ChemicalBook > CAS DataBase List > 5-Amino-2-bromo-6-iodopyridine

5-Amino-2-bromo-6-iodopyridine

Product Name
5-Amino-2-bromo-6-iodopyridine
CAS No.
915006-52-9
Chemical Name
5-Amino-2-bromo-6-iodopyridine
Synonyms
6-bromo-2-iodopyridin-3-amine;3-AMino-6-broMo-2-iodopyridine;5-Amino-2-bromo-6-iodopyridine;3-PyridinaMine, 6-broMo-2-iodo-;6-BroMo-2-iodo-pyridin-3-ylaMine;5-Amino-2-bromo-6-iodopyridine ISO 9001：2015 REACH
CBNumber
CB92484995
Molecular Formula
C5H4BrIN2
Formula Weight
298.91
MOL File
915006-52-9.mol
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5-Amino-2-bromo-6-iodopyridine Property

Boiling point:
362.5±42.0 °C(Predicted)
Density 
2.426±0.06 g/cm3(Predicted)
storage temp. 
under inert gas (nitrogen or Argon) at 2–8 °C
pka
-0.19±0.10(Predicted)
Appearance
Brown to reddish brown Solid
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Hazard and Precautionary Statements (GHS)

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N-Bromosuccinimide Price

Biosynth Carbosynth
Product number
FA152973
Product name
5-Amino-2-bromo-6-iodopyridine
Packaging
2mg
Price
$59
Updated
2021/12/16
Biosynth Carbosynth
Product number
FA152973
Product name
5-Amino-2-bromo-6-iodopyridine
Packaging
5mg
Price
$117
Updated
2021/12/16
Biosynth Carbosynth
Product number
FA152973
Product name
5-Amino-2-bromo-6-iodopyridine
Packaging
10mg
Price
$203
Updated
2021/12/16
AK Scientific
Product number
5369AC
Product name
6-Bromo-2-iodopyridin-3-amine
Packaging
1g
Price
$384
Updated
2021/12/16
Biosynth Carbosynth
Product number
FA152973
Product name
5-Amino-2-bromo-6-iodopyridine
Packaging
25mg
Price
$405
Updated
2021/12/16
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5-Amino-2-bromo-6-iodopyridine Chemical Properties,Usage,Production

Synthesis

13534-97-9

915006-52-9

General procedure for the synthesis of 5-amino-2-bromo-6-iodopyridine from 5-amino-2-bromopyridine: To a stirring solution of 6-bromo-pyridin-3-ylamine (10.2 g, 0.0580 mol) and Ag2SO4 (18.1 g, 0.0580 mol) in ethanol (150 mL) was added iodine (7.59 g, 0.0580 mol). The reaction mixture was stirred overnight. Subsequently, hexane (200 mL) was added and the mixture was filtered through diatomaceous earth. The solvent was removed under reduced pressure and the residue was dissolved in chloroform (200 mL), washed sequentially with saturated aqueous sodium thiosulfate (100 mL) and water (1 x 100 mL), and dried over anhydrous sodium sulfate. The solvent was concentrated under reduced pressure and the residue was dissolved in hot ethyl acetate (100 mL), filtered and treated with hexane (100 mL). Filtration afforded a white crystalline product 5-amino-2-bromo-6-iodopyridine 11.2 g in 65% yield. 1H-NMR (CDCl3; 400 MHz): δ 7.10 (d, 1H, J=8.2 Hz), 6.74 (d, 1H, J=8.2 Hz), 4.06 (br s, 2H).

References

[1] Patent: US2007/249649, 2007, A1. Location in patent: Page/Page column 74
[2] Patent: US2007/249608, 2007, A1. Location in patent: Page/Page column 41
[3] Patent: WO2007/123516, 2007, A1. Location in patent: Page/Page column 109-110
[4] Patent: WO2009/149820, 2009, A1. Location in patent: Page/Page column 82-83
[5] Journal of Medicinal Chemistry, 2013, vol. 56, # 21, p. 8860 - 8871

5-Amino-2-bromo-6-iodopyridine Preparation Products And Raw materials

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Preparation Products

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View Lastest Price from 5-Amino-2-bromo-6-iodopyridine manufacturers

Dideu Industries Group Limited
Product
5-Amino-2-bromo-6-iodopyridine 915006-52-9
Price
US $1.10/g
Min. Order
1g
Purity
99.00%
Supply Ability
100 Tons min
Release date
2021-09-01

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