Cobalt carbonyl

ChemicalBook > CAS DataBase List > Cobalt carbonyl

Description Reaction Sources

Product Name: Cobalt carbonyl
CAS No.: 10210-68-1
Chemical Name: Cobalt carbonyl
Synonyms: Co2(CO)8;DICOBALT OCTACARBONYL;DicobaL;t OctacarbonyL;cobaltcarbonyle;COBALT CARBONYL;dicobaltcarbonyl;cobaltoctacarbonyl;carbonyl,tetra-cobal;OCTACARBONYLDICOBALT
CBNumber: CB9432426
Molecular Formula: C8Co2O8+4
Formula Weight: 341.95
MOL File: 10210-68-1.mol

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Cobalt carbonyl Property

Melting point:: 51-52 °C
Boiling point:: 52°C
Density: 1.81
vapor pressure: 9.333-200Pa at 15-25℃
Flash point:: -13 °C
storage temp.: 2-8°C
solubility: Dichloromethane (Slightly), Methanol (Slightly)
form: crystal
Specific Gravity: 1.73
color: dark orange
Water Solubility: Insoluble in water. Soluble in alcohol, ether and carbon disulfideSoluble in ether, naphtha and carbon disulfide. Slightly soluble in alcohol. Insoluble in water.
Sensitive: Air Sensitive
Hydrolytic Sensitivity: 7: reacts slowly with moisture/water
Merck: 13,3112
Exposure limits: TLV-TWA: 0.1 mg/m³ as Co (ACGIH)
PEL-TWA: 0.1 mg/m³ as Co (OSHA).
Stability:: Air sensitive
CAS DataBase Reference: 10210-68-1(CAS DataBase Reference)
EPA Substance Registry System: Cobalt carbonyl (10210-68-1)

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Safety

Hazard Codes: F,Xn,T+
Risk Statements: 11-22-40-43-48/20-52/53-62-26
Safety Statements: 36/37-61-45-28
RIDADR: UN 3190 4.2/PG 2
WGK Germany: 3
RTECS: GG0300000
F: 23-25
TSCA: No
HazardClass: 4.1
PackingGroup: II
HS Code: 29319090
Hazardous Substances Data: 10210-68-1(Hazardous Substances Data)
Toxicity: LD50 in mice, rats (mg/kg): 377.7, 753.8 by gavage (Spiridonova, Shabalina)

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Danger

Hazard statements

H251Self-heating; may catch fire

H302Harmful if swallowed

H315Causes skin irritation

H317May cause an allergic skin reaction

H330Fatal if inhaled

H351Suspected of causing cancer

H373May cause damage to organs through prolonged or repeated exposure

H412Harmful to aquatic life with long lasting effects

Precautionary statements

P201Obtain special instructions before use.

P235Keep cool.

P273Avoid release to the environment.

P280Wear protective gloves/protective clothing/eye protection/face protection.

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N-Bromosuccinimide Price

Sigma-Aldrich

Product number: 60811
Product name: Cobalt carbonyl
Purity: 96%
Packaging: 5g
Price: $393
Updated: 2024/03/01

Sigma-Aldrich

Product number: 60811
Product name: Cobalt carbonyl
Purity: 96%
Packaging: 25g
Price: $520
Updated: 2024/03/01

TCI Chemical

Product number: D3213
Product name: Dicobalt Octacarbonyl (stabilized with 1-5% Hexane)
Packaging: 5g
Price: $179
Updated: 2024/03/01

TCI Chemical

Product number: D3213
Product name: Dicobalt Octacarbonyl (stabilized with 1-5% Hexane)
Packaging: 25g
Price: $548
Updated: 2024/03/01

Alfa Aesar

Product number: 013060
Product name: Octacarbonyldicobalt, stab. with 1-5% hexane
Packaging: 2.5g
Price: $73.65
Updated: 2024/03/01

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Cobalt carbonyl Chemical Properties,Usage,Production

Description

Cobalt carbonyl (known as dicobalt octocarbonyl) is a versatile reagent and catalyst in organometallic chemistry and organic synthesis. It has catalytic applications in various chemical reactions such as hydroformylation of unsaturated compound, homogeneous hydrogenation of aromatic hydrocarbons, hydrosilation of alkenes, reactions of disulfides such as carbonylation to thio-esters and desulfurization to sulfides, hydroformylation as well as the conversion of alkenes into aldehydes. It can also promote both the Pauson-Khand reactions and Nicholas reaction.

