5-Bromo-3-methylpyridine-2-carboxylic acid methyl ester

Product Name: 5-Bromo-3-methylpyridine-2-carboxylic acid methyl ester
CAS No.: 213771-32-5
Chemical Name: 5-Bromo-3-methylpyridine-2-carboxylic acid methyl ester
Synonyms: Methyl 5-Bromo-3-methylpicolinate;METHYL-5-BROMO-3-METHYLPICOLINATE (TAX I;5-Bromo-3-methylpicolinic acid methyl ester;methyl 3-methyl-5-bromo-2-pyridinecarboxylate;Methyl 5-bromo-3-methyl-pyridine-2-carboxylate;5-BroMo-3-Methylpyridine-2-Carboxylic Acid Methyl;5-Bromo-3-methyl-2-pyridinecarboxylic acid methyl ester;2-Pyridinecarboxylic acid, 5-bromo-3-methyl-, methyl ester;5-bromo-3-methyl-2-Pyridinecarboxylic acid methyl ester (9CI ACI);2-Pyridinecarboxylic acid, 5-bromo-3-methyl-, methyl ester (9CI, ACI)
CBNumber: CB91563729
Molecular Formula: C8H8BrNO2
Formula Weight: 230.06
MOL File: 213771-32-5.mol

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5-Bromo-3-methylpyridine-2-carboxylic acid methyl ester Property

Boiling point:: 302.2±37.0 °C(Predicted)
Density: 1.503
storage temp.: Inert atmosphere,Room Temperature
pka: -0.17±0.10(Predicted)
Appearance: White to yellow Solid
InChI: InChI=1S/C8H8BrNO2/c1-5-3-6(9)4-10-7(5)8(11)12-2/h3-4H,1-2H3
InChIKey: KZPOANNAYCXMSH-UHFFFAOYSA-N
SMILES: C1(C(OC)=O)=NC=C(Br)C=C1C

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Safety

HS Code: 2933399990

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P271Use only outdoors or in a well-ventilated area.

P280Wear protective gloves/protective clothing/eye protection/face protection.

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N-Bromosuccinimide Price

TRC

Product number: M296493
Product name: Methyl5-Bromo-3-methylpicolinate
Packaging: 100mg
Price: $75
Updated: 2021/12/16

Frontier Specialty Chemicals

Product number: B13142
Product name: Methyl5-bromo-3-methylpicolinate
Purity: 95%
Packaging: 5g
Price: $80
Updated: 2021/12/16

SynQuest Laboratories

Product number: 4H23-9-X5
Product name: Methyl 5-bromo-3-methylpyridine-2-carboxylate
Purity: 98%
Packaging: 10g
Price: $424
Updated: 2021/12/16

Frontier Specialty Chemicals

Product number: B13142
Product name: Methyl5-bromo-3-methylpicolinate
Purity: 95%
Packaging: 1g
Price: $25
Updated: 2021/12/16

Matrix Scientific

Product number: 072770
Product name: 5-Bromo-3-methylpyridine-2-carboxylicacid methyl ester
Purity: 95+%
Packaging: 5g
Price: $639
Updated: 2021/12/16

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5-Bromo-3-methylpyridine-2-carboxylic acid methyl ester Chemical Properties,Usage,Production

Synthesis

886365-43-1

74-88-4

213771-32-5

Step C: Synthesis of methyl 5-bromo-3-methylpyridine-2-carboxylate 5-Bromo-3-methylpyridine-2-carboxylic acid (2.6 g, 12 mmol) was dissolved in N,N-dimethylformamide (20.0 mL) followed by addition of potassium carbonate (4.99 g, 36.1 mmol) and iodomethane (1.50 mL, 24.1 mmol). The reaction mixture was stirred at 80 °C for 40 min. After completion of the reaction, the mixture was extracted with ethyl acetate and water by partitioning. The organic layer was separated, washed with saturated brine, dried over anhydrous sodium sulfate, filtered and concentrated to give methyl 5-bromo-3-methylpyridine-2-carboxylate 2.3 g in yellow solid form in 83% yield.

References

[1] Patent: US2013/96144, 2013, A1. Location in patent: Paragraph 0392; 0393
[2] Patent: WO2008/100715, 2008, A1. Location in patent: Page/Page column 34

5-Bromo-3-methylpyridine-2-carboxylic acid methyl ester Preparation Products And Raw materials

Raw materials

Preparation Products

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5-Bromo-3-methylpyridine-2-carboxylic acid methyl ester Suppliers

China 123 Germany 1 India 4 United Kingdom 1 United States 12 Global 141

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View Lastest Price from 5-Bromo-3-methylpyridine-2-carboxylic acid methyl ester manufacturers

Dideu Industries Group Limited

Product: 5-Bromo-3-methylpyridine-2-carboxylic acid methyl ester 213771-32-5
Price: US $1.10/g
Min. Order: 1g
Purity: 99.00%
Supply Ability: 100 Tons Min
Release date: 2021-10-26

Career Henan Chemical Co

Product: 5-Bromo-3-methylpyridine-2-carboxylic acid methyl ester 213771-32-5
Price: US $1.00/kg
Min. Order: 1kg
Purity: 99%
Supply Ability: 100kGS
Release date: 2018-12-14

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METHYL-5-BROMO-3-METHYLPICOLINATE (TAX I

213771-32-5

Heterocycle-Pyridine series