3-(2-IODOPHENYL)PROPIONIC ACID
- Product Name
- 3-(2-IODOPHENYL)PROPIONIC ACID
- CAS No.
- 96606-95-0
- Chemical Name
- 3-(2-IODOPHENYL)PROPIONIC ACID
- Synonyms
- 3-(2-Iodphenyl)propionsSre;2-Iodobenzenepropanoic acid;Benzenepropanoic acid, 2-iodo-;3-(2-lodophenyl)propionic acid;3-(2-iodophenyl)propanoic acid;3-(2-IODOPHENYL)PROPIONIC ACID
- CBNumber
- CB8708247
- Molecular Formula
- C9H9IO2
- Formula Weight
- 276.07
- MOL File
- 96606-95-0.mol
3-(2-IODOPHENYL)PROPIONIC ACID Property
- Melting point:
- 86-88°C
- Boiling point:
- 354℃
- Density
- 1.775
- Flash point:
- 168℃
- storage temp.
- Keep in dark place,Sealed in dry,Room Temperature
- form
- solid
- Appearance
- White to off-white Solid
Safety
- Hazard Codes
- Xi,Xn
- Risk Statements
- 22-37/38-41-52/53
- Safety Statements
- 26-39-61
- WGK Germany
- 3
- Hazard Note
- Irritant
- HS Code
- 2918999090
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Danger
- Hazard statements
-
H302Harmful if swallowed
H315Causes skin irritation
H318Causes serious eye damage
H335May cause respiratory irritation
- Precautionary statements
-
P280Wear protective gloves/protective clothing/eye protection/face protection.
P302+P352IF ON SKIN: wash with plenty of soap and water.
N-Bromosuccinimide Price
- Product number
- 739138
- Product name
- 3-(2-Iodophenyl)propionic acid
- Purity
- 97%
- Packaging
- 1g
- Price
- $49.7
- Updated
- 2025/07/31
- Product number
- 6771AC
- Product name
- 3-(2-Iodophenyl)propanoicacid
- Packaging
- 1g
- Price
- $110
- Updated
- 2021/12/16
- Product number
- 2721-H-06
- Product name
- 3-(2-Iodophenyl)propanoic acid
- Packaging
- 1g
- Price
- $141
- Updated
- 2021/12/16
- Product number
- 2721-H-06
- Product name
- 3-(2-Iodophenyl)propanoic acid
- Packaging
- 5G
- Price
- $394
- Updated
- 2021/12/16
- Product number
- HCH0020309
- Product name
- 3-(2-IODOPHENYL)PROPIONIC ACID
- Purity
- 95.00%
- Packaging
- 100MG
- Price
- $926.77
- Updated
- 2021/12/16
3-(2-IODOPHENYL)PROPIONIC ACID Chemical Properties,Usage,Production
Synthesis
111373-31-0
96606-95-0
Diethyl 2-(2-iodobenzyl)malonate (1.4 g, 3.6 mmol) was added to concentrated HCl (2.3 mL) and water (0.3 mL) and the mixture was refluxed overnight. The progress of the reaction was monitored by TLC and it was confirmed that the feedstock was still unreacted. Concentrated HCl (2 mL) was added additionally and refluxing continued overnight. Upon completion of the reaction, water (20 mL) and ether (50 mL) were added to the mixture for liquid-liquid separation. The organic phase was extracted with 5N ammonium hydroxide solution (30 mL). The basic aqueous phase was slowly added to ice-cold concentrated HCl and a white precipitate was precipitated. The precipitate was collected by filtration, washed with ice water and the solvent was removed in vacuum. 3-(2-iodophenyl)propionic acid was obtained in a yield of 0.32 g and 32%.
References
[1] Journal of Organic Chemistry, 1998, vol. 63, # 20, p. 6859 - 6866
[2] Patent: WO2004/96761, 2004, A1. Location in patent: Page 45
3-(2-IODOPHENYL)PROPIONIC ACID Preparation Products And Raw materials
Raw materials
Preparation Products
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