Carbamic acid, [(1S,2R)-2-aminocyclohexyl]-, 1,1-dimethylethyl ester (9CI)

Product Name: Carbamic acid, [(1S,2R)-2-aminocyclohexyl]-, 1,1-dimethylethyl ester (9CI)
CAS No.: 365996-30-1
Chemical Name: Carbamic acid, [(1S,2R)-2-aminocyclohexyl]-, 1,1-dimethylethyl ester (9CI)
Synonyms: RB4005;N-Boc-1(S),2(R)-diaMinocyclohexane;(1S,2R)-2-(Boc-amino)cyclohexylamine;(1S,2R)-N1-Boc-1,2-cyclohexanediamine;(1S,2R)-cis-N-Boc-1,2-cyclohexanediamine;(1S,2R)-2-Amino-1-(Boc-amino)cyclohexane;(1S,2R)-BOC-1,2-Diaminocyclohexane (cis);Cis-(1S, 2R)-1N-Boc-cyclohexane-1,2-diamine;tert-butyl (1S,2R)-2-aminocyclohexylcarbamate;(1S,2R)-1,2-Diaminocyclohexane, N1-BOC protected
CBNumber: CB91071394
Molecular Formula: C11H22N2O2
Formula Weight: 214.3
MOL File: 365996-30-1.mol

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Carbamic acid, [(1S,2R)-2-aminocyclohexyl]-, 1,1-dimethylethyl ester (9CI) Property

Boiling point:: 322.1±31.0 °C(Predicted)
Density: 1.02
storage temp.: under inert gas (nitrogen or Argon) at 2–8 °C
form: powder to lump to clear liquid
pka: 12.26±0.40(Predicted)
color: White or Colorless to Almost white or Almost colorless

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Safety

Hazard Codes: Xi
Risk Statements: 38-41
Safety Statements: 26-39
WGK Germany: 3
HazardClass: IRRITANT
HS Code: 2922498590

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Danger

Hazard statements

H315Causes skin irritation

H318Causes serious eye damage

H319Causes serious eye irritation

Precautionary statements

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TCI Chemical

Product number: B3483
Product name: (1S,2R)-N1-(tert-Butoxycarbonyl)-1,2-cyclohexanediamine
Purity: >98.0%(GC)(T)
Packaging: 1g
Price: $64
Updated: 2024/03/01

TCI Chemical

Product number: B3483
Product name: (1S,2R)-N1-(tert-Butoxycarbonyl)-1,2-cyclohexanediamine
Purity: >98.0%(GC)(T)
Packaging: 5g
Price: $319
Updated: 2024/03/01

Apolloscientific

Product number: OR15997
Product name: (1S,2R)-Cyclohexane-1,2-diamine,N1-BOCprotected
Packaging: 5g
Price: $375
Updated: 2021/12/16

SynQuest Laboratories

Product number: 4256-1-X5
Product name: (1S,2R)-Cyclohexane-1,2-diamine, N1-Boc protected
Packaging: 5G
Price: $413
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FB60249
Product name: tert-Butyl ((1S,2R)-2-aminocyclohexyl)carbamate
Packaging: 250mg
Price: $50
Updated: 2021/12/16

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Carbamic acid, [(1S,2R)-2-aminocyclohexyl]-, 1,1-dimethylethyl ester (9CI) Chemical Properties,Usage,Production

Synthesis

Triphenylphosphine (14.3 g) was added to a THF (190 ml) solution containing tert-butyl S,2S)-2-hydroxycyclohexyl) carbamate (10.0 g), followed by ice cooling. Diethyl azodicarboxylate (40% in toluene) (24.3 g) and DPPA (15.3 g) were added dropwise to the reaction solution, followed by stirring at room temperature for 1 hour. The reaction solution was left overnight. The solvent was distilled away under reduced pressure. Water was added, and then a 20% sodium hydroxide aqueous solution was added. Then, the organic layers were collected. Water (30 ml) was added to the obtained organic layers, followed by heating to 60 C. A THF (40 ml) solution containing triphenylphosphine (14.3 g) was added dropwise, followed by reflux for 2.5 hours. The solvent was distilled away under ordinary pressure. Toluene was added, and the pH was adjusted with 3M hydrochloric acid to pH=1 or less. Then, the resulting aqueous layers were collected, ethyl acetate was added, and the pH was adjusted with a 20% sodium hydroxide aqueous solution to pH 12. The organic layers were collected and dried over anhydrous sodium sulfate. Light yellow oily matter of tert-butyl ((1S,2R)-2-aminocyclohexyl)carbamate (Carbamic acid, [(1S,2R)-2-aminocyclohexyl]-, 1,1-dimethylethyl ester (9CI))was thus obtained.