Reaction

Reagent for the Pauson-Khand conversion of an olefin, an alkyne and carbon monoxide into a cyclopentenone.
Precatalyst in combination with triphenylphosphite for the cataytic Pauson-Khand reaction.
Catalyzes the rearrangement of 1-alkynylcyclopropanols to cyclopentenones.
Catalyzes the conversion of aziridines to β-lactams.
Catalyzes the conversion of diallylanilines and aryliminies to quinolines.
Reagent for the selective cleavage of benzyl ethers.
Domino Nicholas and Pauson-Khand process induced by nitroarene reduction.

Sources

Adkins, Homer., and G. Krsek. JACS 71.9(1949):3051-3055.
Feder, Harold M., and J. Halpern. Cheminform 7.7(1976):no-no.
Seitz, Friedrich, and M. S. Wrighton. Angewandte Chemie International Edition 27.2(1988):289-291.
Antebi, Shlomo, and H. Alper. Tetrahedron Letters 16.38(1985):no-no.
Krafft, Marie E., L. V. R. Boñaga, and C. Hirosawa. Cheminform 32.37(2001):no-no.
https://en.wikipedia.org/wiki/Dicobalt_octacarbonyl

Description

Cobalt carbonyl is a pyrophoric (spontaneously flammable in air), red-orange (when pure) to darkbrown crystalline solid. Molecular weight =341.94; Boilingpoint =(decomposes) 52℃; Freezing/Melting point =(decomposes) 50.5℃; Vapor pressure = 0.7 mmHg at 25℃.Hazard Identification (based on NFPA-704 M RatingSystem): Health 3, Flammability 3, Reactivity 2 .Insoluble in water.

Chemical Properties

red-orange to dark red crystals or flakes

Chemical Properties

Cobalt carbonyl is a pyrophoric (spontaneously flammable in air), red-orange (when pure) to dark-brown crystalline solid.

Physical properties

Orange crystals; density 1.78 g/cm³; melts at 5l°C; decomposes above this temperature; insoluble in water; soluble in most organic solvents including alcohol, ether, carbon disulfide.

Uses

The use of dicobalt octacarbonyl as a catalyst in a variety of organic syntheses has led to the study of an extensive and important organometallic chemistry of cobalt.

Uses

Cobalt carbonyl [Co₂(CO)₈] is commonly used as a catalyst in the hydroformylation (oxo reaction) of alkenes.
Along with pyridine, it can be used as a catalyst in the carboxylation of alkenes into corresponding acids and esters.
It is employed as a key precursor in the preparation of cobalt platinum (CoPt₃), cobalt sulfide (Co₃S₄) and cobalt selenide (CoSe₂) nanocrystals.
It is also used as a reagent in Pauson-Khand cyclizations and Nicholas reaction.

Uses

Cobalt octacarbonyl is used as a catalyst in the Oxo process. It also is used as a catalyst for hydrogenation, isomerization, hydrosilation and polymerization reactions. The compound is also a source of producing pure cobalt metal and its purified salts.

Uses

It is used as a catalyst in many organicconversion reactions, which include hydrogenation,isomerization, hydroformylation,polymerization, and carbonylation.

Preparation

Cobalt octacarbonyl is prepared by the reaction of finely divided cobalt with carbon monoxide under pressure:
2Co + 8CO → Co₂(CO)₈
The compound may be prepared in a similar way from cobalt(II) iodide. Also, it may be prepared by thermal decomposition of cobalt carbonyl hydride:
2HCo(CO)₄ → Co₂(CO)₈ + H₂

Hazard

Toxic by ingestion and inhalation.

