FMOC-ASN(TRT)-OPFP
- Product Name
- FMOC-ASN(TRT)-OPFP
- CAS No.
- 132388-64-8
- Chemical Name
- FMOC-ASN(TRT)-OPFP
- Synonyms
- CAS:132388-64-8;FMOC-ASN(TRT)-OPFP;FMOC-L-ASN(TRT)-OPFP;pentafluorophenyl ester;FMOC-ASPARAGINE(TRT)-OPFP;FMOC-ASN(TRT)-OPFP USP/EP/BP;(9H-Fluoren-9-yl)MethOxy]Carbonyl Asn(Trt)-Opfp;N2-Fmoc-N4-trityl-L-asparagine pentafluorophenyl ester;FMOC-N-BETA-TRITYL-L-ASPARAGINE PENTAFLUOROPHENYL ESTER;FMOC-N-GAMMA-TRITYL-L-ASPARAGINE PENTAFLUOROPHENYL ESTER
- CBNumber
- CB9278053
- Molecular Formula
- C44H31F5N2O5
- Formula Weight
- 762.72
- MOL File
- 132388-64-8.mol
FMOC-ASN(TRT)-OPFP Property
- alpha
- -7 º (C=1 IN DIOXANE)
- Boiling point:
- 888.2±65.0 °C(Predicted)
- Density
- 1.358±0.06 g/cm3(Predicted)
- storage temp.
- Store at -15°C to -25°C.
- solubility
- Soluble in water or 1% acetic acid
- form
- Powder
- pka
- 9.80±0.46(Predicted)
- Major Application
- peptide synthesis
- InChIKey
- YSONQVIVMGOLBG-UMSFTDKQSA-N
- SMILES
- Fc1c(c(c(c(c1F)F)OC(=O)[C@@H](NC(=O)OCC5c6c(cccc6)c7c5cccc7)CC(=O)NC(c4ccccc4)(c3ccccc3)c2ccccc2)F)F
Safety
- WGK Germany
- WGK 2 water endangering
- HS Code
- 2924 29 70
- Storage Class
- 11 - Combustible Solids
- Hazard Classifications
- Skin Irrit. 2
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
- Precautionary statements
-
P264Wash hands thoroughly after handling.
P264Wash skin thouroughly after handling.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P302+P352IF ON SKIN: wash with plenty of soap and water.
P332+P313IF SKIN irritation occurs: Get medical advice/attention.
N-Bromosuccinimide Price
- Product number
- 8.52132
- Product name
- Fmoc-Asn(Trt)-OPfp
- Purity
- Novabiochem?
- Packaging
- 5G
- Price
- $281
- Updated
- 2025/07/31
- Product number
- F604133
- Product name
- Fmoc-Asn(Trt)-OPfp
- Packaging
- 10mg
- Price
- $45
- Updated
- 2021/12/16
- Product number
- 094180
- Product name
- (S)-Perfluorophenyl 2-((((9H-fluoren-9-yl)methoxy)-carbonyl)amino)-4-oxo-4-(tritylamino)butanoate
- Purity
- 95+%
- Packaging
- 1g
- Price
- $114
- Updated
- 2021/12/16
- Product number
- 094180
- Product name
- (S)-Perfluorophenyl 2-((((9H-fluoren-9-yl)methoxy)-carbonyl)amino)-4-oxo-4-(tritylamino)butanoate
- Purity
- 95+%
- Packaging
- 5g
- Price
- $303
- Updated
- 2021/12/16
- Product number
- 100305
- Product name
- Fmoc-Asn(Trt)-OPfp
- Purity
- ≥98.00%
- Packaging
- 25g
- Price
- $469
- Updated
- 2021/12/16
FMOC-ASN(TRT)-OPFP Chemical Properties,Usage,Production
Uses
peptide synthesis
General Description
The product number for this product was previously 04-12-1538.
To obtain a certificate of analysis (CoA) of a lot that begins with the letter “A”, please select the option in the right hand menu “Request a COA for Lot#s starting with A”.
reaction suitability
reaction type: Fmoc solid-phase peptide synthesis
Synthesis
(1) 25 kg of maleic anhydride waste residue added to 200 liters of tap water, heated to 85 C to make the waste residue dissolved, filtration to remove insoluble matter, add 0.5 kg of thiourea, hydrochloric acid to adjust the pH of the system to 3, heated reflux for 2.5 hours, cooling precipitation of crystals, and filtration of 17.6 kg of solid.
(2) the above obtained 17.6 kg of solid with 180 kg of tap water heated to 90 C to dissolve, add 2 kg of activated carbon heated reflux 1 hour decolorization, while hot filtration and removal of impurities, the filtrate pH with ammonia to 10, to the filtrate to add 44 grams of Escherichia coli, the reaction for 5 hours with 10 wt% hydrochloric acid solution to adjust the pH to 6, cooled dialysis of the crystals, filtration to get 15.7 kg of solid.
(3) Soak 15.7 kg of solid obtained above with 157 kg of ethanol at 20C for 5 hours, filter to obtain 5.8 kg of crystals, and bake the obtained crystals at 80C for 8 hours to obtain 4.9 kg of product, which is asparagine, and the HPLC content is 97.4%.
FMOC-ASN(TRT)-OPFP Preparation Products And Raw materials
Raw materials
Preparation Products
FMOC-ASN(TRT)-OPFP Suppliers
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View Lastest Price from FMOC-ASN(TRT)-OPFP manufacturers
- Product
- FMOC-ASN(TRT)-OPFP 132388-64-8
- Price
- US $1.00/KG
- Min. Order
- 1KG
- Purity
- 99%
- Supply Ability
- 20kg
- Release date
- 2018-08-22