ChemicalBook > CAS DataBase List > Methyl 5-aMino-2-nitro benzoate

Methyl 5-aMino-2-nitro benzoate

Product Name
Methyl 5-aMino-2-nitro benzoate
CAS No.
35998-96-0
Chemical Name
Methyl 5-aMino-2-nitro benzoate
Synonyms
Methyl 5-aMino-2-nitro benzoate;5-aMino-2-nitro-benzoic acid Methyl ester;Benzoic acid, 5-amino-2-nitro-, methyl ester
CBNumber
CB92570948
Molecular Formula
C8H8N2O4
Formula Weight
196.16
MOL File
35998-96-0.mol
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Methyl 5-aMino-2-nitro benzoate Property

Melting point:
98-100 °C
Boiling point:
394.5±22.0 °C(Predicted)
Density 
1.386±0.06 g/cm3(Predicted)
storage temp. 
Keep in dark place,Inert atmosphere,Room temperature
pka
-0.15±0.10(Predicted)
Appearance
Light yellow to yellow Solid
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H302Harmful if swallowed

Precautionary statements

P280Wear protective gloves/protective clothing/eye protection/face protection.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

AK Scientific
Product number
4298AJ
Product name
Methyl5-amino-2-nitrobenzoate
Packaging
1g
Price
$208
Updated
2021/12/16
Matrix Scientific
Product number
132408
Product name
Methyl5-amino-2-nitrobenzoate
Purity
97%
Packaging
1g
Price
$352
Updated
2021/12/16
AK Scientific
Product number
4298AJ
Product name
Methyl5-amino-2-nitrobenzoate
Packaging
10g
Price
$624
Updated
2021/12/16
Matrix Scientific
Product number
132408
Product name
Methyl5-amino-2-nitrobenzoate
Purity
97%
Packaging
5g
Price
$1239
Updated
2021/12/16
Ambeed
Product number
A435238
Product name
Methyl5-amino-2-nitrobenzoate
Purity
97%
Packaging
250mg
Price
$20
Updated
2021/12/16
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Methyl 5-aMino-2-nitro benzoate Chemical Properties,Usage,Production

Chemical Properties

Reddish brown solid

Synthesis

67-56-1

13280-60-9

35998-96-0

5-Amino-2-nitrobenzoic acid (Compound A) (910 mg) was dissolved in methanol (50 mL). Thionyl chloride (0.74 mL) was added slowly and dropwise to the above solution under cooling in an ice bath. Subsequently, the reaction mixture was heated to reflux for 12 hours. Upon completion of the reaction, the reaction solution was cooled to room temperature and concentrated under reduced pressure. The residue was purified by column chromatography using a chloroform-methanol solvent mixture as eluent to finally obtain methyl 5-amino-2-nitrobenzoate (410 mg, 42% yield).

References

[1] Tetrahedron Letters, 2005, vol. 46, # 44, p. 7477 - 7481
[2] Patent: EP1614676, 2006, A1. Location in patent: Page/Page column 179
[3] European Journal of Medicinal Chemistry, 2012, vol. 57, p. 468 - 482

Methyl 5-aMino-2-nitro benzoate Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from Methyl 5-aMino-2-nitro benzoate manufacturers

Career Henan Chemical Co
Product
Methyl 5-aMino-2-nitro benzoate 35998-96-0
Price
US $1.00/kg
Min. Order
1kg
Purity
95%-99%
Supply Ability
1000kg
Release date
2018-12-25

35998-96-0, Methyl 5-aMino-2-nitro benzoateRelated Search:

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  • 35998-96-0