ChemicalBook > CAS DataBase List > 2-Pyridinecarboxamide,5-fluoro-(9CI)

2-Pyridinecarboxamide,5-fluoro-(9CI)

Product Name: 2-Pyridinecarboxamide,5-fluoro-(9CI)
CAS No.: 499796-71-3
Chemical Name: 2-Pyridinecarboxamide,5-fluoro-(9CI)
Synonyms: 5-fluoropicolinaMide;5-Fluoro-2-pyridinecarboxaMide;2-PyridinecarboxaMide, 5-fluoro;2-Pyridinecarboxamide,5-fluoro-(9CI)
CBNumber: CB91271084
Molecular Formula: C6H5FN2O
Formula Weight: 140.12
MOL File: 499796-71-3.mol

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2-Pyridinecarboxamide,5-fluoro-(9CI) Property

Boiling point:: 272.9±25.0 °C(Predicted)
Density: 1.327±0.06 g/cm3(Predicted)
storage temp.: Inert atmosphere,Room Temperature
pka: 15.00±0.50(Predicted)
Appearance: White to off-white Solid

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Safety

HS Code: 2933399990

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P280Wear protective gloves/protective clothing/eye protection/face protection.

P301+P312IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P321Specific treatment (see … on this label).

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N-Bromosuccinimide Price

TRC

Product number: F621508
Product name: 5-Fluoropicolinamide
Packaging: 50mg
Price: $110
Updated: 2021/12/16

TRC

Product number: F621508
Product name: 5-Fluoropicolinamide
Packaging: 100mg
Price: $175
Updated: 2021/12/16

Apolloscientific

Product number: PC408426
Product name: 5-Fluoro-2-pyridinecarboxamide
Packaging: 1g
Price: $78
Updated: 2021/12/16

SynQuest Laboratories

Product number: 4H48-3-3E
Product name: 5-Fluoro-2-pyridinecarboxamide
Packaging: 1g
Price: $125
Updated: 2021/12/16

Apolloscientific

Product number: PC408426
Product name: 5-Fluoro-2-pyridinecarboxamide
Packaging: 5g
Price: $142
Updated: 2021/12/16

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2-Pyridinecarboxamide,5-fluoro-(9CI) Chemical Properties,Usage,Production

Synthesis

717871-83-5

499796-71-3

A solution of tetrahydrofuran (THF, 40 mL) of 5-fluoro-2-pyridinecarbonyl chloride (2.30 g, 14.4 mmol, 1.00 eq.) was slowly added dropwise to a stirred saturated ammonium hydroxide solution (40 mL) at 0 °C. The reaction mixture was stirred continuously at 10 °C for 30 min. Subsequently, the solvent was removed by distillation under reduced pressure. The residue was dissolved in dichloromethane (30 mL) and washed with saturated saline (2 x 30 mL). The organic phase was dried over anhydrous sodium sulfate (Na2SO4), filtered and concentrated under reduced pressure to give 1.82 g of 5-fluoro-2-pyridine carboxamide as a yellow solid in 71% yield. Mass spectrum (electrospray ionization, m/z): 140.9 ([M+H]+).

References

[1] Patent: WO2015/51479, 2015, A1. Location in patent: Page/Page column 65; 66
[2] Patent: WO2015/54038, 2015, A1. Location in patent: Page/Page column 57; 65; 66

2-Pyridinecarboxamide,5-fluoro-(9CI) Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from 2-Pyridinecarboxamide,5-fluoro-(9CI) manufacturers

Career Henan Chemical Co

Product: 2-Pyridinecarboxamide,5-fluoro-(9CI) 499796-71-3
Price: US $1.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: 1ton
Release date: 2019-07-11

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499796-71-3

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