description Chemical properties Application and Synthesis Improvement of UV - 9 Production Process
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UV absorber UV-9

description Chemical properties Application and Synthesis Improvement of UV - 9 Production Process
Product Name
UV absorber UV-9
CAS No.
131-57-7
Chemical Name
UV absorber UV-9
Synonyms
BENZOPHENONE-3;HMB;BP-3;2-HYDROXY-4-METHOXYBENZOPHENONE;Uv 9;HMBP;component of Presun 29;MOD;uf3;Oxybenzon
CBNumber
CB9276251
Molecular Formula
C14H12O3
Formula Weight
228.24
MOL File
131-57-7.mol
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UV absorber UV-9 Property

Melting point:
62-64 °C(lit.)
Boiling point:
150-160 °C5 mm Hg(lit.)
Density 
1,3 g/cm3
vapor pressure 
0.001Pa at 25℃
refractive index 
1.5805 (estimate)
Flash point:
216°C
storage temp. 
2-8°C
solubility 
95% ethanol: soluble50mg/mL, clear, colorless
form 
Crystalline Powder
pka
7.56±0.35(Predicted)
color 
White to light yellow
Odor
ylsh. cryst., rose-like odor
Water Solubility 
<0.1 g/100 mL at 20 ºC
Merck 
14,6954
BRN 
1913145
InChIKey
DXGLGDHPHMLXJC-UHFFFAOYSA-N
LogP
3.45 at 40℃
CAS DataBase Reference
131-57-7(CAS DataBase Reference)
NIST Chemistry Reference
Oxybenzone(131-57-7)
EPA Substance Registry System
2-Hydroxy-4-methoxybenzophenone (131-57-7)
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Safety

Hazard Codes 
Xi
Risk Statements 
36/37/38
Safety Statements 
26-36-37
RIDADR 
UN 3077 9/PG III
WGK Germany 
2
RTECS 
DJ1575000
TSCA 
Yes
HazardClass 
9
PackingGroup 
III
HS Code 
29145000
Hazardous Substances Data
131-57-7(Hazardous Substances Data)
Toxicity
LD50 orally in rats: >12.8 g/kg (Lewerenz)
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H410Very toxic to aquatic life with long lasting effects

Precautionary statements

P273Avoid release to the environment.

P391Collect spillage. Hazardous to the aquatic environment

P501Dispose of contents/container to..…

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N-Bromosuccinimide Price

Sigma-Aldrich
Product number
1485001
Product name
Oxybenzone
Purity
United States Pharmacopeia (USP) Reference Standard
Packaging
150mg
Price
$436
Updated
2024/03/01
TCI Chemical
Product number
H0266
Product name
2-Hydroxy-4-methoxybenzophenone
Purity
>99.0%(GC)
Packaging
25g
Price
$24
Updated
2024/03/01
TCI Chemical
Product number
H0266
Product name
2-Hydroxy-4-methoxybenzophenone
Purity
>99.0%(GC)
Packaging
500g
Price
$114
Updated
2024/03/01
Alfa Aesar
Product number
A17662
Product name
2-Hydroxy-4-methoxybenzophenone, 98+%
Packaging
50g
Price
$22.65
Updated
2024/03/01
Alfa Aesar
Product number
A17662
Product name
2-Hydroxy-4-methoxybenzophenone, 98+%
Packaging
250g
Price
$87.4
Updated
2024/03/01
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UV absorber UV-9 Chemical Properties,Usage,Production

description

Oxybenzone is an organic compound used in sunscreens. It is a derivative of benzophenone. It forms colorless crystals that are readily soluble in most organic solvents. It is used as an ingredient in sunscreen and other cosmetics because it absorbs UV-A ultraviolet rays.
Oxybenzone absorbs UVB and UVA II rays, resulting in a photochemical excitation and absorption of energy. Upon return to ground state, the absorbed energy results in emission of longer wavelength radiation and decreased skin penetration of radiation which reduces the risk of DNA damage.

Chemical properties

light yellow crystalline powder, soluble in ethanol, acetone and other organic solvents, insoluble in water.

Application and Synthesis

UV-9 is a light yellow or white crystalline powder, also known as sunscreen 2, BP-3, suitable for polyvinyl chloride, polyvinylidene chloride, polymethyl methacrylate , unsaturated polyester, ABS resin and cellulose resin and other plastics, the maximum absorption wavelength range of 280-340 nm, the general amount of 0.1-1.5%, good thermal stability, does not decompose at 200 ℃. This product hardly absorb visible light, it applies to light-colored transparent products. This product can also be used for paints and synthetic rubber. For the broad-spectrum UV absorbers, with high absorption rate, non-toxic, non-teratogenic effect, light, thermal stability. UV-9 can absorb UV-A and UV-B together, is the US FDA approved Class I sunscreen and being used with a higher frequency in the US and European countries. UV-9 is widely used in sunscreen cream, cream, honey, lotion, oil and other sunscreen cosmetics, but also as a product from the photosensitive and discoloration of the anti-discoloration agent. In addition, it is usually used for PVC and unsaturated polyester and many other fields, because UV-9 has good compatibility with many kinds of plastics and resins.

Improvement of UV - 9 Production Process

Using mixed acid as catalyst, trichloromethylbenzene and resorcinol were condensed into intermediate 2,4-dihydroxydiphenyl ketone in aqueous phase, and then the catalyst was treated with phase transfer catalyst, etherification of the target product UV-9.

