4-Methyl-3-(hydroxyMethyl)Morpholine
- Product Name
- 4-Methyl-3-(hydroxyMethyl)Morpholine
- CAS No.
- 1159598-86-3
- Chemical Name
- 4-Methyl-3-(hydroxyMethyl)Morpholine
- Synonyms
- 4-Methyl-3-morpholinemethanol;3-Morpholinemethanol, 4-methyl-;(4-Methylmorpholin-3-yl)methanol;4-Methyl-3-(hydroxyMethyl)Morpholine
- CBNumber
- CB92629985
- Molecular Formula
- C6H13NO2
- Formula Weight
- 131.17
- MOL File
- 1159598-86-3.mol
4-Methyl-3-(hydroxyMethyl)Morpholine Property
- Boiling point:
- 201.1±15.0 °C(Predicted)
- Density
- 1.031±0.06 g/cm3(Predicted)
- storage temp.
- 2-8°C
- pka
- 14.85±0.10(Predicted)
- Appearance
- Colorless to light yellow Liquid
Safety
- HS Code
- 2934999090
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- B585958
- Product name
- 4-Methyl-3-(hydroxymethyl)morpholine
- Packaging
- 100mg
- Price
- $240
- Updated
- 2021/12/16
- Product number
- CS-0061777
- Product name
- (4-Methylmorpholin-3-yl)methanol
- Packaging
- 100mg
- Price
- $93
- Updated
- 2021/12/16
- Product number
- CS-0061777
- Product name
- (4-Methylmorpholin-3-yl)methanol
- Packaging
- 250mg
- Price
- $155
- Updated
- 2021/12/16
- Product number
- CS-0061777
- Product name
- (4-Methylmorpholin-3-yl)methanol
- Packaging
- 1g
- Price
- $309
- Updated
- 2021/12/16
- Product number
- OR55495
- Product name
- 4-Methyl-3-(hydroxymethyl)morpholine
- Purity
- 95%
- Packaging
- 1g
- Price
- $432
- Updated
- 2021/12/16
4-Methyl-3-(hydroxyMethyl)Morpholine Chemical Properties,Usage,Production
Synthesis
50-00-0
106910-83-2
1159598-86-3
Step 2: Preparation of (4-methylmorpholin-3-yl)methanol To a solution of morpholin-3-ylmethanol (0.540 g, 4.6 mmol) in methanol (20 mL) was added formaldehyde (1.86 g, 23 mmol, 37% aqueous solution) and palladium/carbon catalyst (0.200 g). The reaction mixture was stirred overnight at room temperature under hydrogen atmosphere (1.0 atm). Upon completion of the reaction, the catalyst was removed by filtration through a diatomaceous earth pad and the filtrate was concentrated under reduced pressure. The residue was purified by silica gel column chromatography (eluent ratio: methanol:dichloromethane=1:15) to afford (4-methylmorpholin-3-yl)methanol (0.130 g, 22% yield) as a yellow oil.
References
[1] Patent: US2016/168090, 2016, A1. Location in patent: Paragraph 0927-0928
4-Methyl-3-(hydroxyMethyl)Morpholine Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 4-Methyl-3-(hydroxyMethyl)Morpholine manufacturers
- Product
- 4-Methyl-3-(hydroxyMethyl)Morpholine 1159598-86-3
- Price
- US $0.00/g
- Min. Order
- 1g
- Purity
- 95%min
- Supply Ability
- 20kg/month
- Release date
- 2019-11-19
- Product
- 4-Methyl-3-(hydroxyMethyl)Morpholine 1159598-86-3
- Price
- US $0.00/g
- Min. Order
- 1g
- Purity
- 95%min
- Supply Ability
- 20kg/month
- Release date
- 2019-11-19