2-BROMO-4-METHYL-6-NITROANILINE

Product Name: 2-BROMO-4-METHYL-6-NITROANILINE
CAS No.: 827-24-7
Chemical Name: 2-BROMO-4-METHYL-6-NITROANILINE
Synonyms: 2-BROMO-4-METHYL-6-NITROANILINE;2-BROMO-4-METHYL-6-NITROBENZENAMINE;2-BROMO-4-METHYL-6-NITRO-PHENYLAMINE;Benzenamine, 2-bromo-4-methyl-6-nitro-;4-Amino-3-bromo-5-nitrotoluene, 2-Bromo-6-nitro-p-toluidine
CBNumber: CB9231193
Molecular Formula: C7H7BrN2O2
Formula Weight: 231.05
MOL File: 827-24-7.mol

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2-BROMO-4-METHYL-6-NITROANILINE Property

Melting point:: 64-66
Boiling point:: 329.1±37.0 °C(Predicted)
Density: 1.698±0.06 g/cm3(Predicted)
storage temp.: under inert gas (nitrogen or Argon) at 2–8 °C
pka: -1.74±0.25(Predicted)
Appearance: Light brown to orange Solid
InChI: InChI=1S/C7H7BrN2O2/c1-4-2-5(8)7(9)6(3-4)10(11)12/h2-3H,9H2,1H3
InChIKey: VFPKZASVVCBVMG-UHFFFAOYSA-N
SMILES: C1(N)=C([N+]([O-])=O)C=C(C)C=C1Br
CAS DataBase Reference: 827-24-7(CAS DataBase Reference)

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Safety

Hazard Codes: Xi
HazardClass: IRRITANT
HS Code: 2921420090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC

Product number: B677970
Product name: 2-Bromo-4-methyl-6-nitroaniline
Packaging: 50mg
Price: $60
Updated: 2021/12/16

SynQuest Laboratories

Product number: 4755-9-X0
Product name: 2-Bromo-4-methyl-6-nitroaniline
Packaging: 5G
Price: $52
Updated: 2021/12/16

AK Scientific

Product number: V7891
Product name: 2-Bromo-4-methyl-6-nitroaniline
Packaging: 25g
Price: $94
Updated: 2021/12/16

SynQuest Laboratories

Product number: 4755-9-X0
Product name: 2-Bromo-4-methyl-6-nitroaniline
Packaging: 25g
Price: $180
Updated: 2021/12/16

Matrix Scientific

Product number: 045534
Product name: 2-Bromo-4-methyl-6-nitroaniline
Purity: >95%
Packaging: 500mg
Price: $181
Updated: 2021/12/16

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2-BROMO-4-METHYL-6-NITROANILINE Chemical Properties,Usage,Production

Synthesis

89-62-3

827-24-7

4-Methyl-2-nitroaniline (131.2 g, 862 mmol) was used as a raw material and suspended in glacial acetic acid (1.25 L). Bromine (54 mL, 1.05 mol) was added slowly over 1 h at ambient temperature. After addition, the reaction mixture was continued to be stirred for 1 hour. Subsequently, the reaction solution was poured into water (7.5 L) and the suspension was stirred for 30 minutes. The solid product was collected by filtration, washed thoroughly with water (5 x 1 L) and dried to give 2-bromo-4-methyl-6-nitroaniline (187.2 g, 94%) as an orange solid. Its 1H NMR (CDCl3) data were as follows: δ 7.94 (1H, s), 7.56 (1H, s), 6.47 (2H, br s), 2.27 (3H, s).

References

[1] Organic Letters, 2006, vol. 8, # 22, p. 4989 - 4992
[2] Chemistry - A European Journal, 2015, vol. 21, # 52, p. 18915 - 18920
[3] Journal of Labelled Compounds and Radiopharmaceuticals, 1995, vol. 36, # 3, p. 281 - 288
[4] Journal of Antibiotics, 1994, vol. 47, # 12, p. 1456 - 1465
[5] Bioorganic and Medicinal Chemistry, 2011, vol. 19, # 20, p. 6026 - 6032

2-BROMO-4-METHYL-6-NITROANILINE Preparation Products And Raw materials

Raw materials

Preparation Products

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2-BROMO-4-METHYL-6-NITROANILINE Suppliers

Belgium 1 China 71 France 1 Germany 1 India 3 Sweden 1 United Kingdom 7 United States 12 Global 97

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3B Scientific Corporation

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View Lastest Price from 2-BROMO-4-METHYL-6-NITROANILINE manufacturers

Career Henan Chemical Co

Product: 2-BROMO-4-METHYL-6-NITROANILINE 827-24-7
Price: US $1.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: 100KG
Release date: 2020-01-09

827-24-7, 2-BROMO-4-METHYL-6-NITROANILINERelated Search:

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2-BROMO-4-METHYL-6-NITROBENZENAMINE

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