Health Hazard

Dicobalt octacarbonyl exhibits moderate toxicityby inhalation route and somewhatlower toxicity by intraperitoneal and oralroutes. However, it is much less toxicthan nickel tetracarbonyl or iron pentacarbonyl.A 2-hour LC50 value in mice isreported as 27 mg/m³ (Lewis 1996). Anoral LD50 value in rats is within the rangeof 750–800 mg/kg. It decomposes, evolvingtoxic carbon monoxide.

Safety Profile

Poison by inhalation and intraperitoneal routes. Questionable carcinogen. Decomposes in air to form a product that ignites spontaneously in air. "hen heated to decomposition it emits acrid smoke and fumes. See also CARBONYLS and COBALT COMPOUNDS.

Potential Exposure

This material is used as a catalyst for a number of reactions. It is also used in antiknock gasoline and for high-purity cobalt salts.

First aid

If this chemical gets into the eyes, remove anycontact lenses at once and irrigate immediately for at least15 min, occasionally lifting upper and lower lids. Seek medical attention immediately. If this chemical contacts theskin, remove contaminated clothing and wash immediatelywith soap and water. Seek medical attention immediately. Ifthis chemical has been inhaled, remove from exposure,begin rescue breathing (using universal precautions, including resuscitation mask) if breathing has stopped and CPR ifheart action has stopped. Transfer promptly to a medicalfacility. When this chemical has been swallowed, get medical attention. Give large quantities of water and inducevomiting. Do not make an unconscious person vomit.Medical observation is recommended for 24-48 h afterbreathing overexposure, as pulmonary edema may bedelayed. As first aid for pulmonary edema, a doctor orauthorized paramedic may consider administering a corticosteroid spray.

storage

Color Code—Red Stripe: Flammability Hazard:Store separately from all other flammable materials. Priorto working with this chemical you should be trained on itsproper handling and storage. Decomposes on exposure toair or heat; stable in atmosphere of hydrogen and carbonmonoxide. Store in airtight, unbreakable containers in acool, well-ventilated area away from strong oxidizers andacids.

Shipping

UN3124 Toxic solids, self-heating, n.o.s., Hazard Class: 6.1; 6.1-Poisonous materials, 4.2-Spontaneously combustible material. Technical Name Required. UN3190 Self-heating solid, inorganic, Hazard Class: 4.2; Labels: 4.2-Spontaneously combustible material, Technical Name Required. UN1325 Flammable solid, organic, n.o.s. Hazard Class: 4.1; Labels: 4.1-Flammable solid

Purification Methods

It forms orange-brown crystals on recrystallisation from n-hexane under a carbon monoxide atmosphere [Ojima et al. J Am Chem Soc 109 7714 1987; see also Hileman in Preparative Inorganic Reactions, Ed. Jolly, Vol 1 p 101 1987].

Incompatibilities

Incompatible with oxidizers (chlorates, nitrates, peroxides, permanganates, perchlorates, chlorine, bromine, fluorine, etc.); contact may cause fires or explosions. Keep away from alkaline materials, strong bases, strong acids, oxoacids, epoxides. Decomposes on exposure to air or heat (@ ~52°C) producing toxic fumes of cobalt and oxides of carbon

Cobalt carbonyl Preparation Products And Raw materials

Raw materials

Preparation Products

Propionaldehyde Butyraldehyde 1-Pentanol

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View Lastest Price from Cobalt carbonyl manufacturers

R&D Scientific Inc.

Product: Cobalt carbonyl (Dicobalt octacarbonyl) 10210-68-1
Price: US $890.00/g
Min. Order: 1g
Purity: 90
Supply Ability: 500 Kg
Release date: 2024-04-19

Henan Fengda Chemical Co., Ltd

Product: Cobalt carbonyl 10210-68-1
Price: US $35.00-1.20/kg
Min. Order: 1kg
Purity: 99%
Supply Ability: g-kg-tons, free sample is available
Release date: 2024-03-28

Hebei Yanxi Chemical Co., Ltd.