Carbamic acid, [(1S,2R)-2-aminocyclohexyl]-, 1,1-dimethylethyl ester (9CI) Preparation Products And Raw materials

Raw materials

Preparation Products

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Carbamic acid, [(1S,2R)-2-aminocyclohexyl]-, 1,1-dimethylethyl ester (9CI) Suppliers

Americas 1 China 129 Europe 2 France 1 Germany 1 India 2 Japan 1 Switzerland 1 United Kingdom 4 United States 19 Global 161

Ark Pharm, Inc.

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View Lastest Price from Carbamic acid, [(1S,2R)-2-aminocyclohexyl]-, 1,1-dimethylethyl ester (9CI) manufacturers

Shanghai Yongzeng Technology Co.,Ltd

Product: tert-Butyl ((1S,2R)-2-aminocyclohexyl)carbamate 365996-30-1
Price: US $0.00/gm
Min. Order: 100gm
Purity: 99%min
Supply Ability: 100kgs
Release date: 2024-09-06

Henan Fengda Chemical Co., Ltd

Product: Carbamic acid, [(1S,2R)-2-aminocyclohexyl]-, 1,1-dimethylethyl ester (9CI) 365996-30-1
Price: US $34.00-1.20/kg
Min. Order: 1kg
Purity: 99%
Supply Ability: g-kg-tons, free sample is available
Release date: 2024-04-08

Career Henan Chemical Co

Product: Cis-(1S, 2R)-1N-Boc-cyclohexane-1,2-diamine 365996-30-1
Price: US $3.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: 100kg
Release date: 2019-08-07

365996-30-1, Carbamic acid, [(1S,2R)-2-aminocyclohexyl]-, 1,1-dimethylethyl ester (9CI)Related Search:

BENZYL CIS-4-AMINOCYCLOHEXYLCARBAMATE L-1-Phenylethylamine 1,2-Diaminocyclohexane N-Boc-1,2-Diaminocyclohexane 1-N-BOC-1,2-CIS-CYCLOHEXYLDIAMINE Carbamic acid, [(1S,2R)-2-aminocyclohexyl]-, 1,1-dimethylethyl ester (9CI)

(1S,2R)-1,2-Diaminocyclohexane, N1-BOC protected

tert-Butyl [(1S,2R)-2-aminocyclohex-1-yl]carbamic acid tert-butyl ester

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tert-Butyl [(1S,2R)-2-aminocyclohex-1-yl]carbamate, (1S,2R)-1,2-Diaminocyclohexane, N1-BOC protected

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Carbamic acid, [(1S,2R)-2-aminocyclohexyl]-, 1,1-dimethylethyl ester (9CI)

RB4005

((1S,2R)-2-Aminocyclohexyl)carbamic acid tert-butyl ester

tert-Butyl N-((2R,1S)-2-aminocyclohexyl)carbamate

CarbaMic acid, [(1S,2R)-2-aMinocyclohexyl]-, 1,1-diMethylethyl ester

N-[(1S,2S)-2-aminocyclohexyl]carbamic acid tert-butyl ester

CarbaMic acid,N-[(1S,2R)-2-aMinocyclohexyl]-, 1,1-diMethylethyl ester

(1S,2R)-2-(Boc-amino)cyclohexylamine

(1S,2R)-cis-N-Boc-1,2-cyclohexanediamine

(1S,2R)-N-tert-Butoxycarbonyl-1,2-cyclohexanediamine

[(1S,2R)-2-Aminocyclohex-1-yl]carbamic acid tert-butyl ester

(1S,2R)-N1-(tert-Butoxycarbonyl)-1,2-cyclohexanediamine

N-Boc-1(S),2(R)-diaMinocyclohexane

(1S,2R)-N1-Boc-1,2-cyclohexanediamine

(1S,2R)-N1-(tert-Butoxycarbonyl)-1,2-cyclohexanediamine &gt

(1S,2R)-2-Amino-1-(Boc-amino)cyclohexane

(1S,2R)-2-Amino-1-(tert-butoxycarbonylamino)cyclohexane

1,1-Dimethylethyl N-[(1S,2R)-2-aminocyclohexyl]carbamate

(1S,2R)-BOC-1,2-Diaminocyclohexane (cis)

365996-30-1

N-BOC