4-METHOXY-2-CHLOROANILINE
- Product Name
- 4-METHOXY-2-CHLOROANILINE
- CAS No.
- 29242-84-0
- Chemical Name
- 4-METHOXY-2-CHLOROANILINE
- Synonyms
- 5 graMs;2-Chloro-4-methoxyan;4-Amino-3-chloroanisole;4-METHOXY-2-CHLOROANILINE;2-chloro-4-methoxybenzenamine;2-Chloro-4-methoxyaniline 97+%;2-Chloro-4-Methoxy-phenylaMine;BenzenaMine,2-chloro-4-Methoxy-;4-AMino-3-chloroanisole[2-Chloro-4-Methoxyaniline]
- CBNumber
- CB92461170
- Molecular Formula
- C7H8ClNO
- Formula Weight
- 157.6
- MOL File
- 29242-84-0.mol
4-METHOXY-2-CHLOROANILINE Property
- Melting point:
- 114℃
- Boiling point:
- 249℃
- Density
- 1.234
- Flash point:
- 105℃
- storage temp.
- Keep in dark place,Inert atmosphere,Room temperature
- pka
- 3.26±0.10(Predicted)
- Appearance
- Brown to black Liquid
Safety
- HS Code
- 2921420090
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H312Harmful in contact with skin
H332Harmful if inhaled
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P264Wash hands thoroughly after handling.
P264Wash skin thouroughly after handling.
P270Do not eat, drink or smoke when using this product.
P271Use only outdoors or in a well-ventilated area.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P301+P312IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.
P302+P352IF ON SKIN: wash with plenty of soap and water.
P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.
P312Call a POISON CENTER or doctor/physician if you feel unwell.
P322Specific measures (see …on this label).
P330Rinse mouth.
P363Wash contaminated clothing before reuse.
P501Dispose of contents/container to..…
N-Bromosuccinimide Price
- Product number
- C349605
- Product name
- 2-Chloro-4-methoxyaniline
- Packaging
- 100mg
- Price
- $45
- Updated
- 2021/12/16
- Product number
- C349605
- Product name
- 2-Chloro-4-methoxyaniline
- Packaging
- 500mg
- Price
- $65
- Updated
- 2021/12/16
- Product number
- FC67022
- Product name
- 2-Chloro-4-methoxyaniline
- Packaging
- 5G
- Price
- $75
- Updated
- 2021/12/16
- Product number
- 119482
- Product name
- 2-Chloro-4-methoxyaniline
- Purity
- 95+%
- Packaging
- 1g
- Price
- $93
- Updated
- 2021/12/16
- Product number
- W5185
- Product name
- 2-Chloro-4-methoxyaniline
- Packaging
- 5g
- Price
- $103
- Updated
- 2021/12/16
4-METHOXY-2-CHLOROANILINE Chemical Properties,Usage,Production
Synthesis
28987-59-9
29242-84-0
The general procedure for the synthesis of 2-chloro-4-methoxyaniline from 2-chloro-4-methoxynitrobenzene was as follows: iron powder (5.10 g, 91.69 mmol) was added to a water (22 mL) and methanol (70 mL) containing 2-chloro-4-methoxy-1-nitrobenzene (1.72 g, 9.17 mmol) and ammonium chloride (1.96 g, 36.68 mmol) in a ) in a mixed suspension. The reaction mixture was heated to 50 °C and stirred at this temperature for 1 hour. After completion of the reaction, the mixture was cooled to room temperature, filtered, and the solid was washed with distilled water (2 x 15 mL). The filtrate was extracted with ethyl acetate (2 x 50 mL) and the combined organic layers were dried over anhydrous sodium sulfate, filtered and concentrated. The crude product was purified by silica gel column chromatography (eluent: 10-22% ethyl acetate/hexane) to afford 2-chloro-4-methoxyaniline (orange oil, 1.24 g, 86% yield).HPLC-MS (Method A): retention time 7.37 min; ESI-MS m/z: 158 ([M+H]+).
References
[1] Patent: WO2018/13774, 2018, A1. Location in patent: Page/Page column 455
[2] Patent: WO2018/1973, 2018, A1. Location in patent: Page/Page column 196
[3] Journal of the Chemical Society, 1927, p. 2218
[4] Journal of the Chemical Society, 1928, p. 331
[5] Journal of the Chemical Society, 1927, p. 2218
4-METHOXY-2-CHLOROANILINE Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 4-METHOXY-2-CHLOROANILINE manufacturers
- Product
- 4-METHOXY-2-CHLOROANILINE 29242-84-0
- Price
- US $1.00/KG
- Min. Order
- 1KG
- Purity
- 99%
- Supply Ability
- 100kg
- Release date
- 2019-07-11