3-Methoxyphenylhydrazine hydrochloride

Product Name: 3-Methoxyphenylhydrazine hydrochloride
CAS No.: 39232-91-2
Chemical Name: 3-Methoxyphenylhydrazine hydrochloride
Synonyms: m-Methoxyphenylhydrazine hydrochloride;Nsc155337;3-Methoxyphenylhydra;3-METHOXYPHENYLHYDRAZINE HCL;3-METHOXYPHENYLHYDRAZINE HYDROCHLORIDE;3-Methoxyphenylhydrazine hydrochloride, 98+%;Hydrazine, (3-methoxyphenyl)-, monohydrochloride;3-Methoxyphenylhydrazine hydrochloride, 98% (Custom work)
CBNumber: CB9759387
Molecular Formula: C7H11ClN2O
Formula Weight: 174.63
MOL File: 39232-91-2.mol

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3-Methoxyphenylhydrazine hydrochloride Property

Melting point:: 142°C (dec.)
storage temp.: Inert atmosphere,2-8°C
form: powder
color: Off-white
BRN: 5304389
InChI: InChI=1S/C7H10N2O.ClH/c1-10-7-4-2-3-6(5-7)9-8;/h2-5,9H,8H2,1H3;1H
InChIKey: GMXFZBZOVZOYNQ-UHFFFAOYSA-N
SMILES: C1C(OC)=CC=CC=1NN.Cl
CAS DataBase Reference: 39232-91-2(CAS DataBase Reference)

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Safety

Hazard Codes: Xi
Risk Statements: 20/21/22-36/37/38-22
Safety Statements: 26-36/37/39-36/37
RIDADR: 2811
HazardClass: 6.1
PackingGroup: III
HS Code: 29280000

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H301Toxic if swalloed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P405Store locked up.

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N-Bromosuccinimide Price

TRC

Product number: M350283
Product name: (3-Methoxyphenyl)hydrazineHydrochloride
Packaging: 10g
Price: $75
Updated: 2021/12/16

Usbiological

Product number: 281532
Product name: 3-Methoxyphenylhydrazine HCl
Packaging: 25g
Price: $410
Updated: 2021/12/16

Oakwood

Product number: 043642
Product name: 3-Methoxyphenyl hydrazine hydrochloride
Packaging: 1g
Price: $9
Updated: 2021/12/16

Matrix Scientific

Product number: 021395
Product name: 3-Methoxyphenylhydrazine hydrochloride
Purity: 98%
Packaging: 5g
Price: $10
Updated: 2021/12/16

AK Scientific

Product number: W5966
Product name: 3-Methoxyphenylhydrazinehydrochloride
Packaging: 1g
Price: $17
Updated: 2021/12/16

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3-Methoxyphenylhydrazine hydrochloride Chemical Properties,Usage,Production

Chemical Properties

PINKISH TO PINK-BROWNISH POWDER

Uses

(3-Methoxyphenyl)hydrazine Hydrochloride can be used to treat brain disorders.

Synthesis

3-Methoxyaniline (0.50mol, 65.6g, 1eq) was mixed well with 416g 18% H2O-HCl (2.0mol, 213g, 4eq) solution and cooled down to 0 to -5??C. Sodium nitrite (0.51 mol, 35 g, 1.02 eq) was weighed to prepare a 30% aqueous solution with 82 g of water, and the solution was slowly added dropwise to the system, and no raw material was detected after 1 h. The diazonium salt system was obtained.

Potassium sulfite (0.87 mol, 144 g, 1.74 eq) was dissolved in 800 g of water, and dilute hydrochloric acid was added to adjust the pH to between 6-8, and cooled down to 0 ??C. The diazonium salt system was added dropwise into potassium sulfite, while 15% potassium hydroxide aqueous solution was added dropwise to control the PH between 6-8, after dropping and adding, the system was kept warm at 0?? for 1h, then the system was heated at 60?? for 2h, and no diazonium salt was detected. Move the system to the reactor, add 1.06g of palladium carbon, pressurized with hydrogen at 4MPa, heated at 90?? for 6h, and detected.

To the system add hydrochloric acid (2mol, 200g, 4eq, 36%), heating at 100 ?? for 2h, the system is clarified, filtration, filtrate cooling precipitation crystals; the system is filtered, the cake is 130g of wet product, content of 63%; yield 93.8%.

3-Methoxyphenylhydrazine hydrochloride Preparation Products And Raw materials

Raw materials

Stannous chloride dihydrate m-Anisidine Sodium nitrite Ethyl acetate Hydrochloric acid Sulfuric acid

Preparation Products

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3-Methoxyphenylhydrazine hydrochloride Suppliers

China 135 Germany 2 India 5 United Kingdom 5 United States 14 Global 161

Nanjing Chalf-Pharm Technology Co., Ltd.

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Country: China
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Jinan Liheng Biotechnology Co., Ltd.

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Advantage: 58

J & K SCIENTIFIC LTD.

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Country: China
ProdList: 96815
Advantage: 76

Meryer (Shanghai) Chemical Technology Co., Ltd.

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Fax: 86-21-61259102
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Country: China
ProdList: 40228
Advantage: 62

Alfa Aesar

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Fax: 021-67582001/03/05
Email: saleschina@alfa-asia.com
Country: China
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Energy Chemical

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JinYan Chemicals(ShangHai) Co.,Ltd.

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Jia Xing Isenchem Co.,Ltd

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Country: China
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Shanghai Longsheng chemical Co.,Ltd.

Tel: 021-58099652-8005 13585536065
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Country: China
ProdList: 9892
Advantage: 59

Nanjing Chemlin Chemical Co., Ltd

Tel: 025-83697070 13913916777;
Fax: +86-25-83453306
Email: info@chemlin.com.cn
Country: China
ProdList: 15724
Advantage: 64

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View Lastest Price from 3-Methoxyphenylhydrazine hydrochloride manufacturers

Shaanxi Dideu Medichem Co. Ltd

Product: 3-Methoxyphenylhydrazine hydrochloride 39232-91-2
Price: US $0.00-0.00/g
Min. Order: 10mg
Purity: 99%HPLC
Supply Ability: 2000tons
Release date: 2020-01-15

Career Henan Chemical Co

Product: 3-Methoxyphenylhydrazine hydrochloride 39232-91-2
Price: US $1.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: Customized
Release date: 2019-07-02

39232-91-2, 3-Methoxyphenylhydrazine hydrochlorideRelated Search:

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Hydrazine, (3-methoxyphenyl)-, monohydrochloride

m-Methoxyphenylhydrazine hydrochloride

Nsc155337

3-Methoxyphenylhydra

3-METHOXYPHENYLHYDRAZINE HCL

3-METHOXYPHENYLHYDRAZINE HYDROCHLORIDE

3-Methoxyphenylhydrazine hydrochloride, 98+%

3-Methoxyphenylhydrazine hydrochloride, 98% (Custom work)

39232-91-2