ChemicalBook > CAS DataBase List > 3-(2-IODOPHENYL)PROPIONIC ACID

3-(2-IODOPHENYL)PROPIONIC ACID

Product Name: 3-(2-IODOPHENYL)PROPIONIC ACID
CAS No.: 96606-95-0
Chemical Name: 3-(2-IODOPHENYL)PROPIONIC ACID
Synonyms: 3-(2-Iodphenyl)propionsSre;2-Iodobenzenepropanoic acid;Benzenepropanoic acid, 2-iodo-;3-(2-lodophenyl)propionic acid;3-(2-iodophenyl)propanoic acid;3-(2-IODOPHENYL)PROPIONIC ACID
CBNumber: CB8708247
Molecular Formula: C9H9IO2
Formula Weight: 276.07
MOL File: 96606-95-0.mol

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3-(2-IODOPHENYL)PROPIONIC ACID Property

Melting point:: 86-88°C
Boiling point:: 354℃
Density: 1.775
Flash point:: 168℃
storage temp.: Keep in dark place,Sealed in dry,Room Temperature
form: solid
Appearance: White to off-white Solid

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Safety

Hazard Codes: Xi,Xn
Risk Statements: 22-37/38-41-52/53
Safety Statements: 26-39-61
WGK Germany: 3
Hazard Note: Irritant
HS Code: 2918999090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Danger

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H318Causes serious eye damage

H335May cause respiratory irritation

Precautionary statements

P280Wear protective gloves/protective clothing/eye protection/face protection.

P302+P352IF ON SKIN: wash with plenty of soap and water.

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N-Bromosuccinimide Price

Sigma-Aldrich

Product number: 739138
Product name: 3-(2-Iodophenyl)propionic acid
Purity: 97%
Packaging: 1g
Price: $49.7
Updated: 2025/07/31

AK Scientific

Product number: 6771AC
Product name: 3-(2-Iodophenyl)propanoicacid
Packaging: 1g
Price: $110
Updated: 2021/12/16

SynQuest Laboratories

Product number: 2721-H-06
Product name: 3-(2-Iodophenyl)propanoic acid
Packaging: 1g
Price: $141
Updated: 2021/12/16

SynQuest Laboratories

Product number: 2721-H-06
Product name: 3-(2-Iodophenyl)propanoic acid
Packaging: 5G
Price: $394
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: HCH0020309
Product name: 3-(2-IODOPHENYL)PROPIONIC ACID
Purity: 95.00%
Packaging: 100MG
Price: $926.77
Updated: 2021/12/16

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3-(2-IODOPHENYL)PROPIONIC ACID Chemical Properties,Usage,Production

Synthesis

111373-31-0

96606-95-0

Diethyl 2-(2-iodobenzyl)malonate (1.4 g, 3.6 mmol) was added to concentrated HCl (2.3 mL) and water (0.3 mL) and the mixture was refluxed overnight. The progress of the reaction was monitored by TLC and it was confirmed that the feedstock was still unreacted. Concentrated HCl (2 mL) was added additionally and refluxing continued overnight. Upon completion of the reaction, water (20 mL) and ether (50 mL) were added to the mixture for liquid-liquid separation. The organic phase was extracted with 5N ammonium hydroxide solution (30 mL). The basic aqueous phase was slowly added to ice-cold concentrated HCl and a white precipitate was precipitated. The precipitate was collected by filtration, washed with ice water and the solvent was removed in vacuum. 3-(2-iodophenyl)propionic acid was obtained in a yield of 0.32 g and 32%.

References

[1] Journal of Organic Chemistry, 1998, vol. 63, # 20, p. 6859 - 6866
[2] Patent: WO2004/96761, 2004, A1. Location in patent: Page 45

3-(2-IODOPHENYL)PROPIONIC ACID Preparation Products And Raw materials

Raw materials

Preparation Products

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96606-95-0, 3-(2-IODOPHENYL)PROPIONIC ACIDRelated Search:

Iopanoic acid TYROPANOATE SODIUM ALPHA-ETHYL-3-HYDROXY-2,4,6-TRIIODOHYDROCINNAMIC ACID Ipodate Sodium 3-(3-AMINO-2,4,6-TRIIODOPHENYL)PROPIONIC ACID 3-(3-IODOPHENYL)PROPIONIC ACID 3-(4-IODOPHENYL)PROPIONIC ACID 2-[3-(butyrylamino)-2,4,6-triiodobenzyl]butyric acid ETHYL 3-(2-IODOPHENYL)-3-OXOPROPIONATE 3-[[(dimethylamino)methylene]amino]-3-(2,4,6-triiodophenyl)propionic acid 3-(2-IODOPHENYL)PROPIONIC ACID FMOC-PHE(3-I)-OH BOC-PHE(2-I)-OH IPODATE CALCIUM (200 MG) 2-Iodo-L-Phenylalanine 3-(4-hydroxy-3-iodophenyl)propionic acid Ioprocemic acid 3-(2-IODO-PHENYL)-3-OXO-PROPIONIC ACID METHYL ESTER

3-(2-IODOPHENYL)PROPIONIC ACID

3-(2-iodophenyl)propanoic acid

3-(2-lodophenyl)propionic acid

3-(2-Iodphenyl)propionsSre

2-Iodobenzenepropanoic acid

Benzenepropanoic acid, 2-iodo-

96606-95-0