ChemicalBook > CAS DataBase List > 5-Bromo-1,3-benzenediol

5-Bromo-1,3-benzenediol

Product Name
5-Bromo-1,3-benzenediol
CAS No.
106120-04-1
Chemical Name
5-Bromo-1,3-benzenediol
Synonyms
Phloroglucinol Impurity;5-BroMoresorcinol;5-BroMo-benzene-1,3-diol;5-Bromoresorcino;5-Bromoresorcinol>5-Bromo-1,3-benzenediol;1,3-Benzenediol, 5-bromo-;3,5-DihydroxybroMobenzene;Phloroglucinol Impurity 14;1-Bromo-3,5-dihydroxybenzene
CBNumber
CB92103634
Molecular Formula
C6H5BrO2
Formula Weight
189.01
MOL File
106120-04-1.mol
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5-Bromo-1,3-benzenediol Property

Melting point:
90.0 to 95.0 °C
Boiling point:
140°C/0.3mmHg(lit.)
Density 
1.844±0.06 g/cm3(Predicted)
storage temp. 
under inert gas (nitrogen or Argon) at 2-8°C
form 
powder to crystal
pka
8.49±0.10(Predicted)
color 
White to Almost white
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Safety

HS Code 
29089990
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

Precautionary statements

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P280Wear protective gloves/protective clothing/eye protection/face protection.

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N-Bromosuccinimide Price

TCI Chemical
Product number
B3731
Product name
5-Bromoresorcinol
Purity
>98.0%(GC)(T)
Packaging
1g
Price
$137
Updated
2025/07/31
TCI Chemical
Product number
B3731
Product name
5-Bromoresorcinol
Purity
>98.0%(GC)(T)
Packaging
5g
Price
$479
Updated
2025/07/31
TRC
Product number
D679043
Product name
3,5-Dihydroxybromobenzene
Packaging
500mg
Price
$155
Updated
2021/12/16
Biosynth Carbosynth
Product number
FD149366
Product name
3,5-Dihydroxybromobenzene
Packaging
1g
Price
$180
Updated
2021/12/16
AK Scientific
Product number
1394AA
Product name
5-Bromobenzene-1,3-diol
Packaging
5g
Price
$276
Updated
2021/12/16
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5-Bromo-1,3-benzenediol Chemical Properties,Usage,Production

Acquired resistance

5-Bromobenzene-1,3-diol is used in the synthesis of antimicrobial compounds, resorcinol derivatives and polycyclic compounds.

Synthesis

20469-65-2

106120-04-1

The general procedure for the synthesis of 5-bromo-1,3-benzenediol from 1-bromo-3,5-dimethoxybenzene was as follows: in Example 24, compound (35) (15.0 g, 69.0 mmol) was dissolved in dichloromethane (40 mL) and cooled to 0°C. A 1 M solution of boron tribromide in dichloromethane (140 mL, 140 mmol) was slowly added, keeping the reaction mixture in an ice bath. After dropwise addition, the reaction mixture was stirred at room temperature for 18 hours. Upon completion of the reaction, the reaction was quenched with methanol and the reaction mixture was subsequently concentrated. The residue was dissolved in ethyl acetate (500 mL) and washed with deionized water (300 mL). The organic layer was separated, dried over anhydrous sodium sulfate and concentrated to give the target product 5-bromo-1,3-benzenediol (45) (13.03 g, yield >99%) as an orange oil.

References

[1] Patent: US2011/136802, 2011, A1. Location in patent: Page/Page column 26-27
[2] Journal of the American Chemical Society, 2014, vol. 136, # 6, p. 2220 - 2223
[3] Patent: WO2014/60431, 2014, A1. Location in patent: Page/Page column 105
[4] Angewandte Chemie - International Edition, 2009, vol. 48, # 7, p. 1283 - 1286
[5] European Journal of Medicinal Chemistry, 2009, vol. 44, # 7, p. 2765 - 2775

5-Bromo-1,3-benzenediol Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from 5-Bromo-1,3-benzenediol manufacturers

Zhuozhou Wenxi import and Export Co., Ltd
Product
5-Bromo-1,3-benzenediol 106120-04-1
Price
US $15.00-10.00/KG
Min. Order
1KG
Purity
99%+ HPLC
Supply Ability
Monthly supply of 1 ton
Release date
2021-06-27
Career Henan Chemical Co
Product
5-Bromo-1,3-benzenediol 106120-04-1
Price
US $1.00/g
Min. Order
1g
Purity
99%
Supply Ability
10000KGS
Release date
2020-01-11

106120-04-1, 5-Bromo-1,3-benzenediolRelated Search:

5-BROMOISOPHTHALIC ACID 5-Bromo-1,3-phenylenediamine DIETHYL 5-BROMOISOPHTHALATE 5-BROMOISOPHTHALALDEHYDE DIMETHYL 5-BROMOISOPHTHALATE 2,4,6-Triformylphloroglucinol 4-(4-Nitrophenyl)azoresorcinol 2,4-Dichlorophenol Resorcinol

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