5-BROMO-2-NITRO-BENZOIC ACID
Uses- Product Name
- 5-BROMO-2-NITRO-BENZOIC ACID
- CAS No.
- 6950-43-2
- Chemical Name
- 5-BROMO-2-NITRO-BENZOIC ACID
- Synonyms
- 5-Bromo-2-nitrobenzoicaci;5-BROMO-2-NITRO-BENZOIC ACID;Benzoic acid, 5-bromo-2-nitro-;5-BROMO-2-NITRO-BENZOIC ACID >98%
- CBNumber
- CB9694158
- Molecular Formula
- C7H4BrNO4
- Formula Weight
- 246.01
- MOL File
- 6950-43-2.mol
5-BROMO-2-NITRO-BENZOIC ACID Property
- Melting point:
- 139-141°C
- Boiling point:
- 382.08°C (rough estimate)
- Density
- 2.0176 (rough estimate)
- refractive index
- 1.6500 (estimate)
- storage temp.
- Sealed in dry,Room Temperature
- form
- powder
- pka
- 1.85±0.25(Predicted)
- color
- Light creamy gold
- InChI
- InChI=1S/C7H4BrNO4/c8-4-1-2-6(9(12)13)5(3-4)7(10)11/h1-3H,(H,10,11)
- InChIKey
- FNINYRSNPGPWEL-UHFFFAOYSA-N
- SMILES
- C(O)(=O)C1=CC(Br)=CC=C1[N+]([O-])=O
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Danger
- Hazard statements
-
H314Causes severe skin burns and eye damage
- Precautionary statements
-
P260Do not breathe dust/fume/gas/mist/vapours/spray.
P264Wash hands thoroughly after handling.
P264Wash skin thouroughly after handling.
P270Do not eat, drink or smoke when using this product.
P271Use only outdoors or in a well-ventilated area.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P301+P330+P331IF SWALLOWED: Rinse mouth. Do NOT induce vomiting.
P303+P361+P353IF ON SKIN (or hair): Remove/Take off Immediately all contaminated clothing. Rinse SKIN with water/shower.
P403+P233Store in a well-ventilated place. Keep container tightly closed.
P405Store locked up.
P501Dispose of contents/container to..…
N-Bromosuccinimide Price
- Product number
- B697960
- Product name
- 5-Bromo-2-nitrobenzoicacid
- Packaging
- 1g
- Price
- $75
- Updated
- 2021/12/16
- Product number
- FB37399
- Product name
- 5-Bromo-2-nitrobenzoic acid
- Packaging
- 500mg
- Price
- $85
- Updated
- 2021/12/16
- Product number
- FB37399
- Product name
- 5-Bromo-2-nitrobenzoic acid
- Packaging
- 1g
- Price
- $136.8
- Updated
- 2021/12/16
- Product number
- OR59833
- Product name
- 5-Bromo-2-nitrobenzoicacid
- Packaging
- 25g
- Price
- $209
- Updated
- 2021/12/16
- Product number
- FB37399
- Product name
- 5-Bromo-2-nitrobenzoic acid
- Packaging
- 2g
- Price
- $218.8
- Updated
- 2021/12/16
5-BROMO-2-NITRO-BENZOIC ACID Chemical Properties,Usage,Production
Uses
5-Bromo-2-nitrobenzoic acid is a carboxylic acid derivative and can be used as an organic intermediate.
Chemical Properties
Colorless crystal
Synthesis
585-76-2
6950-43-2
3-Bromobenzoic acid (249 g, 1.24 mol, 1.0 eq.) was suspended in concentrated sulfuric acid (800 mL), and the suspension was cooled to 0 °C. The solution was then mixed with nitric acid (57.2 mL, 1.2 mol). Nitric acid (57.1 mL, 1.2 mol) was slowly added dropwise with stirring. After the dropwise addition was completed, the reaction mixture was gradually warmed to 20 °C and stirring was continued for 1 hour. After completion of the reaction, the mixture was carefully poured into ice water (2 L). The precipitate precipitated was collected by filtration, washed sequentially with water (1000 mL x 2) and dried to give 5-bromo-2-nitrobenzoic acid (280 g, 1.14 mol, 91.94% yield) as a white solid. The product was characterized by 1H NMR (400 MHz, DMSO-d6): δ= 14.12 (br.s, 1H), 8.00 (d, J = 1.8 Hz, 1H), 7.98-7.90 (m, 2H).
References
[1] Patent: US2017/190713, 2017, A1. Location in patent: Paragraph 0188
[2] Small, 2015, vol. 11, # 33, p. 4090 - 4096
5-BROMO-2-NITRO-BENZOIC ACID Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 5-BROMO-2-NITRO-BENZOIC ACID manufacturers
- Product
- 5-BROMO-2-NITRO-BENZOIC ACID 6950-43-2
- Price
- US $150.00-450.00/KG
- Min. Order
- 1KG
- Purity
- 98%
- Supply Ability
- 3MT per month
- Release date
- 2023-04-02
- Product
- 5-Bromo-2-nitrobenzoic acid 6950-43-2
- Price
- US $0.00/kg
- Min. Order
- 1kg
- Purity
- 98%
- Supply Ability
- 2000kg
- Release date
- 2023-06-09
- Product
- 5-BROMO-2-NITRO-BENZOIC ACID 6950-43-2
- Price
- US $15.00-10.00/KG
- Min. Order
- 1KG
- Purity
- 99%+ HPLC
- Supply Ability
- Monthly supply of 1 ton
- Release date
- 2021-07-10