ChemicalBook > CAS DataBase List > 3-Iodo-2-methoxypyridine

3-Iodo-2-methoxypyridine

Product Name
3-Iodo-2-methoxypyridine
CAS No.
112197-15-6
Chemical Name
3-Iodo-2-methoxypyridine
Synonyms
2-METHOXY-3-IODOPYRIDINE;3-IODO-2-METHOXYPYRIDINE;5-Iodo-2-Methoxypyridinne;Anhydrous lithium acetate;Pyridine,3-iodo-2-Methoxy-;3-Iodo-2-methoxypyridine>3-IODO-2-METHOXYPYRIDINE 99%;3-Iodo-2-methoxypyridine,96%;3-Iodo-2-Methoxypyridine, 97+%;2-Amino-3-bromo-6-nitropyridine
CBNumber
CB9175624
Molecular Formula
C6H6INO
Formula Weight
235.02
MOL File
112197-15-6.mol
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3-Iodo-2-methoxypyridine Property

Melting point:
66 °C(Solv: hexane (110-54-3))
Boiling point:
131-133 °C (43 mmHg)
Density 
1.831 g/mL at 25 °C
refractive index 
1.617-1.619
Flash point:
>110℃
storage temp. 
2-8°C
pka
1.38±0.10(Predicted)
form 
clear liquid
color 
Light yellow to Brown
Sensitive 
Light Sensitive
InChI
InChI=1S/C6H6INO/c1-9-6-5(7)3-2-4-8-6/h2-4H,1H3
InChIKey
BXCHJERCAUZLOE-UHFFFAOYSA-N
SMILES
C1(OC)=NC=CC=C1I
CAS DataBase Reference
112197-15-6(CAS DataBase Reference)
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Safety

Hazard Codes 
Xn,Xi
Risk Statements 
36/37/38-20/21/22-41-37/38-22-36/37/39
Safety Statements 
36/37/39-26-37
RIDADR 
UN 3334
WGK Germany 
3
HazardClass 
IRRITANT
HS Code 
29339900
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Danger
Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H318Causes serious eye damage

H335May cause respiratory irritation

Precautionary statements

P280Wear protective gloves/protective clothing/eye protection/face protection.

P302+P352IF ON SKIN: wash with plenty of soap and water.

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N-Bromosuccinimide Price

Sigma-Aldrich
Product number
692816
Product name
3-Iodo-2-methoxypyridine
Purity
97%
Packaging
1g
Price
$49.8
Updated
2023/06/20
TCI Chemical
Product number
I0924
Product name
3-Iodo-2-methoxypyridine
Purity
>98.0%(GC)(T)
Packaging
1g
Price
$39
Updated
2025/07/31
TCI Chemical
Product number
I0924
Product name
3-Iodo-2-methoxypyridine
Purity
>98.0%(GC)(T)
Packaging
5g
Price
$143
Updated
2025/07/31
TRC
Product number
I737070
Product name
3-Iodo-2-methoxypyridine
Packaging
10mg
Price
$45
Updated
2021/12/16
Matrix Scientific
Product number
016060
Product name
3-Iodo-2-methoxy-pyridine
Packaging
500mg
Price
$90
Updated
2021/12/16
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3-Iodo-2-methoxypyridine Chemical Properties,Usage,Production

Chemical Properties

Light yellow Cryst

Synthesis

1628-89-3

112197-15-6

The general procedure for the synthesis of 3-iodo-2-methoxypyridine using 2-methoxypyridine as starting material was as follows: firstly, [Li(TMP)Zn(tBu)2] was prepared in 0.4 mmol scale THF solution according to the literature method. To this solution, 2-methoxypyridine (0.042 mL, 0.4 mmol) was added and the reaction mixture was stirred at room temperature for 2 h to obtain a light orange solution. Subsequently, the solution was cooled to 0°C and the reaction was quenched with I2 (508 mg, dissolved in 1 mL THF) and stirring was continued for 1 hour. Upon completion of the reaction, 10% Na2S2O3 solution was added until the solution was bleached and the product was extracted with DCM (3 x 1 mL). The organic phases were combined, dried with MgSO4 and concentrated under reduced pressure to remove the solvent. The residue was purified by silica gel column chromatography using heptane:DCM (20:80→40:60) as eluent to afford 3-iodo-2-methoxypyridine (2a) as a colorless oil (87.1 mg, 92% yield).1H NMR (400 MHz, CDCl3) δ ppm 4.00 (s, 3H), 6.65 (dd, J = 7.61, 4.88 Hz, 1H), 8.03 (dd, J = 7.61, 1.76 Hz, 1H), 8.13 (dd, J = 4.88, 1.76 Hz, 1H). The data obtained are in agreement with literature reports.

References

[1] Tetrahedron, 2016, vol. 72, # 17, p. 2196 - 2205
[2] Tetrahedron Letters, 2011, vol. 52, # 36, p. 4590 - 4594
[3] Journal of the American Chemical Society, 2004, vol. 126, # 34, p. 10526 - 10527
[4] Journal of the American Chemical Society, 2007, vol. 129, # 7, p. 1921 - 1930
[5] Chemical Communications, 2014, vol. 50, # 85, p. 12859 - 12862

3-Iodo-2-methoxypyridine Preparation Products And Raw materials

Raw materials

Preparation Products

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3-Iodo-2-methoxypyridine Suppliers

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View Lastest Price from 3-Iodo-2-methoxypyridine manufacturers

Shaanxi Dideu New Materials Co. Ltd
Product
3-Iodo-2-methoxypyridine 112197-15-6
Price
US $0.00-0.00/KG
Min. Order
1KG
Purity
98.0%
Supply Ability
10000KGS
Release date
2025-06-03
Henan Fengda Chemical Co., Ltd
Product
3-Iodo-2-methoxypyridine 112197-15-6
Price
US $5.00-0.10/KG
Min. Order
1KG
Purity
98%
Supply Ability
g-kg-tons, free sample is available
Release date
2024-04-08
Hebei Zhanyao Biotechnology Co. Ltd
Product
3-Iodo-2-methoxypyridine 112197-15-6
Price
US $10.00/KG
Min. Order
1KG
Purity
99%
Supply Ability
20 Tons
Release date
2021-10-18

112197-15-6, 3-Iodo-2-methoxypyridineRelated Search:

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  • 3-IODO-2-METHOXYPYRIDINE
  • 3-Iodo-2-Methoxypyridine, 97+%
  • 2-METHOXY-3-IODOPYRIDINE
  • 3-Iodo-2-methoxypyridine,96%
  • 3-IODO-2-METHOXYPYRIDINE 99%
  • Pyridine,3-iodo-2-Methoxy-
  • 3-Iodo-2-methoxypyridine&gt
  • 2-Amino-3-bromo-6-nitropyridine
  • Anhydrous lithium acetate
  • 5-Iodo-2-Methoxypyridinne
  • 112197-15-6
  • C6H6INO
  • alkyl Iodine
  • Pyridines
  • Pyridine
  • Furans