ChemicalBook > CAS DataBase List > 3-CHLORO-N-METHYLBENZYLAMINE

3-CHLORO-N-METHYLBENZYLAMINE

Product Name
3-CHLORO-N-METHYLBENZYLAMINE
CAS No.
39191-07-6
Chemical Name
3-CHLORO-N-METHYLBENZYLAMINE
Synonyms
3-Chloro-N<;3-CHLORO-N-METHYLBEN;M-CHLORO-N-METHYLBENZYLAMINE;3-CHLORO-N-METHYLBENZYLAMINE;N-Methyl-3-chlorobenzylamine;Benzylamine, m-chloro-N-methyl-;N-(3-CHLOROBENZYL)-N-METHYLAMINE;3-Chloro-N-methylbenzylamine ,97%;3-Chloro-N-methylbenzenemethanamine;3-Chloro-N-methylbenzylamine
CBNumber
CB9110797
Molecular Formula
C8H10ClN
Formula Weight
155.62
MOL File
39191-07-6.mol
More
Less

3-CHLORO-N-METHYLBENZYLAMINE Property

Boiling point:
97 °C/0.6 mmHg (lit.)
Density 
1.072 g/mL at 25 °C (lit.)
refractive index 
n20/D 1.5395(lit.)
Flash point:
115 °F
storage temp. 
Keep in dark place,Inert atmosphere,Room temperature
pka
9.34±0.10(Predicted)
Appearance
Colorless to light yellow Liquid
Sensitive 
Air Sensitive
NIST Chemistry Reference
N-methyl-m-chlorobenzylamine(39191-07-6)
EPA Substance Registry System
Benzenemethanamine, 3-chloro-N-methyl- (39191-07-6)
More
Less

Safety

Hazard Codes 
Xn
Risk Statements 
10-22-38-41
Safety Statements 
16-26-36/37/39
RIDADR 
UN 1993 3/PG 1
WGK Germany 
2
TSCA 
Yes
HazardClass 
3
PackingGroup 
Ⅲ
HS Code 
29214990
More
Less

Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Danger
Hazard statements

H226Flammable liquid and vapour

H302Harmful if swallowed

H315Causes skin irritation

H318Causes serious eye damage

Precautionary statements

P210Keep away from heat/sparks/open flames/hot surfaces. — No smoking.

P233Keep container tightly closed.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P301+P312IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.

P303+P361+P353IF ON SKIN (or hair): Remove/Take off Immediately all contaminated clothing. Rinse SKIN with water/shower.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

More
Less

N-Bromosuccinimide Price

Sigma-Aldrich
Product number
631116
Product name
3-Chloro-N-methylbenzylamine
Purity
97%
Packaging
1g
Price
$50.2
Updated
2023/06/20
Sigma-Aldrich
Product number
631116
Product name
3-Chloro-N-methylbenzylamine
Purity
97%
Packaging
5g
Price
$163
Updated
2023/06/20
AK Scientific
Product number
X5274
Product name
3-Chloro-N-methylbenzylamine
Packaging
5g
Price
$145
Updated
2021/12/16
American Custom Chemicals Corporation
Product number
HCH0026638
Product name
3-CHLORO-N-METHYLBENZYLAMINE
Purity
95.00%
Packaging
1G
Price
$648.83
Updated
2021/12/16
Biosynth Carbosynth
Product number
FC147164
Product name
3-Chloro-N-methylbenzylamine
Packaging
25g
Price
$669
Updated
2021/12/16
More
Less

3-CHLORO-N-METHYLBENZYLAMINE Chemical Properties,Usage,Production

Synthesis

104-83-6

74-89-5

39191-07-6

GENERAL STEPS: An ethanol solution of methylamine (33% w/v, 17 mL) was slowly added dropwise to 4-chlorobenzyl chloride (2.0 g, 12.42 mmol), followed by heating the reaction mixture to reflux overnight. Upon completion of the reaction, ethanol was removed by distillation under reduced pressure by rotary evaporator. The residue was diluted with deionized water (100 mL) and washed with ethyl acetate (150 mL × 2). The aqueous phase was adjusted to pH 8 with solid potassium carbonate and then extracted with ethyl acetate (100 mL × 2). All organic phases were combined, washed with deionized water (100 mL), dried over anhydrous sodium sulfate, and finally the target product, N-methyl-3-chlorobenzylamine (1.7 g), was obtained by concentration under reduced pressure. The product was characterized by 1H NMR (300 MHz, DMSO-d6): δ 2.22 (s, 3H), 3.32 (br s, 1H), 3.62 (s, 2H), 7.25-7.38 (m, 4H); ESI-MS (m/z) 156 (M + H).

