ChemicalBook > CAS DataBase List > 6-Bromo-5-methoxypicolinic acid

6-Bromo-5-methoxypicolinic acid

Product Name: 6-Bromo-5-methoxypicolinic acid
CAS No.: 54232-43-8
Chemical Name: 6-Bromo-5-methoxypicolinic acid
Synonyms: 6-BROMO-5-METHOXYPICOLINIC ACID;6-bromo-5-methoxypyridine-2-carboxylicaci;6-bromo-5-methoxypyridine-2-carboxylic acid;2-Bromo-3-methoxypyridine-6-carboxylic acid;6-BROMO-5-METHOXY-2-PYRIDINECARBOXYLIC ACID;2-Pyridinecarboxylic acid, 6-bromo-5-methoxy-;6-Bromo-5-methoxy-2-pyridinecarboxylic acid ,97%;6-Bromo-5-Methoxy-2-Pyridinecarboxylic Acid 6-Bromo-5-Methoxy-2-Pyridinecarboxylic Acid ,97%
CBNumber: CB9304947
Molecular Formula: C7H6BrNO3
Formula Weight: 232.03
MOL File: 54232-43-8.mol

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6-Bromo-5-methoxypicolinic acid Property

Boiling point:: 362.8±42.0 °C(Predicted)
Density: 1.713±0.06 g/cm3(Predicted)
storage temp.: under inert gas (nitrogen or Argon) at 2-8°C
pka: 3.52±0.10(Predicted)
Appearance: White to off-white Solid
InChI: InChI=1S/C7H6BrNO3/c1-12-5-3-2-4(7(10)11)9-6(5)8/h2-3H,1H3,(H,10,11)
InChIKey: WOXIJGVDMQJTAC-UHFFFAOYSA-N
SMILES: C1(C(O)=O)=NC(Br)=C(OC)C=C1

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Safety

Risk Statements: 36/37/38
Safety Statements: 26-37/39
HS Code: 29339900

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

Precautionary statements

P280Wear protective gloves/protective clothing/eye protection/face protection.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

Biosynth Carbosynth

Product number: FB139448
Product name: 6-Bromo-5-methoxypicolinic acid
Packaging: 50mg
Price: $65
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FB139448
Product name: 6-Bromo-5-methoxypicolinic acid
Packaging: 100mg
Price: $100
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FB139448
Product name: 6-Bromo-5-methoxypicolinic acid
Packaging: 250mg
Price: $175
Updated: 2021/12/16

AK Scientific

Product number: Z3030
Product name: 6-Bromo-5-methoxy-2-pyridinecarboxylicacid
Packaging: 1g
Price: $222
Updated: 2021/12/16

Matrix Scientific

Product number: 082355
Product name: 6-Bromo-5-methoxypyridine-2-carboxylic acid
Purity: 97%
Packaging: 1g
Price: $223
Updated: 2021/12/16

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6-Bromo-5-methoxypicolinic acid Chemical Properties,Usage,Production

Chemical Properties

White solid

Synthesis

2-Bromo-3-methoxy-6-methylpyridine 760 mg (3.76 mmol) was dissolved in 15 ml of water, and to the resulting solution was added potassium permanganate (KMnO4) (1.49 g, 9.40mmol) and the mixture was heated at 80 °C for 3 hrs. After TLC was conducted, pH was adjusted to 4 with 10 percent hydrochloric acid (HCl) and filtration was conducted with celite. The filtrate was extracted with 50 ml of ethyl acetate (EA). The organic layer was treated with magnesium sulfate (MgSO4) and filtered, and the solution was concentrated to give 6-Bromo-5-methoxypicolinic acid as a white solid (665 mg, 2.87 mmol, 75 percent) without purification.

References

[1] Journal of Organic Chemistry, 1996, vol. 61, # 14, p. 4623 - 4633
[2] Patent: EP3255042, 2017, A2. Location in patent: Paragraph 0122; 0125
[3] Tetrahedron Letters, 1995, vol. 36, # 30, p. 5319 - 5322
[4] Patent: WO2014/78690, 2014, A1. Location in patent: Paragraph 00201
[5] Patent: WO2016/29214, 2016, A1. Location in patent: Page/Page column 148

6-Bromo-5-methoxypicolinic acid Preparation Products And Raw materials

Raw materials

Ammonium hydroxide Hydrogen peroxide Potassium carbonate 3-Hydroxy-6-methylpyridine Sodium nitrite 5-Amino-2-methylpyridine Hydrogen bromide Potassium permanganate Methanol Iodomethane Dimethyl sulfate

Preparation Products

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View Lastest Price from 6-Bromo-5-methoxypicolinic acid manufacturers

Career Henan Chemical Co

Product: 2-Bromo-3-methoxypyridine-6-carboxylic acid 54232-43-8
Price: US $1.00/g
Min. Order: 1g
Purity: 99%
Supply Ability: 1ton
Release date: 2020-01-10

Career Henan Chemical Co

Product: 6-BROMO-5-METHOXY-2-PYRIDINECARBOXYLIC ACID 54232-43-8
Price: US $1.00/KG
Min. Order: 1KG
Purity: 95-99%
Supply Ability: 1ton
Release date: 2020-01-08

54232-43-8, 6-Bromo-5-methoxypicolinic acidRelated Search:

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6-BROMO-5-METHOXY-2-PYRIDINECARBOXYLIC ACID

6-BROMO-5-METHOXYPICOLINIC ACID

2-Bromo-3-methoxypyridine-6-carboxylic acid

6-bromo-5-methoxypyridine-2-carboxylic acid

6-Bromo-5-methoxy-2-pyridinecarboxylic acid ,97%

6-Bromo-5-Methoxy-2-Pyridinecarboxylic Acid 6-Bromo-5-Methoxy-2-Pyridinecarboxylic Acid ,97%

2-Pyridinecarboxylic acid, 6-bromo-5-methoxy-

6-bromo-5-methoxypyridine-2-carboxylicaci

54232-43-8

Carboxylic Acids

Pyridines

Pyridine series