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2-Pyridinecarboxamide,5-fluoro-(9CI)

Product Name
2-Pyridinecarboxamide,5-fluoro-(9CI)
CAS No.
499796-71-3
Chemical Name
2-Pyridinecarboxamide,5-fluoro-(9CI)
Synonyms
5-fluoropicolinaMide;5-Fluoro-2-pyridinecarboxaMide;2-PyridinecarboxaMide, 5-fluoro;2-Pyridinecarboxamide,5-fluoro-(9CI)
CBNumber
CB91271084
Molecular Formula
C6H5FN2O
Formula Weight
140.12
MOL File
499796-71-3.mol
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2-Pyridinecarboxamide,5-fluoro-(9CI) Property

Boiling point:
272.9±25.0 °C(Predicted)
Density 
1.327±0.06 g/cm3(Predicted)
storage temp. 
Inert atmosphere,Room Temperature
pka
15.00±0.50(Predicted)
Appearance
White to off-white Solid
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Safety

HS Code 
2933399990
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P280Wear protective gloves/protective clothing/eye protection/face protection.

P301+P312IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P321Specific treatment (see … on this label).

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N-Bromosuccinimide Price

TRC
Product number
F621508
Product name
5-Fluoropicolinamide
Packaging
50mg
Price
$110
Updated
2021/12/16
TRC
Product number
F621508
Product name
5-Fluoropicolinamide
Packaging
100mg
Price
$175
Updated
2021/12/16
Apolloscientific
Product number
PC408426
Product name
5-Fluoro-2-pyridinecarboxamide
Packaging
1g
Price
$78
Updated
2021/12/16
SynQuest Laboratories
Product number
4H48-3-3E
Product name
5-Fluoro-2-pyridinecarboxamide
Packaging
1g
Price
$125
Updated
2021/12/16
Apolloscientific
Product number
PC408426
Product name
5-Fluoro-2-pyridinecarboxamide
Packaging
5g
Price
$142
Updated
2021/12/16
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2-Pyridinecarboxamide,5-fluoro-(9CI) Chemical Properties,Usage,Production

Synthesis

717871-83-5

499796-71-3

A solution of tetrahydrofuran (THF, 40 mL) of 5-fluoro-2-pyridinecarbonyl chloride (2.30 g, 14.4 mmol, 1.00 eq.) was slowly added dropwise to a stirred saturated ammonium hydroxide solution (40 mL) at 0 °C. The reaction mixture was stirred continuously at 10 °C for 30 min. Subsequently, the solvent was removed by distillation under reduced pressure. The residue was dissolved in dichloromethane (30 mL) and washed with saturated saline (2 x 30 mL). The organic phase was dried over anhydrous sodium sulfate (Na2SO4), filtered and concentrated under reduced pressure to give 1.82 g of 5-fluoro-2-pyridine carboxamide as a yellow solid in 71% yield. Mass spectrum (electrospray ionization, m/z): 140.9 ([M+H]+).

References

[1] Patent: WO2015/51479, 2015, A1. Location in patent: Page/Page column 65; 66
[2] Patent: WO2015/54038, 2015, A1. Location in patent: Page/Page column 57; 65; 66

2-Pyridinecarboxamide,5-fluoro-(9CI) Preparation Products And Raw materials

Raw materials

Preparation Products

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2-Pyridinecarboxamide,5-fluoro-(9CI) Suppliers

CHEMSWORTH
Tel
--
Fax
--
Email
info@chemsworth.com
Country
India
ProdList
6700
Advantage
30
A.J Chemicals
Tel
--
Fax
--
Email
sales@ajchem.in
Country
India
ProdList
6100
Advantage
58
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View Lastest Price from 2-Pyridinecarboxamide,5-fluoro-(9CI) manufacturers

Career Henan Chemical Co
Product
2-Pyridinecarboxamide,5-fluoro-(9CI) 499796-71-3
Price
US $1.00/KG
Min. Order
1KG
Purity
99%
Supply Ability
1ton
Release date
2019-07-11

499796-71-3, 2-Pyridinecarboxamide,5-fluoro-(9CI)Related Search:


  • 2-Pyridinecarboxamide,5-fluoro-(9CI)
  • 5-Fluoro-2-pyridinecarboxaMide
  • 2-PyridinecarboxaMide, 5-fluoro
  • 5-fluoropicolinaMide
  • 499796-71-3
  • AMIDE
  • PYRIDINE