References

[1] Patent: WO2017/199103, 2017, A1. Location in patent: Page/Page column 28

3-CHLORO-N-METHYLBENZYLAMINE Preparation Products And Raw materials

Raw materials

3-Chlorobenzaldehyde Methylamine Sodium borohydride Dichloromethane Methanol

Preparation Products

More
Less

3-CHLORO-N-METHYLBENZYLAMINE Suppliers

Belgium 1 China 75 Germany 1 India 4 Switzerland 1 United Kingdom 2 United States 14 Global 98
Tel
022-83946278 13820503911
Fax
022-83945176
Email
sales@creasyn.com
Country
China
ProdList
958
Advantage
68
Tel
18210857532; 18210857532
Fax
86-10-82849933
Email
jkinfo@jkchemical.com
Country
China
ProdList
96815
Advantage
76
Tel
400-6106006
Fax
021-67582001/03/05
Email
saleschina@alfa-asia.com
Country
China
ProdList
30123
Advantage
84
Tel
021-021-58432009 400-005-6266
Fax
021-58436166
Email
sales8178@energy-chemical.com
Country
China
ProdList
44801
Advantage
61
Tel
400-6009262 16621234537
Fax
021-64823266
Email
chenyj@titansci.com
Country
China
ProdList
14101
Advantage
59
Tel
021-54306202 13764082696
Email
info@hanhongsci.com
Country
China
ProdList
42934
Advantage
64
Tel
4009903999 13355009207
Fax
0539-6365991
Email
3007715519@qq.com
Country
China
ProdList
18729
Advantage
57
Tel
Fax
E-Mail Inquiry
Email
info@syntechem.com
Country
China
ProdList
12984
Advantage
57
Tel
024-31298370 15040047923
Fax
024-62665110
Email
yuanchengchem@163.com
Country
China
ProdList
252
Advantage
52
Tel
800-810-5118
Fax
+86-10-84193589
Email
cnchemical@thermofisher.com
Country
China
ProdList
17770
Advantage
75
More
Less

View Lastest Price from 3-CHLORO-N-METHYLBENZYLAMINE manufacturers

Career Henan Chemical Co
Product
3-CHLORO-N-METHYLBENZYLAMINE 39191-07-6
Price
US $1.00/KG
Min. Order
1KG
Purity
99%
Supply Ability
200kg
Release date
2020-01-09

39191-07-6, 3-CHLORO-N-METHYLBENZYLAMINERelated Search:

3,3',4',5-TETRACHLOROSALICYLANILIDE 6-Chloroquinazoline-2,4(1H,3H)-dione 7-CHLORO-3,4-DIHYDRO-1H-BENZO[E][1,4]DIAZEPINE-2,5-DIONE Tetrachlorophthalimide Tecloftalam 5-CHLOROSALICYLANILIDE (3,4-Dichlorobenzyl)methylamine 3-CHLORO-2-METHYLBENZYLAMINE 2,4-DICHLORO-6-METHYLBENZYLAMINE (S)-1-(4-Chlorophenyl)ethylamine 3-CHLORO-2-METHYLBENZYLAMINE 4-CHLORO-2-METHYLBENZYLAMINE (2,4-Dichlorobenzyl)methylamine O-CHLORO-N-METHYLBENZYLAMINE,2-CHLORO-N-METHYLBENZYLAMINE (2,3-Dichlorobenzyl)methylamine 5-CHLORO-2-METHYLBENZYLAMINE 2-CHLORO-6-METHYLBENZYLAMINE 4-Chloro-N-methylbenzylamine,P-CHLORO-N-METHYLBENZYLAMINE

  • 3-CHLORO-N-METHYLBENZYLAMINE
  • M-CHLORO-N-METHYLBENZYLAMINE
  • 3-Chloro-N-methylbenzenemethanamine
  • N-Methyl-3-chlorobenzylamine
  • N-(3-CHLOROBENZYL)-N-METHYLAMINE
  • 1-(3-Chlorophenyl)-N-MethylMethanaMine
  • 3-Chloro-N-methylbenzylamine ,97%
  • 3-CHLORO-N-METHYLBEN
  • N-(3-Chlorobenzyl)-N-methylamine, Tech.
  • Benzylamine, m-chloro-N-methyl-
  • Benzenemethanamine, 3-chloro-N-methyl-
  • N-(3-Chlorobenzyl)methylamine(N-(3-Chlorobenzyl)-N-methylamine)
  • 3-Chloro-<I>N<
  • 3-Chloro-<i>N</i>-methylbenzylamine
  • 39191-07-6
  • Amines
  • Building Blocks
  • C8
  • Nitrogen Compounds
  • Organic Building Blocks
  • Polyamines
  • Amines
  • C8
  • Nitrogen Compounds