0.6 mmol) in DMF (3.0 mL) was placed in air and reacted with stirring for 34 h at 100 °C, followed by cooling to room temperature. Upon completion of the reaction, the reaction mixture was quenched with 10 mL of water followed by extraction with dichloromethane (DCM, 3 x 10 mL). The organic layers were combined, washed with saturated aqueous sodium chloride solution and dried with anhydrous magnesium sulfate (MgSO?). Finally, the solution was concentrated under reduced pressure and purified by column chromatography to afford the target product 5-chloro-3-cyanoindole.

References

[1] Tetrahedron, 2013, vol. 69, # 21, p. 4236 - 4240

5-CHLORO-3-CYANOINDOLE Preparation Products And Raw materials

Raw materials

Preparation Products

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5-CHLORO-3-CYANOINDOLE Suppliers

Achemica
Tel
--
Fax
--
Email
contact@achemica.com
Country
Switzerland
ProdList
6155
Advantage
50
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View Lastest Price from 5-CHLORO-3-CYANOINDOLE manufacturers

ZHENGZHOU JIUYI TIME NEW MATERIALS CO,.LTD
Product
5-chloro-3-cyanoindole 194490-14-7
Price
US $1.60-9.60/kg
Min. Order
1kg
Purity
99%
Supply Ability
100kg
Release date
2025-06-20
Zhuozhou Wenxi import and Export Co., Ltd
Product
5-CHLORO-3-CYANOINDOLE 194490-14-7
Price
US $15.00-10.00/KG
Min. Order
1KG
Purity
99%+ HPLC
Supply Ability
Monthly supply of 1 ton
Release date
2021-07-10
Zhuozhou Wenxi import and Export Co., Ltd
Product
5-CHLORO-3-CYANOINDOLE 194490-14-7
Price
US $15.00-10.00/KG
Min. Order
1KG
Purity
99%+ HPLC
Supply Ability
Monthly supply of 1 ton
Release date
2021-07-09