Chemical Properties

white to light yellow crystalline powder

Uses

ultraviolet screen

Uses

Oxybenzone is an organic compound used in sunscreens. Oxybenzone is used as an ingredient in sunscreen and other cosmetics because it absorbs UVB and short-wave UVA (ultraviolet) rays. Oxybenzone was one of the first compounds incorporated into sunscreen formulations to offer enhanced UVA protection because its absorption spectrum extends to less than 350 nm.

Uses

Sunscreen. UV stabilizer

Uses

Ultraviolet light absorber and stabilizer, especially in plastics and paints.

Uses

benzophenone-3 (oxybenzone) is an oil-soluble uV absorber and filter with absorption rates within the uVA and uVB peak ranges. It has an approved usage level of up to 6 percent in the united States and 10 percent in the european union. Benzophenone-3 enhances SPF and is popular among sunscreen formulators given a concern over potential safety problems associated with more traditional sunscreen chemicals. However, some reports associate it with causing photocontact allergy. It is considered a non-comedogenic raw material.

Uses

oxybenzone (benzophenone-3) is the drug name for an FDAapproved uV filter and absorber.

Preparation

Preparation by partial methylation of 2,4- dihydroxy-benzophenone,
? with methyl iodide in the presence of sodium hydroxide;
? with a methyl halide;
? with dimethyl sulfate in the presence of sodium hydroxide or alkaline solution.

Definition

ChEBI: A hydroxybenzophenone that is benzophenone which is substituted at the 2- and 4-positions of one of the benzene rings by hydroxy and methoxy groups respectively.

brand name

Uvinul M40 (BASF).

Synthesis Reference(s)

Tetrahedron, 42, p. 885, 1986 DOI: 10.1016/S0040-4020(01)87495-0

General Description

White to off-white or light yellow powder.

Air & Water Reactions

Insoluble in water.

Fire Hazard

Flash point data for Oxybenzone are not available; however, Oxybenzone is probably combustible.

Flammability and Explosibility

Non flammable

Contact allergens

BZP-3 is used as a direct sunscreen agent and in antiaging creams. Allergic reactions have been reported. Cross-reactivity is expected in an average of one in four patients photoallergic to ketoprofen.

Safety Profile

Poison by intraperitoneal route. Mddly toxic by ingestion. Experimental reproductive effects. Mutation data reported. When heated to decomposition it emits acrid smoke and irritating fumes.

UV absorber UV-9 Preparation Products And Raw materials

Raw materials

Preparation Products

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UV absorber UV-9 Suppliers

Shanghai Juankai Biopharma Co., Ltd
Tel
15052267297 15052267297
Email
630819472@qq.com
Country
China
ProdList
57
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58
Jobachem Suzhou Co., Ltd
Tel
0512-62927368; 18136961057
Email
min.li@jobachem.com
Country
China
ProdList
51
Advantage
58
Lianyungang Shenghe Biotechnology Co., Ltd.
Tel
13585296001 13585296001
Email
haizaofu@163.com
Country
China
ProdList
42
Advantage
58
Hubei Hengluyuan Technology co.ltd
Tel
027-88188016 18717196322
Email
1764683941@qq.com
Country
China
ProdList
5749
Advantage
58
Hubei Yiling Biotechnology Co., Ltd
Tel
15102793023 17771822910
Email
2056564811@qq.com
Country
China
ProdList
2064
Advantage
58
Tianjin Zhongxin Chemtech Co., Ltd.
Tel
022-66880623
Fax
86(0)22-66880086
Email
sales@tjzxchem.com
Country
China
ProdList
613
Advantage
60
J & K SCIENTIFIC LTD.
Tel
010-82848833 400-666-7788
Fax
86-10-82849933
Email
jkinfo@jkchemical.com
Country
China
ProdList
96815
Advantage
76
Changzhou Sunchem Pharmaceutical Chemical Material Co.,Ltd.
Tel
0519-85195575 15861192208
Fax
85195585
Email
850305@sunkechem.com
Country
China
ProdList
75
Advantage
69
Meryer (Shanghai) Chemical Technology Co., Ltd.
Tel
021-61259108 18621169109
Fax
86-21-61259102
Email
market03@meryer.com
Country
China
ProdList
40228
Advantage
62
Alfa Aesar
Tel
400-6106006
Fax
021-67582001/03/05
Email
saleschina@alfa-asia.com
Country
China
ProdList
30123
Advantage
84
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View Lastest Price from UV absorber UV-9 manufacturers

Watson Biotechnology Co.,Ltd
Product
Oxybenzone/Benzophenone-3 131-57-7
Price
US $0.00-0.00/kg
Min. Order
1kg
Purity
99%
Supply Ability
20MT
Release date
2024-07-31
Hebei Zhuanglai Chemical Trading Co.,Ltd
Product
Oxybenzone 131-57-7
Price
US $10.00/kg
Min. Order
1kg
Purity
99%
Supply Ability
20ton
Release date
2024-05-13
WUHAN FORTUNA CHEMICAL CO., LTD
Product
2-Hydroxy-4-Methoxy Benzophenone 131-57-7
Price
US $0.00-0.00/Kg/Drum
Min. Order
1KG
Purity
97.0-103.0%,USP
Supply Ability
5ton/month
Release date
2021-05-28

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