3-(3-IODOPHENYL)PROPIONIC ACID
Uses- Product Name
- 3-(3-IODOPHENYL)PROPIONIC ACID
- CAS No.
- 68034-75-3
- Chemical Name
- 3-(3-IODOPHENYL)PROPIONIC ACID
- Synonyms
- 3-Iodobenzenepropanoic acid;3-(3-iodo)phenylacetic acid;3-(3-Iodophenyl)propanoicaci;3-(3-IODOPHENYL)PROPIONIC ACID;3-(3-iodophenyl)propanoic acid;Benzenepropanoic acid, 3-?iodo-;3-(3-IODOPHENYL)PROPIONIC ACID ISO 9001:2015 REACH
- CBNumber
- CB8279811
- Molecular Formula
- C9H9IO2
- Formula Weight
- 276.07
- MOL File
- 68034-75-3.mol
3-(3-IODOPHENYL)PROPIONIC ACID Property
- Boiling point:
- 357℃
- Density
- 1.775
- Flash point:
- 170℃
- storage temp.
- 2-8°C(protect from light)
- pka
- 4.59±0.10(Predicted)
- Appearance
- white solid
Safety
- Hazard Codes
- Xi
- HazardClass
- IRRITANT
- HS Code
- 2916399090
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- I718963
- Product name
- 3-(3-Iodophenyl)propionicAcid
- Packaging
- 500mg
- Price
- $110
- Updated
- 2021/12/16
- Product number
- 2721-H-05
- Product name
- 3-(3-Iodophenyl)propionic acid
- Packaging
- 250mg
- Price
- $43
- Updated
- 2021/12/16
- Product number
- 2721-H-05
- Product name
- 3-(3-Iodophenyl)propionic acid
- Packaging
- 1g
- Price
- $86
- Updated
- 2021/12/16
- Product number
- 007467
- Product name
- 3-(3-Iodophenyl)propionic acid
- Purity
- 98%
- Packaging
- 1g
- Price
- $105
- Updated
- 2021/12/16
- Product number
- HCH0020347
- Product name
- 3-(3-IODOPHENYL)PROPIONIC ACID
- Purity
- 95.00%
- Packaging
- 1G
- Price
- $180.6
- Updated
- 2021/12/16
3-(3-IODOPHENYL)PROPIONIC ACID Chemical Properties,Usage,Production
Uses
3-(3-iodo)phenylacetic acid can be used as a pharmaceutical synthesis intermediate and can be used in laboratory research and development processes.
Synthesis
A stirred solution of (3-aminophenyl)propionic acid (4.91 g, 29.7 mmol) in water (50 mL) and concentrated H2SO4 (4 mL) was stirred at -7 C. A solution of NaNO2 (2.4 g, 34.7 mmol) in a minimum amount of water was added to the (ice-salt bath), draining the nitrite solution below the surface of the solution and maintaining the temperature below 0C. After 10 min, the mixture was checked for the presence of excess NO2- using starch-KI indicator paper to ensure that diazotization was complete. Ether (50 mL) was added, followed by a slow addition of a solution of KI (15 g, 90 mmol) in a minimum amount of water to control the dramatic release of N2. After addition, the reactants were stirred and warmed to ambient temperature within 3 hours. The layers were separated and the aqueous layer was extracted with additional ether (2 x 50 mL). The combined ether layers were back-extracted with 5% (w/v) NaHSO3 (aqueous), brine (1 x 25 mL), dried over MgSO4, filtered and concentrated to give (3-iodo)phenylacetic acid in 8.0 g yield.
3-(3-IODOPHENYL)PROPIONIC ACID Preparation Products And Raw materials
Raw materials
Preparation Products
3-(3-IODOPHENYL)PROPIONIC ACID Suppliers
- Tel
- 18210857532; 18210857532
- Fax
- 86-10-82849933
- jkinfo@jkchemical.com
- Country
- China
- ProdList
- 96815
- Advantage
- 76
- Tel
- 0731-85526065 13308475853
- ivy@hnhbsj.com
- Country
- China
- ProdList
- 7245
- Advantage
- 62
- Tel
- 021-60343070
- Fax
- 021-35122006
- Country
- China
- ProdList
- 12740
- Advantage
- 55
- Tel
- 18860950986
- tangmanman@zenjipharma.com
- Country
- China
- ProdList
- 1733
- Advantage
- 55
- Tel
- +86-021-50935922
- Fax
- +86-021-33847795
- Country
- China
- ProdList
- 7865
- Advantage
- 55
- Tel
- +91-22-26355700
- Fax
- +91-22-26355701
- info@clearsynth.com
- Country
- India
- ProdList
- 9679
- Advantage
- 58
- Tel
- 0512-56316828 4008675858
- Fax
- +86-512-56316826
- sales@amateksci.com
- Country
- China
- ProdList
- 9858
- Advantage
- 55
- Tel
- 86-574-27787657
- Fax
- 86-574-27912196
- info@dearchem.com
- Country
- China
- ProdList
- 4613
- Advantage
- 58
- Tel
- 025-66023220 15250997978
- Fax
- 025-58362220
- 1511893459@qq.com
- Country
- China
- ProdList
- 4876
- Advantage
- 55
- Tel
- 571-89925085
- Fax
- 0086-571-89925065
- sales@amadischem.com
- Country
- China
- ProdList
- 131957
- Advantage
- 58