Product: Cobalt carbonyl 10210-68-1
Price: US $100.00-20.00/kgkg
Min. Order: 1kgkg
Purity: 99%
Supply Ability: 100 tons
Release date: 2023-10-09

10210-68-1, Cobalt carbonylRelated Search:

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OCTACARBONYLDICOBALT

carbonyl,tetra-cobal

Co2(CO)8

Cobalt carbonyl (Co2(CO)8)

Cobalt tetracarbonyl dimer

Cobalt, di-mu-carbonylhexacarbonyldi-

Cobalt, di-mu-carbonylhexacarbonyldi-, (Co-Co)

Cobalt,di-μ-carbonylhexacarbonyldi-,(Co-Co)

cobaltcarbonyl(asco)

cobaltcarbonyl(co2(co)8)

Octacarbonyldicobalt,stab. with 1-5% hexan

Cobalt, di-M-carbonylhexacarbonyldi-, (Co-Co)

Cobalt carbonyl Moistened with hexane (hexane 1-10%), >=90% (Co)

Di-μ-carbonylhexacarbonyldicobal

Cobalt tetracarbonyl dime

Octacarbonyldicobalt, stabilized

Cobalt carbonyl (Dicobalt octacarbonyl) (Stabilized with 1-5% hexanes)

cobaltcarbonyle

cobaltoctacarbonyl

cobalttetracarbonyldimer

Dicobalt carbonyl (Co2(CO)8)

dicobaltcarbonyl

di-mu-carbonylhexacarbonyldi-cobal

di-mu-carbonylhexacarbonyldi-cobal(co-co)

Di-mu-carbonylhexacarbonyldicobalt

di-mu-carbonylhexacarbonylidicobalt

Dicobalt octacarbonyl, stabilized, 95% 5GR

Dicobalt octacarbonyl(Stabilised with 1-5% hexane) Co2(CO)8

Dicobalt octacarbonyl(Stabilised with 1-5% hexane)

Dicobalt Octacarbonyl (stabilized with 1-5% Hexane)

Dicobalt octacarbonyl ,94% [stabilized]

Cobalt carbonyl purum, moistened with hexane (hexane 1-10%)

COBALT CARBONYL, MOISTENED WITH HEXANE

contains1-5%hexaneasastabilizer

Dicobalt octacarbonyl, stabilized, 95%

Dicobalt octacarbonyl, 95%, stabilized

DICOBALT OCTACARBONYL

COBALT CARBONYL

COBALT TETRACARBONYL

Cobaltcarbonyl(Dicobaltoctacarbonyl)(Stabilizedwith1-5%hexane)

Enquiry for Octacarbonyl Dicobalt

COBALT CARBONYL: STABILIZED WITH 1-5% HEXANE

Octacarbonyldicobalt, stab. with 1-5% hexane

Cobalt octacarbonyl (Co2(CO)8)

Di-μ-carbonylhexacarbonyldicobalt

Cobalt Carbonyl Octacarbonyldicobalt

Di-my-carbonylhexacarbonyldicobalt

Dicobalt Octacarbonyl (stabilized with 5-10% Hexane)

DicobaL

t OctacarbonyL

COBALT CARBONYL ISO 9001：2015 REACH

3-methyl-1,1,1,3,3,3-hexakis(oxidaniumylidynemethyl)-2,4-dioxo-1,3-dicobaltabicyclo[1.1.0]butane-1,1,1,3,3,3-hexauide

Octacarbonyldicobalt, contains 1-5% hexane as a stabilizer

Carbon monooxide - cobalt (4:1)

Cobalt carbonyl (Dicobalt octacarbonyl)

10210-68-1

C8Co2O8

C8O8Co2